查询词典 amino-isovalerianic acid

The optimum synthetic conditions of hexadecanoic acid diethanolamide used two-step method are as follows:(1)reaction temperature was 140℃, reaction time was 4.5hours and molar ratio of hexadecanoic acid to diethanolamide was 1:1.15.(2)reaction temperature was 80℃, molar ratio of hexadecanoic acid to diethanolamide was 1:1.55 and mass concentration of the catalyst was 0.8%, reaction time was 3 hours.

二步法合成十六酸二乙醇酰胺最佳合成工艺为：(1)反应温度140℃、反应摩尔比n十六酸∶n二乙醇胺=1∶1.15、反应时间4.5h；(2)反应温度80℃、反应总摩尔比n十六酸∶n二乙醇胺=1∶1.55、催化剂用量0.8%、反应时间3h。

The obtained CBC was further reacted with stearic acid at 140℃ and hexadecyl alcohol at 180℃ in turn to form citric acid-beta-butylene glycol-citric acidstearic acid-hexadecyl alcohol claw large molecule.

以1，3-丁二醇、柠檬酸为原料，设计、合成了以1，3-丁二醇为核心的柠檬酸－1，3-丁二醇－柠檬酸爪状物小分子；再用酯化反应依次与带有功能化集团的硬酯酸、十六醇接枝合成了多元酯类爪形大分子柠檬酸－1，3-丁二醇－柠檬酸－硬酯酸－十六醇。

Six experimental stages were designed in our procedure, those are:(1) metabolite recovery and tested sample preparation: the metabolites were recovered by Amberlite XAD-2 absorption, followed by MeOH elution and solvent concentration;(2) antioxidant detection and strain selection: samples were quantitatively analyzed by the inhibition effects on formation of lipid peroxides and TBARS to screen the strains able to produce antioxidants. According to the established screening methods, we chose out a strain of actinomycetes, designed as AMBL-029C;(3) antioxidant purification: the fermentation broth was recovered by a series of separation techniques including centrifugation, Amberlite XAD-2 absorption, followed by MeOH elution and a successive TLC purification. The resulting primary purified compound [temperately designed as AMBL-029C-TS] was further analyzed by HPLC to monitor its purity;(4) physical-chemical characteristics: judging from the acid-base fractionation experiments, and the pH and temperature stability tests, the compound was deduced to be a acidic compound with the properties of low polarity and highly pH and temperature stable;(5) mechanism of the antioxidant: in comparison with some other known antioxidants, TS was subjected to investigate its antioxidant mechanism, together with BHT,-tocopherol, as well as two streptomyces metabolites, homogentisic acid and -phenylpyruvic acid, which were previously isolated as the natural antioxidants in our laboratory.

针对本实验目的，我们设计了以下的实验步骤﹔（1）二次代谢物回收及检测样本处理：我们将发酵所得的培养上清液，利用疏水吸附性树酯Amberlite XAD-2吸附回收，并以甲醇溶离及真空减压浓缩脱水等方式处理，以取得提供抗氧化活性筛选之检测样本；（2）抗氧化活性检测及菌种筛选：以「过氧化脂质」和「硫丙二醯尿」的生成量进行定性定量分析以作为抗氧化物质生产菌筛选之用；经此筛选程序，我们选获了具有抗氧化物质高生产力的菌株，命名为AMBL-029C；（3）抗氧化物质的分离纯化：针对生产菌株的发酵回收处理液，以矽胶薄层色层分离法经物质层析纯化后，并以高效能液相层析法(High performance liquid chromatography；HPLC)分析物质可得一初级纯化物质，命名为AMBL-029C-TS；（4）抗氧化物质的物理化学性质分析：由酸碱转溶（acid-base fractionation）实验得知，此抗氧化物质属於中低极性的强酸性物质，对温度（37℃-100℃）及酸碱度（pH3.0-13.0）均表现出高稳定性；（5）在抗氧化机制探讨方面，我们针对数种不同的抗氧化机制进行探讨，即： 1。

Results At 2 h after damage in cerebral cortex 5-hydroxyindolecetic acid (5-HIAA) elevated remarkably; At 8 h after da-mage 5-hydroxytryptamine (5-HT), homovanillic acid elevated; but there was no obvious change on norepinephrine and 3,4-dihydroxyphenyl acetic acid.

