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Methods:total alkaloids of radix Sophora lavescens were extracted by acidified water,then adjusted to neutral by sodium hydroxide solution, dissolved with buffer solution,then were mixed with 0.025% of bromothymol solution and chloroform,and then the mixture was shaken,standing and demixed,the absorbability of chloroform layer was detected at the wavelength of 413nm.

将苦参的酸水提取液用氢氧化钠溶液调节至中性后,依次加入pH=7.6缓冲溶液,溴代麝香草酚蓝指示液、氯仿混合振摇,静置分层,于413 nm波长处测定氯仿层吸收度。

The core value of character should base on self-cultivation, love oneself first, then love others at your side, then extend to the public, and then spread to the social moral value and to behave companionate and coadjutant manners.

品德内涵的核心价值,应以个人修养为基础,从爱自己出发,再爱身边的人,并扩及到群己观念,再延伸至社会道德价值,表现友爱互助的群性。

In the preformulation study, the ultraviolet spectrum and HPLC methods for the assay of α-asarone were established firstly and then the physicochemical properties, especially the octanol/water partition coefficient and the solubility in various solvent systems such as alcohol, PEG 400, IPM, octanol were examined. The prediction permeability was then compared with actual transdermal parameters obtained from the in-vitro diffusion study , and feasibility of drug transdermal absorption was then analyzed.

在制剂开发的处方前研究工作中,首先建立了α-细辛醚的紫外及HPLC分析方法,测定了药物的油水分配系数及在生理盐水、各系列浓度的乙醇、PEG400、肉豆蔻酸异丙酯、正辛醇等溶媒中溶解度;其次,确立了药物体外经皮渗透研究的方法,并考察溶媒及促渗剂(乙醇、丙二醇、肉豆蔻酸异丙酯等)对药物体外经皮渗透性能的影响,计算药物经皮渗透的各参数,根据药物的药物动力学参数,分析了药物经皮吸收的可行性。

The results showed with the fruit ripening granulation index rose; semicellulose content of granulated juicy sac decreased first and then increased, while semicellulose content of non-granulated juicy sac reduced; the cellulose content of granulated juicy sac rose, while cellulose content of non-granulated juicy sac decreased first, and then rose to the top, and then reduced; and protopectin content reduced.

结果表明:粒化指数随着果实成熟而上升;粒化汁胞的半纤维素含量下降后上升,未粒化汁胞的半纤维素含量下降;粒化汁胞的纤维素含量增加,未粒化汁胞的纤维素含量下降后上升又下降;原果胶含量降低。

This was Jay Chou Chieh-lun's world back then,where he would dream and then redream his melodies and lyrics,and then he would rouse himself,stumble over to the keyboards and transpose those nocturnal audio tapes.

这就是周杰伦当初的世界。在这里他创造的旋律和歌词在梦中反复吟唱。然后他会醒来,走到键盘前,将那些夜晚声音图象转化成乐谱和试听带。

The tensile property was improved and then stable with the increasing content of coupling agent, however, the crupture ratio up and then down. And the tensile strength increase stey by step and electric insulation property is up and then descended with the addition of radiation agents.

结果表明,随着阻燃剂含量的增加和粒径超细化,其阻燃性能不断得到提高;而随着偶联剂含量的增加,其拉伸强度逐渐增大到一定程度后趋向稳定,断裂伸长率则先增大后下降;随着辐照剂量的增大,拉伸强度逐渐增大,电气绝缘性能先上升后下降。

Since it is the economic trade, then there may be disputes, and even the sale of even more than ordinary trouble,"meta-institutions is" contains: his wife, both into the Code-employed home and openly as husband and wife or Biqie too often there are a three-year five-year expiration date, although men say that the return of local deity, or the main tanha Code of pretty women, and then homes money, or the woman who aspire to master the economic prosperity, abandoning too fu master, a long time then fell in love, its potential may not otherwise have .

既然是经济买卖,那么就可能有纠纷,甚至比普通买卖还要麻烦,《元典章》载:其妻既入典雇之家,公然得为夫妇或婢妾,往往又有所出,三年五年期满之日,虽曰归还本主,或典主贪爱妇之姿色,再舍钱财,或妇人贪慕主之丰足,弃嫌夫主,久则相恋,其势不得不然也。

Secondly, if the morning of his eight 9:00, and after did not sleep, you wake your baby to 7:00, to speak, he said, touching the whole body massage, and then suck the breast, around 9:00 I think he should be trapped, if, sleep 1-2 hours, then close at noon, and then suck the breast, making a will, will be sleeping the afternoon between 4-6 points must let baby stay sober, so that he finished more than 7:00 after the milk definitely is trapped (at least my house is such a baby).

第二,如果早上他八九点起来,之后一直不睡,那么你7点把宝宝弄醒,给他说说话,全身抚摸按摩一下,再吃奶,我想到9点左右他应该会困的,如果能睡1-2个小时,那就接近中午了,再吃奶,拍一会,也会睡着的,下午4-6点间一定要让宝宝保持清醒,这样他7点多吃完奶后,肯定很困。

Through a variety of resin filter, adsorption and elution conditions for the optimization, as well as decolorization, crystallization methods of research, this article eventually determine the strong acid cation resin HZ-001 which is at pH 3, 3BV / h, having the largest adsorption to the tryptophan; the fermentation broth were centrifuged to remove sediment,then treated with activated carbon to be decolored and then treated with strong acid cation resin HZ-001. After that,2mol/l amino acid were passed through the HZ-001 ion exchanging column,kept almost constants when the flow rate stayed 6 BV / h. At 60℃,it was condensed into the saturated state and then added Ethanol until its percentage reaching 30%. At 4 ℃ under 100rpm placed in the shaker 20h, the collection of L-tryptophan was dried up in vacuo.

本文通过对种树脂的筛选、吸附和洗脱条件的优化,以及对脱色、结晶方法的研究与摸索,最终确定强酸型阳离子树脂HZ-001在pH=3,3倍床体积流速,温度室温,对色氨酸有最大的吸附作用;将发酵液离心去沉淀并用活性炭脱色后通过HZ-001强酸型阳离子交换树脂柱,再用2mol/L的氨水6倍床体积流速在室温下进行洗脱,收集洗脱液,60℃浓缩为过饱和状态后加入30%无水乙醇,4℃下100rpm摇起晶20h,过滤搜集结晶并真空干燥得白色粉片状L-色氨酸晶体。

Methods: 2ethyl aniline was used as starting material of the synthesis and was processed by acetic anhydride acylation, strong nitric acid nitraction at low temperature, and desacyl synthesis to produce 2ethyl5nitro aniline. The product was then synthesized to 3methyl6nitro1Hindazole by using ringclosing reaction in the presence of NaNO2, and then ethylated to obtain 2,3diethyl6 nitro2Hindazole. The latter compound was then reduced by SnCl2/Hcl to get target compound 2,3diethyl6nitro2Hindazole.

以2乙基苯胺为原料经醋酐酰化、浓硝酸低温硝化及去酰基保护合成2乙基5硝基苯胺,后用亚硝酸钠关环得3甲基6硝基1H吲唑,经硫酸二甲酯甲基化得2,3二甲基6硝基2H吲唑,最后用氯化亚锡将其还原得到目标产物,通过1H NMR确定结构与目标产物一致。

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Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

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