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They were acetic acid, benzaldehyde, n caproic acid, methyl pentadecanoic methyl ester, glycerin, benzoic acid,,9 octadecadienoic methyl ester, squalane, stearic acid and oleic eicosyl ester.

它们是乙酸、苯甲醛、正葵酸、-甲基十五烷酸甲酯、丙三醇、苯甲酸、,9-十八碳二烯酸甲酯、角鲨烷、硬脂酸和二十烷基油酸酯。

With the observation of the outward appearances, it can be known roughly that if the sample was added with adulterations. Since the beeswax dissolves in the benzene but the adulterations, such as gypsum, starch and so on do not, these can be determined. By the verification of acid value and alcohol dissolve ability, the acid or non acid added can be determined. By the change of saponification value, the ester or non ester added can be determined. By the carbonification degree in the concentrated sulphuric acid, the mineral wax, such as paraffin wax added can be determined.

通过样品外观的观察初步定性是否掺有杂质;利用纯蜂蜡在苯中溶解,而掺入的石膏、面粉和淀粉等杂质在苯中不溶而定量鉴定这类杂质;由酸值变化和乙醇溶解物的量,测定掺入的硬脂酸等酸性物质或其它的非酸性物质;由皂化值变化,定量测定掺入的动物脂等酯类物质或其它的非酯类物质;根据蜂蜡中的烃类在浓硫酸中可被炭化,加入的石蜡等矿物蜡不被炭化来测定此类掺杂物。

objective effects of plant tannins,chebulinic acid and tellimagrandin i on chemically induced hemoglobin synthesis in k562 cells were investigated.methods the hemoglobin synthesis situation was assayed with benzidine staining.erythroid antigens glycophorin a expression on the surface of k562 cells was labeled by direct immunofluorescence using fluorescein isothiocyanate-conjugated anti-gpa antibodies.then flow cytometric analysis was performed to detect gpa expression levels on surface of the cells.results both chebulinic acid and tellimagrandin i could inhibit the hemoglobin synthesis of butyric acid and hemin-treated k562 cells in a concentration-dependant manner.however,the ba-induced k562 cells were more sensitive to two tannins than heroin-induced cells.conclusion chebulinic acid and tellimagrandin i have inhibitory effect on the erythroid differentiation.

目的 研究可水解单宁诃子酸和特里马素i对氯化高铁血红素和丁酸钠诱导k562细胞红系分化的影响。方法四甲基偶氮噻唑蓝法分析诃子酸和特里马素i对k562细胞生长的影响,联苯胺染色法检测血红蛋白合成情况,应用免疫荧光和流式细胞术检测血型糖蛋白a在细胞表面的表达。结果诃子酸和特里马素i在0.04~0.09?mmol/l浓度下均可显著抑制k562细胞的生长增殖。2种单宁化合物(0.002~0.01?mmol/l)可显著抑制丁酸钠诱导的k562细胞血红蛋白合成,2种单宁化合物(0.01~0.05?mmol/l)还可显著抑制氯化高铁血红素诱导的血红蛋白合成,特里马素i(0.01?mmol/l)还抑制丁酸钠诱导的gpa在细胞表面表达。结论诃子酸和特里马素i对红系分化有抑制作用。

In this paper,firstly a series of acryloxyl derivatives were synthesized from the dehydrogenated abietic acid,a main composition of disproportionated rosin, through acyl chloridation and esterification.The derivatives included the (β-acryloxyl ethyl) esters of dehydrogenated abietie acid,(β-methacryloxyl ethyl) esters of dehydrogenated abietic acid and (β-methacryloxyl propyl)esters of dehydrogenated abietic acid.

论文首先以歧化松香中的主要成分脱氢枞酸为模型化合物,采用酰氯化、酯化手段合成了它的一系列丙烯酰氧基衍生物,包括脱氢枞酸酯、脱氢枞酸(β-甲基丙烯酰氧基乙基)酯和脱氢枞酸(β-甲基丙烯酰氧基丙基)酯。

Kinetics of photo-chlorination of acetic acid to form monochloroacetic acid ;2. The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究,采用硫磺及乙酐复合催化剂,并且对氯化温度、氯化气氛、尾气回收等进行了过程优化,实现了乙酸氯化反应工艺条件的重大突破,使得氯乙酸的收率达到92。

Diluted nitric acid, phosphoric acid, organic acid and medium containing smal amount of sulfuric acid or chlorion

抗病毒中和生物鉴定法进行干扰素中和抗体检测。2。但CO2只适用于强碱性、高酸中和能力的灰渣。

Sodium5sulfoisophthalic acid dimethyl ester was prepared by sulfonation of mC 6H 4 2 with chlorosulphonic acid , treatment of the 5sulfoisophthalic acid with methanol to esterify the -CO 2H groups and separation of the product in the form of sodium salt of sulfonic acid.

研究了由氯磺酸和间苯二甲酸经磺化及酯化反应合成间苯二甲酸二甲酯磺酸钠盐的工艺方法,探讨了投料比、反应温度、催化剂用量和反应时间对产物的影

Glycocholic acid is a kind of glycol-conjugated bile acid which exists in many animals'bile. It is one of main component of bile acid and was synthesized from cholalic acid and glycine in liver.

甘氨胆酸是胆汁酸的主要成分之一,属于结合型胆汁酸,在肝脏中由胆酸和甘氨酸结合而成。

The optimum condition was determined via orthogonal experiments, and the result shows that the technology of bile extraction and purification adopts 10L chromato bar with 3L bile, gel silica as fixed phase, the mixed chloroform and isopropanol as mobile phase, gradient elution with mobile phase (the mobile phase ratio in extraction of cholalic acid and glycocholic acid is 4:1 , and then becomes 3:2 in extraction of glycocholic acid and glycocholic acid), and eluting velocity of 3~5mL/s .

采用正交试验筛选了柱层析最佳条件,以容积为10L的层析柱进行分离纯化,固定相为硅胶,流动相为氯仿和正丁醇混合溶剂,一次装样量3000mL胆汁,流动相采用梯度洗脱,先按4:1比例分离胆酸和甘氨胆酸,然后按3:2比例分离甘氨胆酸和牛磺胆酸,流动相洗脱速度为3~5mL/s。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果:得到并鉴定了16个化合物,分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力