查询词典 amination

The illicit synthesis of this compound has been achieved most commonly by the reductive amination of phenyl-2-propanone 2, by the Leuckart formamidation of 2 followed by hydrolysis or by the reduction of ephedrine or pseudoephedrine 3 with hydriodic acid and red phosphorus.

此化合物非法合成的方法有，通过1-苯基-2丙酮的还原胺化作用；通过1-苯基-2丙酮的洛卡特氐反应后进行水解生成；在红磷、氢碘酸的参与下，通过还原麻黄素或伪麻黄素合成。

The optimum reaction conditions were that the molar ratio of maleic anhydride and p-nitroaniline was 1.2:1, the volume ratio of toluene and DMF was 10:1, the amination temperature was 20~30℃ the cyclization temperature was 145~150℃ and the cyclization time was 6 h over; the amount of p-toluene sulfonic acid was 12% of total reactant mass, the amount of copper sulfate was 0.1~0.5% of total reactant mass, the amount of hydroquinol was 0.1% of total reactant mass.

得到的最佳工艺条件是：n：n为1.2：1，V：V为10：1；胺化反应温度为20~30℃，环化反应温度为140~150℃，环化反应时间为6h以上；对甲基苯磺酸用量为反应物总质量的1%~2%；硫酸铜用量为反应物总质量的0.1%~0.5%；对苯二酚用量为反应物总质量的0.1%。

Starting with commercial available tosylmethyl isocyanide and but-2-enoic methyl ester, pyrrolo[2,1-f][1,2,4]triazine derivatives was prepared by twelve-steps process in total yiled of 5.0%~8% via pyrrole and pyrrolo [2,1-f] [1,2,4] triazine ring formation, substitution and amination reactions etc.

本文以简单的对甲基苯磺酰甲基乙腈和反-2-丁烯酸为原料，经过形成吡咯，吡咯并[2，1-f][1，2，4] 三嗪环，取代，酰胺化等等12步反应，合成了结构新颖的吡咯并[2，1-f][1，2，4] 三嗪衍生物，总收率达5%～8%。

The location, shape, signaland the effect to the nearby tissues in MRI of the lesion,symptomatic spinal epidural lipomatosis have its own rules and MRI ex-amination is one of the better means in providing information for clinical diagnosis and treatment.

特发性椎管内硬膜外脂肪增多症的MRI在病灶的部位、形态、信号及其对周围组织的影响等方面均有规律可循，且MRI优于其它影像学检查，为临床诊断及治疗提供依据。

Starting from 4-androstenedione, three novel 3-oxo-4-aza-5-androstene-17-oxime derivatives 7, 8 and 9 were synthesized through oxidation ring cleavage, amination ring closure, oximation,and substitution .

以4雄烯二酮为起始原料，经过氧化开环、氨解闭环、肟化、取代等4-步反应，合成了3个新的3-羰基-4-氮杂-5-雄甾烯-17肟衍生物7、8和9，并用质谱、1HNMR、13CNMR等测试手段对目标化合物的结构进行了表征

Androstenedione and dehydroepiandrosterone as a new steroid material attracts people's attention because of the shortage of diosgenin resource and successful synthesis of AD by degradation of sterols. The followings were included in this thesis: 1. 24 new oxime-ether and oxime-ester compounds from AD were synthesized by cleavage of A-ring through NaIO_4/KMnO_4 oxidation, ring closure by amination, oximation with hydroxylaminechloride in C-17 position.

甾体药物的合成原料一般为薯蓣皂素、剑麻皂素、番麻皂素等，随着薯蓣资源日渐枯竭，使得甾体药物工业不得不寻求新的原料，而微生物降解胆固醇和植物甾醇合成雄烯二酮获得成功，使得AD成为新兴的甾体原料吸引了人们的注意。

The lignin-quaternary/polyvinyl alcohol composite resin was made from lignin after phenolization and amination,using glutaraldehyde as cross-linking agent,PVA as carrier.

利用木质素为原料，经酚化、胺化改性后，以戊二醛为交联剂，聚乙烯醇为载体，合成了季铵型木质素/PVA复合阴离子交换树脂。

With sodium acetate as catalyst, inosine was esterified with acetic anhydride in the yield of 92% to give 2',3',5'-triacetyl inosine, which was treated with pyridine and phosphorus oxychloride to form a pyridinium solution, followed by performing an amination at 40℃ and 0.25~0.30 MPa to achieve adenosine in the yield of 67%.

肌苷在醋酸钠存在下与醋酸酐发生酯化反应以92%的收率得到2'，3'，5'-三乙酰肌苷，其化合物经吡啶和三氯氧磷处理形成吡啶盐溶液，未分离直接在40℃、0.25~0.30 MPa压力下进行氨解反应以67%产率制得腺苷。

The studies found that compatibility between ZDDP and succinimide dispersants primarily depended upon active α-amino-group content in succinimides. The active α-amino-group content was affected by the alkylation and amination processes, and also affected by the structure of polyisobutylene in succinimides.

研究结果表明，丁二酰亚胺与 ZDDP 的相互作用主要取决于丁二酰亚胺中活泼的伯胺氮含量，而伯胺氮含量则决定于丁二酰亚胺在生产中的烃化、胺化工艺和聚异丁烯基的结构。

Objective To discuss the methods and effects of the treatment under endoscope and the courses of massive hemorrhage of upper digestive tract after gastrectomy and esophagectomy.Methods Emergency endoscope ex-amination were carried out in20massive hemorrhage clients after gastrectomy and esophagectomy,after exposed and washed the bleeding part by cold0.9%NS,1∶10000adrenaline and hypertonic saline were injected in perifocal sub-mucosa.After stop bleeding and before move back the endoscope,spray some YunNanBaiYao and thrombase in the bleeding part to prevent secondary hemoorahge.

目的 探讨食管、胃切除术后上消化道出血的原因及内镜下治疗的方法、效果方法对食管、胃切除术后引起大出血的患者行急症内镜检查，用冰冻生理盐水100ml+去甲肾上腺素8mg反复冲洗，暴露出血部位后在病灶周围黏膜下注射1∶10000肾上腺素及高渗盐水，无出血后，退镜于出血部位喷洒云南白药及凝血酶，防止再次出血。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。