查询词典 antimony

The antimony doped tin oxide nanoparticles were synthesized at 240℃for 17 h by the complexing hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

摘 要：以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimony-doped tin oxide nanoparticles were synthesized at 240℃ for 17h by the complexing-hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合－水热氧化法在水热氧化温度为240℃和水热保温时间为17h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合－水热氧化合成机理进行探讨。

The study of the mineralogy indicates:(1)Few impurity and poor sulfur in thestibnite of Shalagang antimony.(2)From the stibnite's cell parameter, it finds that thecell parameter of Shalagang antimony's stibnite approachs the standard value. And iteduces the forming temperature of the stibnite is between 150℃～200℃.(3)Thequartz in different period have different thermoluminescence curve, and thethermoluminescence curves of the quartz in rich ore havethe characters of gently curve, unconspicuous peak and the luminous intensity has therelationship of positive correlation with the temperature.

矿物学研究发现：(1)沙拉岗锑矿床辉锑矿以所含杂质少，贫硫为主要特征；(2)利用晶胞参数测定得出，沙拉岗锑矿床辉锑矿晶胞参数接近于标准值，推算形成温度在150℃～200℃之间；(3)不同期次石英具有明显不同的热释光曲线，其中主成矿期石英的热释光曲线以发光曲线平缓，峰位不明显，发光强度随温度升高而增强为特征。

Antimony and its compounds occur widely in the supergene environment induced by natural processes and human activities, and lead to increasing contamination of antimony.

由于自然过程和人为活动的影响，锑及其化合物广泛分布于大气、土壤、水体等表生环境中，锑的环境污染日益严重。

Carbon disulfide, dialkylamine, antimony trioxide have been used to synthesize the other organic antimony compounds-dialkyldithiocarbamate. The optimal technological conditions and purificating method have been studied in detail.

以二硫化碳、二元仲胺、三氧化二锑为原料合成了结构为Sb-〓的另一类含Sb-S键的有机锑化合物，通过大量的实验探索，详细研究了各种二烷基二硫代氨基甲酸锑的最佳合成工艺条件及产品的提纯方法，为该类化合物的制备提供了一种工艺简便，收率较高的合成工艺途径。

Direct separation of lead and antimony from jamesonite by oxidizing volatilization roasting, with addition of one kind of catalyst; in addition, it discusses separately the factors that affect lead and antimony separation results under such process.

本试验研究了一种新工艺，通过加入一种催化剂，对脆硫铅锑矿进行氧化挥发焙烧，实现铅锑的一步分离；同时，对该工艺下影响脆硫铅锑矿铅锑分离效果的因素也分别进行了讨论。

The new synthesis techniques, applied properties, high-effect compounding optimization mathematical model, thermolytic dynamics of PVC stabilizing system containing organic antimony compounds, the accurate molecular structure and optimal geometry of antimony mercaptides and the heat stabilizing mechanism to PVC have been studied systematically.

据此，本文研究了性能优异，应用前景广阔的含Sb-S键的有机锑化合物的合成方法，应用性能、含有机锑热稳定体系的高效配方模式、热分解动力学及机制，以及从分子水平研究了疏醇锑分子的精确结构及其对PVC的热稳定作用机理。

When the temperature of a substrate is 250 DEG to 650 DEG C, the proportion of antimony doping to ZnO is controlled by adjusting the carrier gas flow rate of antimony metallorganic and zinc metallorganic to grow p type ZnO.

在衬底温度为250℃～650℃时，通过调节锑的金属有机物与锌的金属有机物源的载气流量来控制锑掺入ZnO的比例进行p型ZnO的生长。

The method is characterized in: with antimony metallorganic as the doping source of p type ZnO, antimony doping p type ZnO film is prepared by metal organic chemical vapor deposition.

其特征是采用锑的金属有机物做为p型ZnO的掺杂源，利用金属有机物化学气相沉积方法制备锑掺杂p型ZnO薄膜。

When the content of antimony in the doped film is overlarge, conducting property becomes badly due to the ion scattering of antimony.

当掺杂浓度过大时，掺杂离子对电子的电离杂质散射作用造成ATO薄膜的导电性能显著降低。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。