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In this paper,the forming mechanism and affecting favtor of bulk metallic glasses is systematically discussed from the aspects of thermodynamic, kinetic and microstructure . Thermodynamic factors which favor the amorphization of alloys analyzed, the glass forming range of ternary alloys system was proposed by using Miedema theory, Toop model and considering the influence of free energy of pure metals at different temperature. The approach was applied to predict the composition range of amorphous Mg-Cu-La alloys. Several methods(such as three empirical criterions ,binary alloys phase diagram , Miedema theory and Toop mode) were used to design a series of Mg65Cu25La10 、Mg68Cu17La15 and Mg57Cu23La20 alloys, These bulk amorphous alloys with maximum diameter thickness reaching to 1mm were prepared by means of graphite-molding casting though the raw materials are of a low purity by conventional casting processes at a low cooling rate.
本文从合金的热力学、动力学及结构形成条件方面系统的讨论了Mg 基大块非晶的形成机制及影响因素,并从非晶形成的热力学观点出发,综合应用Miedema理论和Toop 模型,并考虑纯金属在不同温度下的自由能,在此基础上提出了一种定量预测三元非晶合金形成范围的方法,用该方法计算Mg-Cu-La 三元合金系的非晶形成范围,应用多项技术(三经验原则、二元合金相图及Miedema 理论和Toop模型)设计了Mg65Cu25La10 、Mg68Cu17La15 和Mg57Cu23La20非晶合金。
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Through a variety of resin filter, adsorption and elution conditions for the optimization, as well as decolorization, crystallization methods of research, this article eventually determine the strong acid cation resin HZ-001 which is at pH 3, 3BV / h, having the largest adsorption to the tryptophan; the fermentation broth were centrifuged to remove sediment,then treated with activated carbon to be decolored and then treated with strong acid cation resin HZ-001. After that,2mol/l amino acid were passed through the HZ-001 ion exchanging column,kept almost constants when the flow rate stayed 6 BV / h. At 60℃,it was condensed into the saturated state and then added Ethanol until its percentage reaching 30%. At 4 ℃ under 100rpm placed in the shaker 20h, the collection of L-tryptophan was dried up in vacuo.
本文通过对种树脂的筛选、吸附和洗脱条件的优化,以及对脱色、结晶方法的研究与摸索,最终确定强酸型阳离子树脂HZ-001在pH=3,3倍床体积流速,温度室温,对色氨酸有最大的吸附作用;将发酵液离心去沉淀并用活性炭脱色后通过HZ-001强酸型阳离子交换树脂柱,再用2mol/L的氨水6倍床体积流速在室温下进行洗脱,收集洗脱液,60℃浓缩为过饱和状态后加入30%无水乙醇,4℃下100rpm摇起晶20h,过滤搜集结晶并真空干燥得白色粉片状L-色氨酸晶体。
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The barrier layer is removed, and the walls of the trench are etched in a manner that etches the lesser doped regions of the substrate at a higher rate than the higher doped regions of the substrate to widen and lengthen the trench and to form rounded corners at the intersections of the walls of the trench.
除去阻挡层,并以比衬底的更高掺杂区域更高的速率蚀刻衬底的更低掺杂区域的方式蚀刻沟槽壁,将沟槽加宽和加长并在沟槽壁的相交处形成圆角。
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Results: in contrast with model group, SSM can (1) increase the survival rate of ARF in rats, cut down Scr and BUN at 24hr, improve renal function, slightly surpass Vp in its therapeutic effect;(2) mitigate the extent of renal pathologicchanges, decrease the numbers of renal tubule necroses and casts;(3) protect renal ultrastructure such as microvilli, mitochondria, endoplasmic reticulum of TEC, podocytic process of glomerulus epithelial cell,endothelial cell etc, better than Vp;(4) enhance SOD activity, lower MDA contents in renal cortex;(5) enhance NO contents in serum, reduce ET levels in plasma;(6) evidently cut down TNF- a contents in serum, superior to Vp;(7) antagonize calcium overload in TEC;(8) alleviate renal pathological changes in ARF metaphase (at 3d), advance regeneration and recovery of TEC, restore renal structure in ARF convalescence (at 5d), and better than Vp;(9) increase the expression of TEC PCNA and prepro EGFmRNA in ARF metaphase.
结果:与模型组相比,SSM能(1)提高ARF大鼠的存活率,降低24hr时Scr及BUN,改善肾功能,其疗效略优于维拉帕米;(2)减轻ARF肾脏病变程度,减少24hr肾小管坏死数及管腔内管型数;(3)对肾脏的超微结构如肾小管上皮细胞微绒毛、线粒体、内质网、肾小球上皮细胞足突、内皮细胞等形态结构均有一定的保护作用,其疗效略优于维拉帕米;(4)提高肾皮质SOD活性,降低MDA含量;(5)提高血清NO水平,同时降低血浆ET含量;(6)显著降低血清TNF-α的水平,疗效明显优于维拉帕米;(7)拮抗小管上皮细胞[Ca~(2+)]_i的升高;(8)使ARF中期(第3d时)肾组织病变较同期其它两组明显减轻,并使肾小管细胞再生修复提前,至ARF恢复期(第5d时)肾组织结构恢复重建良好;作用明显优于维拉帕米;(9)促进ARF中期肾小管上皮细胞PCNA的表达及EGF前体mRNA的合成,从而增加EGF的合成释放,而维拉帕米无此作用。
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OBJECTIVE:To establish the RP-HPLC method for determination of methyl hydroxybenzoate and ethyl hydroxybenzoate in oral liquid preparations METHODS:The Nova-Park C18 column(3 9mm×150mm,5μm)was used The mobile phase consisted of acetonitrile-water(25∶75)at a flow rate of 1ml/min,the detection wavelength was set at 254nm and the sensitivity was set at 0 01 AUFS RESULTS:The linear ranges of methyl hydroxybenzoate and ethyl hydroxybenzoate were 0 4 412~13 2 360μg/ml(r=0 9 999) and 0 6 672~20 0 160μg/m...
