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The resules show that the optimal reaction conditions are as follows: tin octoate is used as catalyst; w(SnOct2)lw and w(nano-SiO2)/w is 1:400 and 1:20, respectively; the reaction temperature is 140 CC and the reaction time is 72 h. Under this conditions, composite withM of 1.5091×10^5 was obtained.
结果表明,最优的反应条件为:采用辛酸亚锡为催化剂,催化剂用量和二氧化硅用量分别为丙交酯用量的0.25%和5%,在140℃油浴中,氮气保护下反应72h,可得到重均分子量为1.5091×10^5的聚乳酸纳米二氧化硅复合材料。
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The product synthesized under the optimum conditions as follows had final acid value of 0.494 mgKOH/g,and conversion of reatants up to 99.59%,molar ratio of isooctanol to phthalic anhydride 3∶1,the dosage of both aluminium oxide and stannous octoate as catalyst 0.2%(based on the total mass of reactants),reaction time 2.5 hours.
考察了工艺条件对合成DOP的影响,结果表明,在异辛醇与苯酐摩尔比3∶1,氧化铝/辛酸亚锡复配催化剂用量分别占反应物总量的0.2%,反应温度230℃,反应时间2.5h的最佳工艺条件下,产品终点酸值0.494mgKOH/g,反应物转化率达99.59%。
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A novel biodegradable copolymer of poly and poly (γ-benzyl-L-glutamate) was successfully synthesized. Under appropriate conditions, the PBLG initiates the ring-opening polymerization of L-lactide to produce block copolymer, by using low toxicity stannous octoate as catalyst. The optimal reaction conditions were determined as follows; the catalytic agent: PBLG=1:1, the temperature is 120℃, the reaction time is 6h.
以L-丙交酯为原料,在催化剂辛酸锡酯Sn2的作用下,利用聚的活性端氨基引发LLA进行开环聚合,合成了聚L-丙交酯与聚的共聚物,对反应条件的各项因素进行了讨论,确定了最佳反应条件是:m:m=1:1;反应温度120℃;反应时间6h。
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According to the year with the best large-seed production, the reasons for empty seeds could be estimated as follows: Seed potential per cone calculated as 2 times the number of fertile ovuliferous scales was about 206 seeds. Percentages of seed losses resulting from pre-and post-pollination ovule abortion, prezygotic factors, embryo degeneration, and efficient seed were 33%, 27%, 39%, and%, respectively.
依据大粒种子产率最高的1年来估测空粒种子产生的因素,可以推估如下:依据每个可孕性鳞片所含2粒种子的鳞片数,潜力种子数约有206粒,再依此值算出受粉前后胚珠败育率、受精前败育率、胚败育率、及有效种子率分别为33%、27%、39%及%。
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The results were as follows: Cd, that existed as the acid extractable and the oxidable spesies with higher activity, could be bioavailable.
Zn、Mn元素主要以氧化物结合态为主,这类重金属离子在高还原条件下就释放出来,因而对作物和人类有潜在的危害。
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The optimum conditions were obtained as follows: the weight ratio of fatty acids and 85%acetic acid is 1:4, ozonolysis temperature is 20-25℃, manganese/copper acetate as catalyst, and the amount of catalyst is 0.15% of fatty acids, oxidation decomposition temperature and oxidation decomposition time are 90-95℃ and 4 hours respectively. the yields of azelaic acid and pelargonic acid are 57.4% and 51.6% respectively.
以菜油酸为原料、85%醋酸水溶液为溶剂,经臭氧化、氧化分解、重结晶等过程制备壬二酸和十三烷二酸的最佳反应条件为:m:m(85%醋酸)=1:4,臭氧化温度20-25℃;氧化分解温度80-85℃,催化剂醋酸锰/醋酸铜用量为原料菜油酸质量的0.12%,氧化分解时间3h,重结晶溶剂壬酸的用量为5倍质量的氧化分解产物时,十三烷二酸的收率为58.3%,壬二酸的收率为57.2%。
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We also studied their inhibition on H2O2,UV-induced hemolysis of RBC. Sodium paeonol sulfonate was used as keep-freshing agent in tomato storage and vitamin C content, brix, acidity, weight loss, membrane permeability, soluble protein content, SOD andPOD activity was determined. The results were as follows: Paeonol and sodiumpaeonol sulfonate had remarkably inhibitory effects on Xanthmonas oryzaepv.oryzicda,Pseudomonas solanacearum Smith, Phyllosticta mali Pril.et Delac.and Rhizoctonia solani Kuhn.
在生物学活性方面,检测了丹皮酚及丹皮酚磺酸钠对植物病原菌的抑制作用,测定了其清除超氧阴离子自由基(O_2~-)、羟自由基的活性及对过氧化氢(H_2O_2)和紫外线诱导红细胞溶血的影响,并用丹皮酚磺酸钠对樱桃番茄进行了保鲜研究,测定贮藏期间番茄的维生素C含量、糖度、酸度、失重率、膜透性、可溶性蛋白含量、超氧化物歧化物及过氧化物活性等。
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The technique comprises the steps as follows: using the waste filtered mud of the sugar-refinery as the material to generate gas which is dehydrated till the water content is less than and equal to 30 percent and through distribution (clay used for of 70.00 to 85.0 percent, dehydrated filtered mud of the sugar-refinery of 15.0 to 30.0 percent, intensifier carboxymethyl cellulose or propyloic fibrin is 0.1 percent of the total dosage of the below material), performaing, moulding with high temperature (800 to 1200 DEG C, 20 to 180min) and acquiring the multi-hole porcelain granule with 20 to 30 percent of poriness, 10 to 20 percent of water absorbing capacity and 1.5 to 7.5/MPa of cylinder pressing intensity.
一种糖厂滤泥生产多孔陶粒技术,是用糖厂废弃物滤泥为发气原料,经脱水至含水≤30%,经配料(陶瓷用黏土70.0~85.0%,糖厂脱水滤泥15.0~30.0%,增强剂羧甲基纤维素或羧乙基纤维素为上述原料总量的0.1%)、制坯、高温(800~1200℃,20~180min)成型,得到孔隙率20~30%、吸水率10~20%、筒压强度1.5~7.5/MPa的多孔陶粒。
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Methods subject selection criteria were as follows: fidelity 120 hires 90k implant(advanced bionics corporation, sylmar, ca) use for at least 6 months,considerable ability of communication and reasonable loudness scaling. a total of 20 prelingual children participated in the present study, with mean age 6.5 years(rang : 3 to 13 years). four cochlear electrodes (3,7,11 and 15) were stimulated as tested electrodes.
选择植入美国advanced bionics 公司的hires 90k人工耳蜗共20例语前聋患者,使用fidelity 120通道言语编码策略至少6个月时间,有一定交流能力,对声音的响度有辨别能力,年龄为3至13岁,平均年龄为6.5岁。
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Article 4 As a consulting service setup for REACH preregistration, Party B shall perform the obligations as follows
第四条 乙方作为 REACH 预注册的咨询服务机构,应履行下列义务
- 推荐网络例句
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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.
曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。
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The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.
稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。
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When I was in school, the rabbi explained everythingin the Bible two different ways.
当我上学的时候,老师解释《圣经》用两种不同的方法。