查询词典 amino acid

We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上，利用传统植化分离手段和现代分离技术，包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱，制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物，其中，2个新化合物和2个己知化合物，并进一步通过现代分析技术IR，ESI-MS，~1H-NMR，~(13C-NMR，HMBC，HMQC，~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是：3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2，6-二甲基-6-O-β-D-吡喃鸡纳糖基-2，7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷，金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷；2个已知化合物结构分别是：金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷，金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

In the medium of 0.013 mol/L H2SO4, phosphate reacts with sodium molybdate and potassium antimonyl tartrate, forming a yellowish phosphorus-antimony-molybdenum heteropoly acid. The acid exhibited a strong resonance scattering peak at 710 nm after added with nanogold. The heteropoly acid was reduced by ascorbic acid to antimony phosphomolybdate blue, which caused the decrease of resonance scattering intensity.

在0.013mol/L H2SO4介质中，磷酸根与钼酸钠、酒石酸锑钾反应生成淡黄色的磷锑钼杂多酸，加入纳米金后在710nm处产生一个较强的共振散射峰，抗坏血酸可将磷锑钼杂多酸还原为磷锑钼蓝，导致710nm处共振光散射信号降低。

The results showed that 4-HR combined preventing browning reagent has good controling browning effects on the above four kinds of materials. The best combination to apple-slice is A2B2C1, namely 0.02% 4-HR, 0.03% antiscorbutic acid and 0.5% citric acid; the best combination to banana-slice is A2B2C2, namely 0.02% 4-HR, 0.03% antiscorbutic acid and 0.75% citric acid; the best combina...

实验结果表明4-HR组合防褐试剂对上述四种材料均表现良好的护色效果，其中对苹果切片的最佳组合是A2B2C1，即0.02%4-HR、0.03%抗坏血酸、0.5%柠檬酸；香蕉最佳组合是A2B2C2，即0.02%4-HR、0.03%抗坏血酸、0.75%柠檬酸；马铃薯切片和莲藕汁的最佳组合都是A1B1C2，即0.01%4-HR、0.02%抗坏血酸、0.75%柠檬酸。

To restore the ability of chromium can be dissolved in sulfuric acid, hydrochloric acid and High-FE acid and release hydrogen, but also of pure chromium with aqua regia does not work, when there is the presence of halogen ions in the acid can not be long-term stability, high temperature with alkali, hydrogen sulfide, sulfur steam, phosphorus, ammonia, such as carbon monoxide and water vapor reaction of the corresponding compounds, in the high temperature reaction of silicon into the silicide also chromium, chromium alloys with many metals generate a wide range of industrial applications, such as chromium-manganese stainless steel is used extensively for chemical plants.

铬的还原能力强，能溶于硫酸、盐酸和高FE氯酸而放出氢气，但纯铬连王水也不起作用，当有卤素离子存在时，在酸中不能长期稳定，高温时能与强碱、硫化氢、硫蒸汽、磷、氨、一氧化碳和水蒸汽等反应生成对应的化合物，在高温下还能与硅反应成硅化铬，铬能与许多金属生成合金广泛在工业上应用，如铬锰不锈钢大量用于化工设备。

Glucose,formic acid and levulinic acid were not detected in the liquors of acid hydrolysis and the concentration of xylose and arabinose was high,while the acetic acid was low.

目前，国内外用高效液相色谱法测定糖类化合物已有许多报道[4-10]，但同时分析单糖及脂肪酸的报道仅在Solang等[3]的研究中略有叙述。

Results: The linear ranges for inorganic arsenic, monomethylarsonic acid and dimethylarsonic acid were all from 5.0 to 100.0 μg/L The detection limits of As(superscript 3+), As(superscript 5+), monomethylarsonic acid and dimethylarsonic acid were 0.05 mg/kg. The recoveries of the method were 78%-110%(n=6), and the relative standard deviations were

