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The experimental results are as follows:(1) TBP was suitable to monobasic carboxylic acid solutes , but was not suitable to polybasic carboxylic acid solutes (such as succinic acid and citric acid).

首次采用BP神经网络分析方法预测了不同操作条件下的络合萃取分配系数,最终获得有工业化应用价值的络合萃取剂以及络合萃取技术处理有机羧酸稀溶液的工艺条件。

The results showed that monocarboxylic acid stearic acid played a role of surfactant, and the product was still orthorhombic Ce2O(CO3)2·H2O with a high crystallization degree. In turn, duality-carboxylic acid tartaric acid...

实验结果表明在尿素及硝酸铈的混合溶液中分别加入一元羧酸硬脂酸,二元羧酸酒石酸和三元羧酸柠檬酸时,一元羧酸硬脂酸在混合溶液中只起表面活性剂的作用,其产物为斜方晶系的单晶Ce2O(CO3)2.H2O微粉,且表面活性剂硬脂酸的加入使得晶体的晶化程度明显提高;而二元羧酸酒石酸与三元羧酸柠檬酸在均相反应中则起螯合剂的作用,分别与Ce3+形成螯合物酒石酸铈和柠檬酸铈,这些结果的造成是由于其反应机理的不同所导致的。

GUS expression activated by the OsGT1 promoter was strongly stimulated by NaCl and low temperature, moderately by abscisic acid and naphthaleneacetic acid, and not at all by salicylic acid and gibberellic acid.

表明水稻OsGT1基因主要在根和花中表达,与水稻抗盐与低温胁迫相关。

Substituted-2-aminobenthiazoles were dissolved in a mixture of acetic acid,phosphoric acid and propionic acid, and diazotized by nitrosylsulphuric acid, then coupled with m-dimethylaminobenzoicacid to form 6-R-BTAMB in good yield.

我们在2-氨基苯并噻唑的6-位引入了不同的取代基R,合成了6种新试剂,2-I2'-(6'-R-苯并噻唑)偶氮-5-二甲氨基苯甲酸(6-R-BTAMB,R=〓,〓,Cl,Br,〓,〓,),并研究了6-R-BTAMB与Fe、Co、Ni、Cu和Pd的络合显色反应的光度性能及不同R基团对试剂灵敏度及选择性的影响将6-〓-BTAMB应用于测定铝合金,电镀废液中的铜,人体毛发和矿泉水中铁的含量均取得了满意的结果。

After catheter insertion under transoral endoscopic guidance, animals were randomly assigned to one of the four groups: acid reflux (pepsin 0.3 mg/mL + taurodeoxycholic acid 0.155 mg/mL + acid pH 2); nonacid reflux (pepsin + taurodeoxycholic acid + pH 6); saline reflux; and unwounded control.

经口腔内镜引导下插入导管,并随机将兔子分组:酸返流组(胃蛋白酶0.3mg/ml+牛磺脱氧胆酸0.155mg/ml+酸pH=2);非酸返流组(胃蛋白酶+牛磺脱氧胆酸+pH=6);生理盐返流组;以及无损伤组。

Results13 compounds were identified, which accounted for 100 % of the essential oil of the skins of stem. The major compositions were n-Hexadecanoic acid (46.13%); Octadecanoic acid (15.44%),-9-Octadecenoic acid (13.73%), and-9,12-Octadecadienoic acid (7.79%).

结果通过计算机检索、图谱分析法鉴定出13种化合物,占总油量的100%,其主要成分为正十六烷酸(46.13 %)、十八烯酸(15.44 %)、-9-十八烯酸(13.73 %)及-9,12-十八碳二烯酸(7.79 %)。

Based on relative literatures,this part has included five resesearch aspects as below.1 Fifteen compounds were isolated and purified by extraction,column chromatography,and their structures were determined on the basis of spectral analysis: acteoside(Ⅰ-1),isoacteoside(Ⅰ-2),crenatoside(Ⅰ-3),cistanoside F(Ⅰ-4),sinapoyl-4-O-β-D-glucoside(Ⅰ-5),adenosine(Ⅰ-6),β-siterol(Ⅰ-7),oleanic acid(Ⅰ-8), succinic acid(Ⅰ-9),caffeic acid(Ⅰ-10),protocatechuic aldehyde(Ⅰ-11),p-hydro xybenzyl alcohol(Ⅰ-12),β-daucosterol(Ⅰ-13),D-galacitol(Ⅰ-14),D-mannitol(Ⅰ-15).Ⅰ-4~15 were obtained from this plant for the first time,andⅠ-6,7,9,and 13 were isolated from Orobanche genus for the first time.2 The scavenging test of DPPH showed that most compounds have comparative antioxidant activity as L-ascorbic acid and part of them show better activity such as the O.coerulescens extract and phenylethanoid glycosides.Acteoside showed potent free radical scavenging effects with a median inhibition concentration of 25.6μg/ml.3 The anti-HBV activities of acteoside,isoacteoside and crenatoside were measured,and all of them showed suppressive activity on the expression of HBsAg and HBeAg in the HepG2.2.15 cell line.

