查询词典 acylation

The acylation of 2,3-dimethyl-2-butene by acetic anhydride in the presence of H3PO4 was investigated.

在H3PO4存在下进行了2，3-二甲基-2-丁烯与乙酐的酰化反应。

The effects of the amount of catalyst, the amount of acetic anhydride, reaction time, and addition of solvents etc. on the acylation reaction were investigated.

考察了催化剂用量、乙酐用量、反应时间和溶剂的加入等因素对该酰化反应的影响。

It was found that H3PO4 is an effective catalyst for the acylation of 2,3-dimethyl-2-butene by acetic anhydride at room temperature.

结果表明，H3PO4是室温下催化2，3-二甲基-2-丁烯与乙酐酰化反应的有效催化剂。

FeCl_3 was used to catalyse the acylation reaction of triisobutylene by acetic anhydride at room temperature.

室温下FeCl3用于催化三聚异丁烯与乙酸酐的酰化反应。

It was found that SnCl_2·2H_2O is an effective catalyst for the acylation of 2,3-dimethyl-2-butene by acetic anhydride at room temperature.

发现SnCl2·2H2O是室温下2，3-二甲基-2-丁烯与乙酐进行酰化反应的有效催化剂。

Methods Starting from anisole, liarozole was synthesized by Friedel-Crafts acylation, nitration, nucleophilic substitution, reduction and cyclization.

以苯甲醚为起始原料，经傅克酰基化、硝化、取代、还原、环合等7步反应得到目标化合物利阿唑。

In the acylation reaction between anisole with acetyl chloride, The catalyst of ZnCl〓/HY-98 prepared by MWI had the best catalytic activity and the selectivity of p-methoxy acetopheone. The catalytic active centers were ZnCl〓 dispersed in zeolite and the Bronsted acid sites in HY-98 zeolite itself.

在苯甲醚与乙酰氯的酰化反应中，微波固相法制备的ZnCl〓／Y催化剂有相对较好的催化活性和选择性，起催化作用的主要是分散在分子筛表面的ZnCl〓和分子筛本身的B酸。

All compounds are synthesized starting from the acylation reaction of gallic acid with L-glutamine to form the basic scaffold, followed by the cyclic reaction in acetic anhydride and the key intermediate cyclic anhydride (compound 4) was obtained. The intermediate compound is condensed with different amino acids or primary amines, and produces the target compounds.

本研究以L－谷氨酸为基本骨架，与甲醚化保护的没食子酸缩合后，经过酰化、环合反应得到关键中间体环状酸酐（化合物4），再经胺解反应合成目标化合物，其化学结构经过红外光谱、电喷雾质谱和核磁共振谱（氢谱、碳谱、碳氢异核多键相关谱）确证。

Three methodsconventional direct acylation,acylation by phase transfer catalyst(PTC,and ionexchange-acylation were selected for the purpose of acetylating κ-carrageenan with 30kDa molecular weight.

选择常规直接酰化、相转移催化酰化和离子交换-酰化共3种方法对3万中等分子量的κ-卡拉胶进行了乙酰化反应。

In this research, liposoluble chlorogenic laurate was synthesized by the acylation with lauroy chloride in the existence of alkali catalyst in non-water phase, and yellowish CGL powders with a yield of 81.24% were obtained under the optimal synthesis conditions determined via single-factor tests and orthogonal experiments, that is, carrying out the acylation at 35℃ for 8h with a n:n: n ratio of 1:1:1.5 and with dimethylformamide as the solvating agent and the thinner.

文中对绿原酸进行了改性，即在碱性催化剂催化的条件下使其与月桂酰氯进行非水相的酯化反应，得到了脂溶性的绿原酸月桂酸酯。经过单因素及正交试验，确定了最佳合成条件为：以N，N-二甲基甲酰胺作为溶解、稀释剂，绿原酸／月桂酰氯／三乙胺的摩尔比为1：1：1.5，温度控制在35℃，反应时间8h。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新