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In the paper, the present state of ultra-fine-grained materials, severe plastic deformation and Asymmetrical-ARB are introduced in detail; the craft to fabricate ultra-fine-grained copper using Asymmetrical -ARB is studied fully; the problem of combination of interface is settled; the affect of homogenizing annealing、 annealing and rolling method on mechanical properties of materials prepared by Asymmetrical-ARB is discussed and analyzed when control parameters of rolling mill such as the press—ratio、 the asynchronous rate、 rolling—speed are fixed, and a kind of craft that meets to requirement of experiment is made out.

本文对超细晶、大塑性变形技术、异步轧制目前国内外研究进行了详细的介绍；对异步叠轧方法制备超细晶铜工艺做了较为细致的研究：解决界面复合问题；在压下率、异步比、轧制速度等轧机控制参数固定条件下，探讨了均匀化退火工艺、去应力退火工艺和轧制方式对异步叠轧材料力学性能的影响，并进行了分析，制定出符合实验要求的轧制工艺。

The membranes were transformed from amorphous phase toα-Al_2O_3 crystalline phase by 5 hours annealing at 800℃and 910℃. At the same time, aluminum and amorphous alumina were found by XRD patterns. The membrane had little change in front side after 5 hours annealing at 800℃, while the back side was transformed from ruleless distributing to cluster distributing.

膜在800℃及910℃下退火5h后，由非晶态的氧化铝转变成为晶态的α-Al_2O_3，但同时也有铝单质和无定形结构的氧化铝存在，膜在800℃下退火5h后的正面没有太大变化，背面由无规则的分布变为簇状分布。

However, it is difficult for the quartz substrate to scale-down by photolithography. In this article, we develop another type of piezoelectric material, PbZrxTi(1-x)O3, as a thin film by sol-gel route to replace the quartz crystal as a resonator. The novel hydrothermal annealing with microwave system is proposed to substitute the conventional furnace annealing.

本研究则是用同样具有压电性质的材料锆钛酸铅(PbZrxTi1-xO3)，以溶胶－凝胶法制成压电薄膜，来取代传统的石英晶体；再以微波反应系统进行水热式退火，来取代传统高温制程上的热处理方式，同时根据实验结果，进一步推论水热式退火的反应机制。

The results showed that RSAP used two primers of 18 nucleotides in which starting at the 3' end of each primer were restriction site sequences (4-6 bases),followed 12-14 bases of arbitary sequence, the differences between two primers were restriction sites and filler sequence; PCR am-plification was run for the first 5 cycles with an annealing temperature of 35℃, followed by 35 cycles with an annealing temperature of 48℃; the PCR reaction of 25 μL included 20ng DNA templates, 2.5mmol/L of Mg(superscript 2+), 0.2 mmol/L of dNTP, 1.5U of Taq DNA polymerase, 600nmol/L of each primers. RSAP is a new maker technique with simplicity, moderate throughput ratio and reliability. RSAP is of good reprodicibity and broad application.

结果显示，RSAP技术的引物为2条长度均为18bp的引物，引物的3'端为4~6个碱基的限制性酶切位点序列，接着是12~14个碱基的随机序列，2条引物的限制性位点和随机序列不同：PCR扩增的前5个循环采用35℃的退火温度，随后的35个循环采用48℃的退火温度；在25μL反应体系中，模板DNA用量为20ng，Mg(上标 2+)浓度为2.5mmol/L dNIPs浓度为0.2 mmol/L，Tap DNA聚合酶用碳为1.5U，2条引物浓度均为600mmol/L；RSAP技术重复性好，适用性广泛，是一种操作简便、产率中等、稳定可靠的DNA标记技术。

It was found that after annealing at different temperatures for lb the static magnetic properties achieves the best velum at T=390℃ and the loss minimum at T=440℃. After annealing at T=440℃, transversal induced magnetic anisotropy develop for the sample of t=2h.

实验发现：经不同温度退火1h后，试样的静态磁性能在T=390℃呈现最佳值；损耗则T=440℃呈现最低值；在T=440℃经不同时间退火后，试样在t=2h呈现横向感生磁各向异性。

The Au/AuGe(88/12)/Au back-contact metal structure was deposited on the GaAs substrate using an electron-beam evaporator. Various post thermal treatments were employed including conventional furnace and rapid thermal annealing. It was found that the outer Au layer thickness and furnace annealing temperature had large effects on the specific contact resistance.

在实验中我们在砷化镓基板背面进行蒸镀背金结构，而此背金结构是由三层金属所组成，分别为金/锗(12%)金(88%)/金，我们控制最外层金的厚度来量测与观察特徵接触电阻的大小，同时改变炉管加热的温度与快速热退火系统做比较，背金结构之元素分布比较可由欧杰电子分析得到，而扫描式电子显微镜可分析其两者之间的表面形貌差异。

In order to achieve the low temperature process, we used metal-induced lateral crystallization to fabricate it . Ni can lower the temperature of process and annealing time because the reaction between Ni and Si of forming Nickel Disilicide(NiSi2) which lowers the annealing time in further process.

在低温制程上采用的是金属侧向诱发结晶(Metal-induced Lateral Crystallization)方式，此方式是使用镍降低制程的温度以及生长时间，原理主要是藉由镍与矽之间的反应产生二矽化镍(NiSi2)，进行退火后可产生金属诱发结晶与金属侧向诱发结晶两种结构，再进行其微结构观察。

A large drop in hardness appears in as deformed samples at a temperature 45 ℃ lower than the start temperature of the exothermal peak after isochronal annealing, indicating that the recrystallization and grain growth process is closely relatine to annealing time and temperatur.

出现明显晶粒长大的温度较DSC曲线显示的放热峰起始温度低45℃左右，这主要是由于变形组织的回复再结晶过程是退火温度与时间的函数，降低处理温度并延长处理时间能达到与高温短时处理相同的效果。

The former consists of the spiculate FeAl3 phase which formed by the temperature deduction and the latter is composed of the lingulate FeAl3 and Fe2Al5 phases which embedded the substrate. Diffusion annealing as taken at 850℃, the structure changs apparently with increasing of the diffusion annealing time.

结果表明：浸镀层由表面富铝层及扩散层构成，富铝层包含降温形成的针状FeAl3相，扩散层由FeAl3、Fe2Al5相组成，形状如舌状指向基体。850℃扩散退火，随扩散时间的延长镀层组织结构明显变化。

Miscut SrTiO_3 (001) substrates were pretreated by ex situ annealing inflow oxygen and in situ annealing in vacuum.

采用流动氧气中退火和真空原位退火法对斜切SrTiO_3 (001)基片进行了预处理。

The circulation, consumption and reproduction of the trilogy have not only testified to its historical significance and literariness, but also invested it with new meanings.

该三部曲的流通、消费与再生产不仅验证了其历史意义及文学性，而切还赋予它以新的意义。

If he thought that he could buy me off, he would be wrong.

如果他认为他可以收买我，那他就大错特错了。