查询词典 adduct

Based on the characteristic that boracic acid (H3BO3) has a condasation and complexation reaction with 3-MCPD forming a negative-charged adduct in aqueous phase, arapid method for the direct determination of 3-MCPD in HVP by capillary electrophoresis with conductivity detection was investigated.

利用硼酸能与3-氯-1，2-丙二醇(3-MCPD)上的2个邻位羟基进行键合生成配合阴离子、从而增加多羟基化合物的负电荷的特性，在15 mmol/L 三羟甲基氨基甲烷-10 mmol/L H3BO3(pH 8.3)介质中，采用毛细管电泳/电导检测法分离检测了3-MCPD，该方法的线性范围为0.5-20 mg/L，检出限为0.1 mg/L(S/N=3)。

Urethane adduct was synthesized from decarboxylated cashew nut shell liquid,hexamethylenediisocynate and polyethylglycol,which was then reacted with melamineformaldehyde resin to form aqueous coating material.

采用天然植物油、己二异氰酸酯和聚乙二醇在较温和的条件下反应，制得了水溶性的氨基甲酸酯加成物，以此和低醚化度甲醚化三聚氰氨甲醚甲醛树脂制备了水性涂料。

Three of the ten were adult denture crowded patients, the others were adults with bimaxillary protrusion. MAS mini-implant were implanted in 15, 16 and 25, 26 separately. The mini-plants were utilized with the rubber chain, ligature silk to move the cuspid to diatal and to adduct the anterior teeth.

收集武汉大学中南医院口腔正畸科就诊成人牙列重度拥挤患者3例，成人双颌前突患者3例，分别在他们15、16和25、26间各植入一枚MAS微型种植体，利用橡皮链，结扎丝和镍铬弹簧等与微植体相连牵引尖牙向远中移动、内收前牙、防止磨牙支抗丧失。

Methods: Mini-implant was used in ten cases as orthodontics anchorage. Three of the ten were adult denture crowded patients, the others were adults with bimaxillary protrusion. MAS mini-implant were implanted in 15, 16 and 25, 26 separately. The mini-plants were utilized with the rubber chain, ligature silk to move the cuspid to diatal and to adduct the anterior teeth.

收集武汉大学中南医院口腔正畸科就诊成人牙列重度拥挤患者3例，成人双颌前突患者3例，分别在他们15、16和25、26间各植入一枚MAS微型种植体，利用橡皮链，结扎丝和镍铬弹簧等与微植体相连牵引尖牙向远中移动、内收前牙、防止磨牙支抗丧失。

The facts that type I compounds could easily undergo deamination reaction to form α-methylene cyclopentanone derivatives and they could react with glutathione to form an adduct provided sufficient evidence for the hypothesis that the compounds acted as masked α-methylenecyclopen- tanones and reacted with biologically important sulfhydry-containing enzymes, and thus produced anticancer activity.

Ⅰ类化合物在稀溶液中极易进行去胺基化反应形成α-亚甲基环戊酮类化合物。并且Ⅰ类化合物于稀溶液中易与谷胱苷肽进行结合，这些事实为Ⅰ类化合物作为隐蔽的α-亚甲基环戊酮与酶进行加成，从而导致酶失活而具有抗癌活性的设想提供了证据。

In addition, IR-spectra of DNA and DNA-indirubin adduct imply indirubin interacts with the phosphate groups of DNA by hydrogen bond or electrostatic interaction.

另外，在最优化条件下，靛玉红峰电流的降低与DNA的浓度在一定范围内存在良好的线性关系，以此进行了DNA样品回收率的测定，结果满意。

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应，用茚〓和1，1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物，发现可控制反应条件，使1，1'-联茚与〓反应，并高产率地得到具有新颖结构的单加成物，用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征，测得它的两个〓杂化的桥头碳的化学位移为〓ppm，证明生成的衍生物为6∶6闭式环加成，〓NMR谱中共给出38个信号，表明〓联茚衍生物分子具有〓对称性；在波长532nm，脉冲宽度8ns的激光下，〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近，由于〓联茚单加成衍生物熱稳定性好，在四氢呋喃，丙酮等极性溶剂中溶解性好，能分别均匀地掺入溶胶-凝胶中，已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能；使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究，通过等温压缩曲线测试，证明浓度为〓〓时，〓联茚衍生物能够形成单层膜。

The pathological changes of hallux valgus are diversity, including adduct of metatarsus primus, increasing of the intermetatarsal angle between the first and second metatarsal bones, increasing of hallux valgus angle, dislocation of sesamoides, lost of soft tissue balancing. X-ray is the most important method to measure the pathological changes of hallux valgus.

拇外翻其病理改变具有多样性的，包括第一跖骨内收、第一，二跖骨间角增大、拇趾外翻角增大、第一跖趾关节近端关节面固定角或远端关节面固定角增大、籽骨移位、软组织平衡的改变等。X射线测量是确定拇外翻病理改变的主要的手段。

The factors influencing nitric oxide release from spermine/nitric oxide adduct and the absorption characteristics of nitric oxide by horticultural products were investigated, which is useful for the application of SPER/NO to the storage of horticultural products.

研究影响精胺／一氧化氮加合物释放NO的因子及园艺产品吸收NO的特性，为SPER/NO应用于园艺产品的贮藏保鲜提供理论依据。

The results demonstrate that ACM-A is capable of intercalating between the base pairs of DNA double helix, the π-π electronic overlapping between π-electron of ACM-A and DNA stabilizes the ACM-DNA adduct, and through electrostatic interaction, the trisaccharide interacts with the minor groove of DNA owing to C(3') amino group.

实验结果表明，ACM-A主要以其蒽环平面嵌入DNA双螺旋碱基对之间，发生-等电子间相互共轭，同时药物糖基上C3'位的-N(CH3)2基团带正电荷，易与带负电荷的磷酸骨架产生静电吸引，从而发生沟槽作用，嵌入DNA的小沟区，这是二者之间的主要结合模式。并且，DNA与ACM-A药物原型的亲和力要强于还原后的药物代谢产物。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。