查询词典 anhydride

Through repairing the fixed bed calandria reactor during the molten salt leakage test in 2×104 t/a cis-butenedioic anhydride unit in Lanzhou Petroleum and Chemical Corporation,a pack of reasonable,practical and feasible technologic means was found to confirm the leakage points caused by molten salt and to repair it in reactor.

通过对兰州石油化工公司2×104t/a顺酐装置中的固定床列管式反应器熔盐渗漏的返修，摸索出一套实用、合理可行的熔盐渗漏漏点确认以及返修的工艺方法，可为类似反应器的制造提供一定的借鉴。

Compared with the Epoxy resorcinol-formaldehyde resin pretreatment system and Maleic anhydride pretreatment system developed by Xusigui, the 40% carbolated styrene-butadiene latex system can keep the composite"s properties and reduce the cost of pretreatment and simplify the pretreatment technology; especially to the HST 2073 latex system, the composite"s mechanics properties are improved greatly. Secondly, the composite"s comprehensive properties and interface performance are improved by reinforced with short fiber grafted with rubber in the surface. Thirdly, to simplify the production technology of composite, we add TKM-M and RF-90 as adhesive agent to the composite blended in an internal mixer, so as to the composite can be used to industry widely, then the effect of the amount adhesive agent on the composite"s properties and interface adhesive performance was studied, from the experiments the optimum amount of adhesive agent was deduced.

其中采用特软羧基丁苯胶乳预处理短纤维的方案，降低了预处理成本，相对许泗贵的低分子环氧和马来酸酐体系来说，预处理工艺大大简化了，而材料的力学性能保持良好，尤其是 HST 2073A 胶乳预处理体系，力学性能有较大幅度的提高；第二，通过对尼龙短纤维表面进行接枝橡胶分子链预处理，改善了复合材料的界面粘合性能，复合材料的综合性能也得到了相应的提高；第三，为了简化复合材料的生产工艺，使复合材料的应用得到工业化推广，我们选用TKM—M和RF—90长效增粘剂，直接加入短纤维橡胶复合材料中，采用密炼工艺，探讨了增粘剂的用量对复合材料界面粘合以及性能的影响，得出了增粘剂在复合材料中的最佳用量。

The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究，采用硫磺及乙酐复合催化剂，并且对氯化温度、氯化气氛、尾气回收等进行了过程优化，实现了乙酸氯化反应工艺条件的重大突破，使得氯乙酸的收率达到92.1%。

Kinetics of photo-chlorination of acetic acid to form monochloroacetic acid ;2. The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究，采用硫磺及乙酐复合催化剂，并且对氯化温度、氯化气氛、尾气回收等进行了过程优化，实现了乙酸氯化反应工艺条件的重大突破，使得氯乙酸的收率达到92。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

Mono-cinnamyl maleate was prepared by esterification of maleic anhydride and cinnamyl alcohol of 1 mol:2 mol at 95 ℃ for 2～4 h.Then added isomeric catalyst and mono-cinnamyl fumarate was made by reacting at 90 ℃ for 4 h.After methanol (methanol:mono-cinnamyl fumarate = 6 mol:1 mol) was added,the mixture maintained at 90 ℃ for 4.0 h to synthesize CMF.

合成试验表明：以摩尔比为1：2的马来酸酐与肉桂醇在95 ℃醇解反应2～4 h后加入异构化催化剂，90 ℃转型反应4 h后，添加6倍摩尔质量的甲醇，在90 ℃恒温反应4 h，反丁烯二酸桂醇甲酯的合成产率较高。

N-p-tolylmaleimide is a kind of monomer to copolymerize with MMA to enhance the thermal stabilities of PMMA.In this article, NPTMI was prepared from the reaction of maleic anhydride and p-toluidine in one stage, which was testified by FTIR. The mp. of NPTMI was 154 and consistent with the literature.

目前国外对这方面的研究比较成熟，国内研究的较少，且还没有对N-对甲基苯基马来酰亚胺、MMA和第三单体丙烯腈或苯乙烯共聚以制备耐热PMMA树脂及其性能的研究。

Ninth Five-Year Plan period, the Company conducted a medical intermediates of the pre-development and market research, the introduction of the development of superior strength skin, crotonic acid, crotonic anhydride and other products; also produced 3,3 dimethyl methacrylate, antibiotics raw material products, as well as more than 20 kinds of iso-vanillin and other pharmaceutical intermediates.

九五期间，本公司进行了医化中间体的前期开发和市场调查，引进开发了优力肤、巴豆酸、巴豆酸酐等系列产品；还生产了3，3二甲基丙烯酸甲酯、抗生素原料药系列产品以及异香兰素等二十多种医药中间体。

Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.

本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法，合成了4种苯并咪唑-2-羧酸衍生物并进行了表征；培养了2个化合物d、e的晶体并测定和讨论了晶体结构；制备了3种未见报道的苯并咪唑金属配合物，对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。

The catalytic activity of iodine in the esterification reaction was studied by synthesis cyclohexyl acetate from acetic anhydride,cyclohexano and acetic acid,cyclohexano.

以单质碘为催化剂，通过乙酸酐、环己醇及乙酸、环己醇为原料合成乙酸环己酯，对碘的催化活性进行了研究。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。