结果：本方法的三价砷、五价砷、一甲基砷和二甲基砷在5.0~100.0 μg/L范围内有良好的线性，方法的测定低限均为0.05 mg/kg；实验表明方法对不同海产品的回收率在78%~110%之间，相对标准偏差在3.0%~12.2%之间。

We can find from the research that the IR and XRD spectrogram shows the exists of H_3BO_3 on the surface of cellulose;there is H~+ released form the solution and the complexation proportion of the boric acid-glucose in the solution is 1:1, the boric acid-mannitol is 1:2 and the boric acid-N-methylglucamine is 1:2;and the half experienced mathematics model experiment on analyzing PH shows that the cellulose's adsorption of the boracic acid is mainly chemical adsorption with a proportion of 1:1 while physical adsorption with the H~+ released during the reaction plays a role as assistance.

研究结果表明，通过IR和XRD谱图分析，表明纤维素上吸附了H_3BO_3；硼酸和葡萄糖、甘露醇、N-甲基葡萄糖胺在水溶中络合比分别为1：1，1：2，1：2，同时溶液中有H~+释放出来；应用半经验数学模型分析pH值-浓度吸附实验，表明纤维素对硼酸主要以化学吸附为主吸附比为1：1，以物理吸附为辅，反应过程中释放出H~+。

The fact that chloric acid, bromic acid and iodic acid in acid solution are different in oxidizing properties is illustrated through the thermodynamic principles in this paper.

应用热力学原理对氯酸、溴酸和碘酸在酸性溶液中的氧化性强度不同的事实进行了分析说明，其氧化性强度按 HIO3

After 20 days, at the end of fermentation, the cassava residue inoculated has better sensory quality, but the treatments of adding low levels of saccharose have low lactic acid accumulation amounts and high butanoic acid accumulation amounts compared with the treatments of adding high levels of saccharose, the treatment with inoculation and 4% saccharose addition has the highest lactic acid accumulation amount, which is 18.7 g/kg, and the treatment with inoculation and 8% saccharose addition has the lowest butanoic acid accumulation amount, which is 0.141g/kg.

结果显示：在发酵开始时接种处理的乳酸菌数为5×108 cfu/g，而对照处理没有检测到；发酵结束后，接种的3个糖水平处理的外观发酵品质比未接种处理好，但糖浓度低时丁酸积累较多，乳酸积累少，接种并添加4%蔗糖的处理乳酸积累量最高，发酵物中乳酸积累达18.7 g/kg，接种并添加8%蔗糖的处理丁酸积累最少，仅为0.141 g/kg。

Content of butanoic acid, methyl ester; butanoic acid, ethyl ester; hexanoic acid, methyl ester; DMHF; DMMF identified in strawberry cultivated from green house were higher than that cultivated in the open field of the correspongding nitrogen levels , and the hexanoic acid, ethyl ester could only identified in green house strawberries.

不同氮素水平温室草莓果实中丁酸甲酯、丁酸乙酯、己酸甲酯、DMHF、DMMF的相对含量和总量均比相应氮素水平的露地草莓的高，且己酸乙酯只是在温室草莓中检测到。

You can snipe the second and third union leaders from this position.

您可以鹬第二和第三工会领袖从这一立场出发。

Aiming at the currently shortage of XML streams quality detecting, this paper proposes a new forecasting method of XML streams quality by least squares support vector machines, which is used the method of XML keys' vector matrix as windows, and vector product wavelet transform to multilevel decompose and refactor the XML streams series, that can fulfill real-time checking demand of XML quality, and ensure constraint, consist- ency and integrality. For even more adapting net load, it proposes a control strategy by weight and adaptive adjustment to ensure XML streams quality.

针对当前XML数据流质量检测存在的不足，提出构建XML键的矢量矩阵作为窗口，利用矢量积小波变换多级分解与重构XML数据流，再结合最小二乘支持向量机对XML数据流质量进行预测的一种方法，满足XML数据流质量重构时实时检测的要求，保证XML数据的约束性、一致性与完整性；为了更好的适应网络负载，采取加权与自适应窗口调整等调度策略充分保证XML数据流的质量检测。