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The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明:紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移,νC=O振动吸收峰在聚合24h后红移;TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01,α为2.28,优于其它功能单体参与得到的聚合物识别特性;TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间,作为色谱固定相具有良好的通量和低的柱压;在乙腈流动相中,TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动,低温有利于分子印迹固定相分离甾醇结构类似物;TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融,Tp=257.40℃,聚合物CP的降解温度在267.79℃,MIP降解温度在343.11℃,制备的固相微萃取头初步经GC/MS 270℃的耐热性测定;不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应;分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性,可作为此类化合物的吸附材料,特别对孕酮强保留的富集特性,可作为孕酮的选择性识别吸附剂,其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡,具有作为传感器核心敏感材料的潜力;对比萃取奶粉中17β-雌二醇性能,MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留,回收率依次为85.5%,43.7%和30.7%。

The250gL-1 hydrogel was applied in tissue engineering;4weeks after injection,the hard nubble was formed subcutaneously and immatural cartilage was observed.8weeks after injection matural catilage was observed.12weeks after injection the amount of matural cartilage increased.

此水凝胶用于软骨组织工程,注射后4wk在皮下形成稍硬的结节。8wk后形成的结节质地坚韧,切面色泽亮白。

Cumulatie patency rates were 67% after 1 year, 56% after 2 years, and 53% after 3 years.

在随访期间,累计开放率1年后67%;2年后56%;3年后53%。

Results:The expression of ICAM1 started to increase after reperfusion for 2 hours,peake d at 48 hours after reperfusion,and continued for 96 hours.Neutrophil infiltrati on in ischemic tissue increased at 12 hours,and peaked at 48 hours after reperfu sion,paralleling the increase in ICAM1 expression.

结果:大鼠脑缺血再灌注2小时局部脑组织ICAM 1的表达开始升高,于再灌注48小时达到峰值,持续至再灌注96小时仍保持较高水平表达;局部缺血区域中性粒细胞浸润于再灌注后12小时开始升高,48小时达到高峰,与ICAM1的表达呈同步改变。

Serum pepsinogenⅠ and pepsinogen Ⅱ levels were measured by radioimmunoassay in 190 healthy controls, 103 patients with gastric cancer before operation, 33 patients after partial gastrectomy, 18 patients after total gastrectomy, and 23 return visit patients after total gastrectomy.

运用放射免疫分析方法测定了190例正常人,103例胃癌手术前病人,33例胃部分切除病人,18例全胃切除病人,23例全胃切除后随访病人的血清PGⅠ、PGⅡ的含量,并进行统计学分析。

At 6h after ischemia both MRI were found to indicate definite infarct foci in the caudate nucleus and the lentiform nucleus,mass effect was seen too.Histopathologic findings:At 2h after ischemia,electro microscope revealed the changes of ischemia and edema.At 4h after ischemia,the photomicroscope demonstrated the changes of ischemia edema and the electromicroscope indicated the damage to blood brain barrier.

结果 梗塞2h MRI T2加权可见尾状核头部、豆状核信号增高;6h MRI可见尾状核、豆状核形成明确梗塞,并出现占位征象。2h电镜下已有缺血水肿改变,4h光镜下出现脑缺血水肿改变,电镜下见到血脑屏障受损。

Structural matter drops to hit water with fixed rate phut from certain height, inchoate and main the structure that attacks water process in the light of phut is answered begin research, and press mutation of field of force and Xing Bo to wait to study however to entering the underwater after water less, and add with each passing day as large bridge and marine project much, the construction in these projects and the phenomenon that phut of large construction content also appeared to hit water in use process, like Guangdong 9 rivers big bridge is bumped to break down after collapsing, large area bridge floor falls into surface to wait, the meeting such as mutation of field of pressure of the underwater after this kind of phut hits water and Xing Bo is right all round structural products gives birth to certain influence, evaluate this kind of influence to have real project sense to construction and design.

结构物从一定高度落下以一定速度砰击水面,早期主要针对砰击入水过程的结构响应开展探究,而对入水后水下压力场突变和兴波等却探究较少,而随着大型桥梁和海洋工程日渐增多,在这些工程的施工和使用过程中也出现了大型结构物砰击入水的现象,如广东九江大桥被撞垮塌后大面积桥面落入水面等,这种砰击入水后水下压力场突变和兴波等会对四周结构物产生一定影响,评价这种影响对施工和设计具有现实的工程意义。

At the same time it researches that when the pigling is 45 days of age,the titer of titer of antibody of sow is higher and it still has protection ability for the pigling and after being immunized concentrated vaccine and common vaccine the pigling and after of antibody raises from transitory decline and after 25 days of immunity the titer of antibody can not reach the critical protective value.

同时研究了仔猪在45日龄时母源抗体效价较高,对仔猪仍然具有保护力,用浓缩疫苗和普通疫苗免疫后,抗体效价由短暂下降至上升,免疫25d后抗体效价达不到临界保护值以上。

Regard domestic head as the home in order to pay close attention to calamity hind " interior home " rebuilding network platform,"Health of the network after calamity ensures platform " urgent psychology is placatory after aiming to pass a network to offer calamity to disaster area people and even social masses, in order to help shadow of the psychology after disaster area people walks out of calamity quickly, face disaster bravely, pick up life confidence again!

作为国内首家以关注灾后"心灵家园"重建的网络平台,"灾后网络健康保障平台"旨在通过网络对灾区人民乃至社会大众提供灾后紧急心理抚慰,以帮助灾区人民迅速走出灾后心理阴影,勇敢面对灾难,重拾生活信心!

Ticket limit:China to Poland, China fly Poland ticket price inquiry flightsTime:1, ticket booking 21 days prior to departure from the book must be in 14 days after a ticket, 21 days starting from the book must be within 7 days after booking tickets, starting from within 7 days after the book must be within 24 hours in book tickets

机票价格,中国飞波兰航班查询 1、出票时限:距出发21天前预订必须在预订后14天之内出票,距出发21天内预订必须在预订后7天之内出票,距出发7天内预订必须在预订后24小时之内出票

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推荐网络例句

Fancy gold-plated dangling earrings with facetted White Opal crystals.

花式镀金悬垂耳环与facetted白欧泊水晶。

This essay chooses the study aim from biology teachers in middle school in Shi Jiazhuang which tells us that most of the middle school biology teachers in Shi Jiazhuang have the"burnout", lower successfulness, individualize.

本文选取石家庄市初中生物教师作为研究对象,运用问卷调查的方法对石家庄市初中生物教师职业倦怠的现状进行调查,调查结果发现,石家庄市初中生物教师这一群体普遍存在职业倦怠,情感枯竭程度偏高,成就感偏低,去个性化程度最为严重。

In measurements of a day,generallyspeaking,the photosynthesis of birch in mesophytic habitat is better than that in xerophytichabitat(peak values are 12.8,10.33μmolCO2m-2s-1 respectively);that of sexual birch inmesophytic habitat is better than that of clone birch(peak values are 9.87,6.71μmolCO2m-2s-1respectively);that of young tree is better than that of seedling(peak values are12.37,10.05μmolCO2m-2s-1 respectively).

在一天中的各个时刻,总体说来,中生生境生长的白桦光合作用超过旱生生境生长的白桦光合作用(净光合速率峰值分别为12.8、10.33μmolCO2m-2s-1);白桦幼树的光合作用超过白桦幼苗(净光合速率峰值分别为12.37、10.05μmolCO2m-2s-1);中生生境有性白桦的光合作用超过无性白桦的光合作用(净光合速率峰值分别为9.87μmolCO2m-2s-1、6.71μmolCO2m-2s-1)。