结果 大脑皮质运动区在损伤后2小时5-羟吲哚乙酸（5-HIAA〕明显升高；8小时后5-羟色胺(5-HT)、高香草酸升高；去甲肾上腺素及3、4-双羟苯乙酸变化不明显。

The soil pH was found to be the main factor affecting BR formation of 14 C\|metsulfuron methyl among the basic properties of soil.(2)During the whole periods of the incubation,the 14 C\|BR of 14 C\|metsulfuron methyl in soils was mainly distributed in fulvic acid and humin.The relative percentage of 14 C\|BR in fulvic acid was higher than in humin,while the content of the 14 C\|BR distributd in humic acid only account for less than 1% of applied amount.

土壤pH是14 C 甲磺隆在土壤中形成BR的主要影响因子。14 C -甲磺隆在各类土壤中的14 C BR的最大值分别占引入量的 48 5%、46 5%、52 6%、1 9 3 %、49 7%、42 0 %和 46 5%；( 2 )在整个培养试验过程中，14 C 甲磺隆在 7种不同类型土壤中的14 C BR ，主要分布在富啡酸和胡敏素中，前者中的相对百分比大于后者，而在胡敏酸中的相对百分比较小。

The results indicated that the total quantity of volatile components in grape wine after MLF had increased and there were evident difference in the contents and proportion of isoamyl alcohol, 2-ethyl hydracrylic acid, ethyl succinate, and acetic acid in the two kinds of grape wine treated or not treated by MLF. Besides, lactic acid and ethyl lactate, which could not be accurately identified in grape wine not treated by MLF, could be easily separated and identified in grape wine treated by MLF like other main components.

结果表明，MLF葡萄酒较未经MLF的葡萄酒中挥发性成分的总量有所提高；异戊醇、2-羟基丙酸乙酯、琥珀酸乙酯和醋酸在两工艺的葡萄酒中的含量和比例存在明显差异；乳酸、乳酸乙酯和两种未能准确鉴定的物质只在MLF葡萄酒中作为主要成分被分离检测到。

Bromoundecanoic acid was synthesized with 10-undecanoic acid and hydrobromic acid as raw materials.

以10-十一烯酸和溴化氢为原料合成11-溴代十一酸，考察了引发剂、溶剂、反应温度、后处理方法、熟化时间等因素对反应和产品的影响。

Bromoundecanoic acid was synthesized with 10-undecanoic acid and hydrobromic acid as raw materials. The effects of initiating agent, solvent, reaction temperature, the ways of disposal, ripening time etc. on the reaction and product were investigated.

以10-十一烯酸和溴化氢为原料合成11-溴代十一酸，考察了引发剂、溶剂、反应温度、后处理方法、熟化时间等因素对反应和产品的影响。

Keywords Black mercury sulfide;Thickish hot hydrochloric acid;Hydrobromic acid;Hydroiodic acid;Dissolve

黑色流化汞；热浓盐酸；氢溴酸；氢碘酸；溶解

The white low-density powder of the the sodium salt of polyaspartic acid was got by dropping the hydrolyzable solution to wiscked high speedly carbinol which Consumption amount is about 3-6 times to the amount of solution, the powders density is about 0.35g/ml.4 Polyaspartic acid was characterized by NMR and IR.5 The scale inhibition behavior of polyaspartic acid was studied and result shows: The calcium carbonate inhibition rate is up to 99% at the dosages of 12.5mg/ Land when pH value is 9.0, Ca2+ concentration is 120mg/L and HCO3- concentration is 366mg/L.6 The primary design was put forward for industrialized production of PASP.

在此工艺下得到聚天冬氨酸钠粉术，外观为白色的轻质粉术，堆积密度0.35g／ml，不用进行脱色和粉碎。 4。用红外光谱和核磁共振谱图对聚天冬氨酸进行了表征。 5。对合成的聚天冬氨酸钠对CaCO_3的阻垢性能进行了研究。结果表明：在Ca~(2+)离子浓度120mg/L(以碳酸钙计300mg/L)，HCO_3~-离子浓度为366mg/L(以碳酸钙计600mgL)，PH值=9.0的条件下，阻垢剂浓度达到12.5mg/L时阻垢率可达99％。

You think you're a big shot.

你认为你是一个大人物？

All states are equal, and none can receive special treatment from the federal government.

所有的州都是平等的，任何州都不能获得联邦政府的特别待遇。