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The invention relates to an electrochemical method for preparing ultra-fine tantalum powder, wherein it uses the mixture slat flux with CaCl2 or CaCl2 as electrolyte; composites Ta2O5 powder/block with metal collector as solid cathode; uses graphite or inertia anode as anode; uses reference polar to control the electrolysis level, under inertia gas to electrolyze at 500-1000Deg. C; and the electrolysis time should make electrolysis electricity reach needed amount; reduces Ta2O5 into ultra-fine metal tantalum powder.

本发明涉及一种超细钽粉的电化学制备方法，以CaCl2或者含有CaCl2的混盐熔体为电解质，将Ta2O5粉末或块与金属集流体复合作为固态阴极，以石墨或惰性阳极作为阳极，用参比电极控制电解电位在惰性气氛保护下进行电解，电解温度控制在500-1000℃，控制电解时间使电解电量到达到理论所需电量及以上，将五氧化二钽电化学还原为超细金属钽粉。

The synthesis of the NiFe〓O〓 spinel matrix material, the utility of grain composition of the spinel ingredients when synthesizing the inert anode, and the synthesis of the inert anode was studied essentially in this thesis.

本文重点研究了镍铁尖晶石原料的合成，合成惰性阳极制品时原料的粒度配比和惰性阳极制品的合成。

The results show that Sb addition can diminish the crystal grain, but the content of segregative phase at crystal boundary increases, and the current efficiency of material is low. Compared with Sb addition, Sn addition can also diminish the crystal grain, the current efficiency increases, the content of segregative phase at crystal boundary reduces, but diffusional corrosion of the anode surface is not uniform. The cooperation of Sb and Sn can prevent Si from segregating effectively and enhance the current efficiency obviously. At the same time, anode materials have preferable surface dissolution characteristics.

结果表明： Sb具有细化晶粒的作用，但晶界存在较多偏析相，电流效率偏低；与Sb相比较， Sn也具有细化晶粒的作用，电流效率有所提高，晶界偏析相较少，但阳极的表面腐蚀溶解不均匀； Sn和Sb的协同作用在于能有效地抑制Si的偏析，显著提高阳极的电流效率，使得阳极表面具有良好的腐蚀溶解性。

At 25℃,in 30w/o KOH aqueous,when current density is 2000A/m 2,the evolution oxygen overpotential of the oxidized Ni anode decreases 260mV relative to unoxidized Ni anode.

常温下，电流密度2000A／m2电解30％KOH水溶液时，脉冲电流氧化的Ni阳极析O2超电势比普通Ni阳极下降260mV。

The invention discloses an electrochemical method for preparing a hydroxylapatite particle thin coating on the surface of a metal implant, which comprises the following steps: electrolyte is put into a container equipped with a constant temperature heating system and heated to be 30 DEG C to 95 DEG C, and then the temperature is kept; platinum is taken as the anode and evenly distributed around the container, and the metal implant is taken as the cathode, put in the middle of the container and totally soaked in the electrolyte; DC voltage of 2V to 4V is added between the anode and the cathode, the surface of the metal implant has cathode reduction reaction, the pH value is increased and the supersaturation degree of the hydroxylapatite is also increased, so as to crystalize on the surface of titanium; after 0.5h to 5h of deposition, a layer of hydroxylapatite particle thin coating which can be excellently adhered to the matrix metal is formed on the surface of the implant.

本发明公开了一种在金属植入体表面制备羟基磷灰石颗粒薄涂层的电化学方法，在装备了恒温加热系统的容器中装入电解液，并将电解液加热到30～95℃恒温；将铂作为阳极均匀分布在容器四周，金属植入体作为阴极置于容器中间，完全浸没在电解液中，两极之间加直流电压2～4V，金属植入体表面发生阴极还原反应，pH值升高，羟基磷灰石过饱和度增加，从而结晶在钛金属表面；经过0.5～5小时沉积后，在植入体表面即可形成一层与基体金属结合优良的、薄的羟基磷灰石颗粒薄涂层。

In the course of selecting oxide additives material in the nickel-ferric spinel based inert anode, both the solubility in the cryolite molted salt of oxide additives and the whole thermodynamics action in electrolyte of oxide additives are discussed in this article, thus to have a comparatively reasonable selection of the nickel-ferric spinel based inert anode material.

在选择镍铁尖晶石基惰性阳极材料氧化物添加剂过程中，不仅探讨了氧化物添加剂在冰晶石熔盐中的溶解度，而且还探讨了氧化物添加剂在电解液中的整个热力学行为，从而对镍铁尖晶石基惰性阳极材料做出了较为合理的选择。

Experimental and practical researches of impurity distribution activities and common effect, and analysis on the removing and distribution activity of the impurities in the Guixi Smelter anode copper like As Sb and Bi and the forming structure and conditions of the flotating anode slime have been done.

很久以来，许多从事冶金或相关专业的研究人员，对As、Sb、Bi、Pb等杂质在铜电解精炼过程中的行为进行了多项研究，如对存在形态和行为、阳极泥的形成机理，以及对阴极铜质量的影响进行了一系列的探索研究，并取得了可喜的科研成果。

The copper anode slime produced in one copper smelter domestically was pre-treated with pressure acid leaching method and the leaching behavior of copper,tellurium and selenium in copper anode slime was studied.

以国内某铜冶炼厂所产的铜阳极泥为原料，采用加压酸浸的方法对该铜阳极泥进行预处理，对铜阳极泥中铜、碲、硒等元素的浸出行为进行了研究。

The best combination of anode and cathode flow channel flow was anode flow channel cross-finger, the flow field composed of the cathode flow channel cross-refers was the best combination of flow field.

阳极流道与阴极流道的最佳组合为阳极交指流道、阴极交指流道组成的流场为最佳组合流场。

The formation of the striations was affected by the combination effect with the distribution of spatial potential and surface charge on the anode surface, especially the distribution of electron charge on the anode surface would greatly influence the structure of striations.

条纹现象的形成是由阳极表面附近的空间电势分布和表面电荷分布共同作用产生的，特别是表面的电子电荷分布对条纹现象的影响很大。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。