本论文在文献调研基础上对紫花列当化学成分及生物活性进行了研究,并从免疫抗病毒角度探讨紫花列当中特征性成分类叶升麻苷的肝保护作用及其机制。1采用大孔树脂、硅胶和Sephadex LH-20等色谱技术对紫花列当进行系统的植物化学研究,从中分离得到19个化合物,利用UV和NMR等波谱手段及理化性质鉴定了其中的15个化合物,分别为类叶升麻苷(Ⅰ-1)、异类叶升麻苷(Ⅰ-2)、crenatoside(Ⅰ-3)、cistanoside F(Ⅰ-4)、sinapoyl-4-O-β-D-glucoside(Ⅰ-5)、腺苷(Ⅰ-6)、β-谷甾醇(Ⅰ-7)、齐墩果酸(Ⅰ-8)、琥珀酸(Ⅰ-9)、咖啡酸(Ⅰ-10)、原儿茶醛(Ⅰ-11)、对羟甲基苯甲酸(Ⅰ-12)、β-胡萝卜苷(Ⅰ-13)、D-半乳糖醇(Ⅰ-14)和甘露醇(Ⅰ-15除化合物Ⅰ-1、Ⅰ-2和Ⅰ-3外,其余化合物均为首次从该植物中分离得到。2)通过大孔树脂富集该药材有效部位苯乙醇总苷,并采用HPLC测得其所含特征性成分类叶升麻苷的含量可达80%以上。3DPPH自由基清除试验显示紫花列当提取物及其所含的苯乙醇苷类化合物均具有较好的抗氧化能力,其清除DPPH自由基能力接近于抗坏血酸。4采用卡介苗整体致敏、脂多糖离体攻击构建大鼠原代肝细胞免疫性损伤模型,在体外观察类叶升麻苷的保肝作用。

All dates were analyzed by the principal component analysis through using the SIMCA-P 10.0 software. Result: The PCA demonstrated that the metabolome between treated group and control group had difference in rat urine sample after of 22 days administrated, for treated group 169 kinds of biomarkers were found including oxalacetic acid, malic acid, 2-ketoglutaric acid, NE, arachidonic acid, 5-HIAA and other compounds, the result was consistent with pharmacological effects of R.coptidis , such as antiinflammatory, inhibiting biosynthesis of CA biosynthesis, anti-central nerve and energy metabolism inhibition.

结果:给药22 d,黄连组与对照组大鼠尿样代谢组有较大差异,发现了169个生物标记物,其中可能的化合物为草酰乙酸、苹果酸、2-酮戊二酸、去甲肾上腺素、花生四烯酸、5-羟吲哚乙酸等物质,这与黄连抗炎、阻止儿茶酚胺的生物合成、抑制中枢神经、降低能量代谢的药理作用相一致。

In acid pulp, the depressing abilities of reagents on diaspore are in the order of hydroxamic acid starch>dialdehyde starch>carboxymethyl starch>cationic starch>primary starch. In addition, hydroxamic acid starch and carboxymethyl starch can activate kaolinite without influence on the recoveries of pyrophyllite and illite, so the two reagents have great potential and prospect to be the depressant of diaspore and the activator of kaolinite in bauxite reverse flotation.(3) By oximation of the copolymer of acrylamide and methyl acrylate, hydroxamic acid polyacrylamide is synthesized.

3对丙烯酰胺和丙烯酸甲酯的共聚物肟化制得氧肟酸聚丙烯酰胺,将它同非离子聚丙烯酰胺、阴离子聚丙烯酰胺、阳离子聚丙烯酰胺和两性聚丙烯酰胺分别应用于四种矿物的单矿物浮选试验,结果显示,改性聚丙烯酰胺对一水硬铝石、高岭石和伊利石均具有活化作用,其中,药剂对高岭石的活化最强,使它的回收率在整个pH值范围达到80%左右,在一定pH条件下超过一水硬铝石的回收率,解决了高岭石难浮选的问题。

In order to improve the electro-catalytic activity of platinum based catalyst to methanol oxidation, in this thesis, firstly prepare heteropoly acid modified Pt/GC electrode with different concentration by cyclic voltammetry method, and then test the cyclic voltammetry curves individually in vitriolic and methanol solution. The study shows the best concentration for both phosphomolybdic acid and phosphotungstic acid is 1×10~(-3)mol/L. And find the more heteropoly acid modified on electrode, the lower peak-up potential towards methanol because of the existence of oxygenous species.

为了改善铂基催化剂氧化甲醇的催化活性,本论文首先通过循环伏安扫描法制备了不同浓度磷钼酸和磷钨酸修饰的Pt/GC电极,通过研究Pt/GC电极在修饰前后在硫酸溶液中及含甲醇的硫酸溶液中的循环伏安行为发现,磷钼酸和磷钨酸均能在PtRu/C电极上发生氧化还原反应,而且杂多酸修饰浓度对Pt/GC电极氧化甲醇的催化活性有很大影响。

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。

However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。