目的 :建立内服液体制剂中羟苯甲酯和羟苯乙酯的反相高效液相色谱测定方法。方法:色谱柱:Nova -ParkC18 柱(3 9mm×150mm ,5μm);流动相:乙腈-水(25∶75);流速:1ml/min ;检测波长:254nm ;灵敏度:0 01AUFS。结果:羟苯甲酯浓度在0 4412~13 2360μg/ml范围内线性关系良好(r=0 9999);羟苯乙酯浓度在0 6672~20 0160μg/ml范围内线性关系良好(r=0 9998)。结论:该方法简便、快速、准确,可用于医院制剂中防腐剂的检测。
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Rated at extraction conditions, one pump is running, because the cycle of water to reduce the system's water resistance decrease the flow of water pumps 12274T / H, head will drop to 15.0-16.0 m, in the extraction steam turbine at the maximum operating conditions, the recycled water to meet the system requirements to run a pump, because of substantial reduction in the volume of water supplied, so that substantially improve pump head, a direct result of the cooling tower water gushing, increase淋水device with a flow rate of the sink, fill up water in the hot淋水exchange reduce the time and reduces the cooling effect of cooling towers.
在额定抽汽工况下,一台水泵运行,由于循环水量减少、系统的水阻下降,水泵的流量12274T/H,扬程将下降至15.0-16.0米,在汽轮机在最大抽汽工况时,为满足循环水系统要求运行一台水泵,由于供水量大幅度减少,使水泵扬程大幅度提高,直接造成冷却塔涌水,加大淋水装置配水槽的流速,水流在淋水填料上热交换的时间减少,降低了冷却塔的冷却效果。
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The experimental group received 10 weeks of walking exercise training, at 50 minuets per session, 5 days per week and at a exercise intensity limit between 60% and 70% maximum heart rate. The control group received ordinary special education curriculums. All participants completed three times of the PACER(Progressive Aerobic Cardiovascular Endurance Run)20-Meter Shuttle Run test and test for the average walking speed during 1600 meters:before the experiment started , after the experiment and the follow-up test at the fourteenth week of the experiment started. All results from these tests were recorded and analyzed by descriptive statistics; repeated measure t-test; the one way analysis of covariance .
实验组进行星期一至星期五每天一次,合计每周五次,每次50分钟,总共10周,运动强度为60%-70%最大心跳率的步行运动;控制组接受学校安排的特殊教育课程,两组学生在进行步行运动前、后以及实验处理结束后第四周,分别接受PACER渐进性心肺耐力跑-20 公尺和1600公尺的步行速度之测验,并将所得的成绩以描述性统计、重复量数t 考验、单因子共变数分析进行统计考验,评估实验处理之运动与维持成效。
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Initially, one specimen is tested at an irradiance of 25kW/m in the presence of a pilot flame and one specimen is tested at an irradiance of 25kW/m in the absence of a pilot flame to determine the mode which gives the quickest rate of smoke production.
首先,把一个样品用带有引燃火焰的25KW/m 的辐射进行测试,另外再用不带引燃火焰的25KW/m 的辐射进行测试,并用此来确定最快产生烟的一种方法。
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The programmed calcination process is necessary, that is, heating the as-elutedhmmersed oxalates mildly from room temperature to 300℃at a heating rate of 5℃/min, and keeping the samples at 300 C for 1 h; consecutively, heating to 900℃at 10℃/min, and then keeping for 4 h.
程控的烧结过程是必须的,这就是,按5度/分钟逐步加热按这种淋洗制备的草酸盐到300度,保温1小时;接着,按10度/分钟加热到900度,保温4小时。
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The difference in yield, its components, basic characteristics such as mean size and bare tip length of cobs, plant height, base internode diameter, secondary root number per plant, LAI and DMW at the same measuring date, between the three treatments were insignificant respectively; the optimized fertilization made the three leaves around corn cob rather smaller, the cob leaf slightly thinner, a decrease of the cob leaf chlorophyll content at greater rate at the later stage, and dry matter accumulation amount slightly reduced from flowering to grain filling.
在优化施肥、秸秆还田优化施肥及传统施肥条件下,夏玉米穗长、穗粗、秃顶长、株高、基部伸长节间粗度、单株各层次生根条数、同一时期的叶面积指数和干物质积累量无显著性差异。在优化施肥条件下,夏玉米棒三叶总叶面积略微减少,穗位叶叶片略微变薄,生育后期穗位叶叶绿素含量下降稍快,吐丝-收获的干物质积累量略有下降。
- 推荐网络例句
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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.
然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。
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Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.
镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。
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A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.
付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。