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By the The equipment,The ratio in use of resin was increased inside VC manufacture , less acid, alcali and water was spend, The operator make less error then before due to automatization level was increased. So the production level of the gulonic acid was increased,The cost price of the gulonic acid was reduced, It is very important to increase greatly the economic effectiveness of the enterprise.3, Finished the industrialization apparatus design and feasibility studies, and the new technical equipment was run triumphantly in industrialized production.

使用该设备系统可提高VC生产中提取工序的树脂用率,减少树脂使用过程中的酸、碱及水的消耗,同时自动化水平提高,人为失误减少,最终可提高古龙酸的生产水平,降低古龙酸的生产成本,对大幅度提升企业的经济效益有重大意义。3、完成工业化装置设计及可行性研究,并推上了生产。

SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.

并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析,结果显示SM6中主要为具有香气成分的不饱和脂肪醛,其中含量较高的依次为:-2,4-癸二烯醛(58%)、十四烷酸(55.78%)、2-癸烯醛(50%)、邻苯二甲酸异丁基十一烷酯(47%)、2,4-癸二烯(41%)、2-十一碳烯醛(31%)、2-甲基-Z,Z-3,13-十八碳二烯酸(18.45%)等;SM7中主要为饱和直链烷烃,其中含量较高的依次为:1,2-苯二羧酸丁基环己酯(23.90%)、三十烷(22.63%)、二十九烷(21.04%)、十七烷(18.84%)、二十八烷(13.58%)。

Mirror infiltrating the cancer vagina the image is that the blood vessel is abnormal mainly,original place cancer vagina mirror visible image acetic acid white epithellum,major partners the shape blood vessei,heterotype blood vessel,mosaic and floccosoids wait a little bit;CIN acetic acid white maximum appears on epithelium,the shape blood vessel,heterotype blood vessel,rnosaic and floccosoids take second place;The chronic cervicitis gives first place to no representative shape blood vessel China and acetic acid white epithelium.

浸润癌阴道镜图像主要是血管异常,原位癌阴道镜图像可见醋酸白色上皮,多数伴有点状血管、异型血管、镶嵌和白斑等;CIN醋酸白色上皮出现最多,点状血管、异型血管、镶嵌和白斑次之;慢性宫颈炎以不典型点状血管和醋酸白色上皮为主。

Mirror infiltrating the cancer vagina the image is that the blood vessel is abnormal mainly,original place cancer vagina mirror visible image acetic acid white epithellum,major partners the shape blood vessei,heterotype blood vessel,mosaic and floccosoids wait a little bit;CIN acetic acid white maximum appears on epithelium,the shape blood vessel,heterotype blood vessel,rnosaic and floccosoids take second place;The chronic cervicitis gives first place to no representative shape blood vessel China and acetic acid white epithelium.

浸润癌阴道镜图像主要是血管异常,原位癌阴道镜图像可见醋酸白色上皮,伴有点状血管、异型血管、镶嵌和白斑等;CIN醋酸白色上皮出现最多,点状血管、异型血管、镶嵌和白斑次之;慢性宫颈炎以不典型点状血管和醋酸白色上皮为主。

hexadecanoic acid,oleic acid and linoleic acid were the major constituents.

结论萝卜秦艽块根中挥发油的主要成分为烷烃类和有机酸及其酯类化合物,其中十六烷酸、油酸、亚油酸等成分含量较高。

The optimum synthetic conditions of hexadecanoic acid diethanolamide used two-step method are as follows:(1)reaction temperature was 140℃, reaction time was 4.5hours and molar ratio of hexadecanoic acid to diethanolamide was 1:1.15.(2)reaction temperature was 80℃, molar ratio of hexadecanoic acid to diethanolamide was 1:1.55 and mass concentration of the catalyst was 0.8%, reaction time was 3 hours.

二步法合成十六酸二乙醇酰胺最佳合成工艺为:(1)反应温度140℃、反应摩尔比n十六酸∶n二乙醇胺=1∶1.15、反应时间4.5h;(2)反应温度80℃、反应总摩尔比n十六酸∶n二乙醇胺=1∶1.55、催化剂用量0.8%、反应时间3h。

The obtained CBC was further reacted with stearic acid at 140℃ and hexadecyl alcohol at 180℃ in turn to form citric acid-beta-butylene glycol-citric acidstearic acid-hexadecyl alcohol claw large molecule.

以1,3-丁二醇、柠檬酸为原料,设计、合成了以1,3-丁二醇为核心的柠檬酸-1,3-丁二醇-柠檬酸爪状物小分子;再用酯化反应依次与带有功能化集团的硬酯酸、十六醇接枝合成了多元酯类爪形大分子柠檬酸-1,3-丁二醇-柠檬酸-硬酯酸-十六醇。

The sequence of amino acid of clone CR271 was highly homologic (61% identify and 76% similarity) to blight resistance gene Xal of rice to Xanthomonas oryzae pv. Oryzae. All other fragments showed significantly amino acidhomology to the NBS-LRR type resistance gene that have been cloned. The length of JR2 and JR3 fragments were 1321bp and 896bp respectively, which did not showed significantly homology on the level of amino acid and nucleotide acid to the sequences that have been known.

其中CR271与水稻白叶枯病抗病基因Xa1(AB002266)氨基酸同源性有61%相同,76%相似,其它片段与已克隆的NBS-LRR类抗病基因同源片段都具有较高的同源性;所获得的右翼序列JR2DNA片段长为1321bp,JR3DNA片段长为896bp,此两片段在核苷酸水平及氨基酸水平上均未找到有显著同源的序列。

Results At 2 h after damage in cerebral cortex 5-hydroxyindolecetic acid (5-HIAA) elevated remarkably; At 8 h after da-mage 5-hydroxytryptamine (5-HT), homovanillic acid elevated; but there was no obvious change on norepinephrine and 3,4-dihydroxyphenyl acetic acid.

结果 大脑皮质运动区在损伤后2小时5-羟吲哚乙酸(5-HIAA〕明显升高;8小时后5-羟色胺(5-HT)、高香草酸升高;去甲肾上腺素及3、4-双羟苯乙酸变化不明显。

The soil pH was found to be the main factor affecting BR formation of 14 C\|metsulfuron methyl among the basic properties of soil.(2)During the whole periods of the incubation,the 14 C\|BR of 14 C\|metsulfuron methyl in soils was mainly distributed in fulvic acid and humin.The relative percentage of 14 C\|BR in fulvic acid was higher than in humin,while the content of the 14 C\|BR distributd in humic acid only account for less than 1% of applied amount.

土壤pH是14 C 甲磺隆在土壤中形成BR的主要影响因子。14 C -甲磺隆在各类土壤中的14 C BR的最大值分别占引入量的 48 5%、46 5%、52 6%、1 9 3 %、49 7%、42 0 %和 46 5%;( 2 )在整个培养试验过程中,14 C 甲磺隆在 7种不同类型土壤中的14 C BR ,主要分布在富啡酸和胡敏素中,前者中的相对百分比大于后者,而在胡敏酸中的相对百分比较小。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

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