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When the concentration of zinc nitrite is lower than 0.1 M,(002) is the prior face for zinc oxide. As the concentration raise, the other kinds of crystal face would appear. Among those data,(002) grows the best when the concentration of zinc nitrite is 0.06 M. We add lactic acid and citric acid respectively; there is an carboxyl group on the lactic acid and three carboxyl groups on the citric acid. The monodentate of lactic acid helps the growth of zinc oxide, compared to the tridentate of citric acid which can only produce zinc oxide film under very low concentration, but the growth of (002) face is not that stable as adding the lactic acid and zinc will electrodeposit to substrate.

实验中,当硝酸锌浓度低於0.1 M 时,氧化锌以(002)面为优选位相,当浓度提高,其他晶面将会出现,当硝酸锌为0.06 M,(002)晶面成长最佳,分别加入乳酸和柠檬酸,乳酸结构上有一羧基团而柠檬酸有三个羧基团,单芽基的乳酸有助於氧化锌成长,对照於三芽基的柠檬酸,则必须在极低的浓度下才能制备氧化锌薄膜,但(002)面成长却没有添加乳酸来的稳定而金属锌也会电沉积到基板上。

There weremainly p-hydroxybenzoic acid,vanillic acid,and syringic acid in soybean root exudates.Vanillicacid,syring acid and ferulic acid were found in soybean shoots.The soybean roots containedvanillic acid and p-coumaric acid.

大豆根分泌物中主要含有对羟苯甲酸、香草酸和丁香酸,而大豆植株地上部主要含有香草酸、丁香酸和阿魏酸,根部以香草酸和香豆酸为主。

Sulfuric acid series, hydrochloric acid (AR hydrochloride, CP hydrochloric acid) series, nitric acid, phosphoric acid, boric acid, protopine, soda ash, ammonia, acetic acid, bleaching powder, chloride, alkaline chlorine of aluminum, nickel chloride, nickel sulphate, polyacrylamide, such as hydrogen peroxide.

硫酸系列,盐酸系列,硝酸,磷酸,硼酸,片碱,纯碱,氨水,冰醋酸,漂白粉,聚合氯化铝,碱式氯化铝,氯化镍,硫酸镍,聚丙烯酰胺、双氧水等。

Thirdly, the acrylic rosin was synthesized by the addition reaction from gum rosin andacrylic acid. The levo-pimaric acid was converted into acrylic pimarie acid throughDiels-Alder addition with acrylic acid. The abietic-type acids in the gum rosin were inisomerization balance under high temperature, and the abietic acid and palstric acid would beconverted into levo-pimaric acid and reacted in the later type.

第三,通过脂松香与丙烯酸加成合成了丙烯酸松香,该反应是左旋海松酸与丙烯酸发生Diels-Alder加成反应生成丙烯海松酸,由于脂松香中的枞酸型树脂酸在高温下处于异构化平衡状态,因此随着反应的进行枞酸、长叶松酸等会异构化为左旋海松酸参与反应。

Most sugars, organic acids, phenolic acids and most amino acids increased significantly with elevated CO_2. The treatment, 950±50μmol·mol-1 CO_2 enrichment for 6 h every day had more obvious effects than the treatment, 950±50μmol·mol-1 CO_2 enrichment for 3 h every day. Levan, sucrose, arginine, oxalic acid, alanine, malic acid, acetic acid, lactic acid cinnamic acid,ρ- hydroxybenzoic acid and benzoic acid increased significantly.

CO_2施肥黄瓜根系分泌有机酸、氨基酸、糖和酚酸的总量增加,上、下午均施肥的处理分泌数量最多;CO_2施肥显著促进了果聚糖、蔗糖、草酸、苹果酸、乙酸、乳酸、多数氨基酸、肉桂酸、对羟基苯甲酸和苯甲酸等组分的分泌;单位鲜重根系分泌糖和酚酸的数量增加,多数氨基酸保持不变或降低,但有机酸分泌规律不一致。

The major acid detected in the apple rhizosphere and the wormcast was oxalic acid, malic acid, tartaric acid, succinic acid and malonic acid, one of highest content was oxalic acid.

苹果根际和蚯蚓粪中检测到的有机酸主要有草酸、苹果酸、酒石酸、琥珀酸和丙二酸,以草酸含量为高。

Kinds of commercial milk powder were analysed with GC-MS in order to learn about their fat acid compose,and the result illuminated that there were 28 kinds of fat acids were detected in all samples,and only octanoic acid and decanoic acid were detected from 4 kinds of season fat acids of hexanoic acid, octanoic acid ,nonanoioc acid and decanoic acid.

用气质联用色谱分析了11个商业奶粉样品的脂肪酸组成以及含量,每个样品均检测到了28种脂肪酸,在表现奶粉风味的4个呈味脂肪酸,也即辛酸、己酸、壬酸和葵酸中只检测到了辛酸和葵酸。

Long-chain Dicarboxylic acid; 11 carbon dicarboxylic acid; twelve carbon dicarboxylic acid; tridecanedioic acid; 14 carbon dicarboxylic acid; 15 carbon dicarboxylic acid; carboxylic acid

一期工程年产6000吨的发酵长碳链二元酸(DC11~DC15、DC18)生产线于2003年3月建成投产,装机容量6万KW的热电厂于2004年3月并网发电。

This article that focuses on the systematic and in-depth research in the current primal problem about abnormal burst pressure reservoir depress burst pressure has procured following main fruits:1 It forms the method which could obtain massive vertical static state mechanics parameters.2 In a foundation of acquisition of rock mechanics parameters,apply bent lamella that as mechanical model along with characteristic of actual geologic characteristics to analysis curvature for anticlinal strcture, get homologous tectonic stress value throug relation between the curvature and stress and different principal curvature in anticlinal structure,consequently set up laminational stress model for anticline reservoir. The block lamination for existed fracturing date has formed method of setting up mechanical model of lamination terrestrial stress by abtaining the block tectonic stress coefficients which are got by complex utilization test, laboratory test and fracturing date playback.3 Analysesing the main reason which lead to high burst pressure by considering the characteristic of reservoir geology,reservoir,and rock mechanics and reservoir damage,etc.Establishing burst pressure quantitative prediction model which provide gist for depressing construction risk and optimizing construction craft under the condition of open hole completion ,gun-perforated completion and damaged reservoir.4 Provding theoretical basis for interpreting acidification pretreatment which could depress busrt pressure by finding the relation between the influencing factors and rock machanics parameters and analysing the factors that have effect on rock mechanics parameters. Expounding the mechanism of reaction of mixed monomineral and acid from the angle of microcosmic element, evaluating quantitatively acid sensilility of different kinds of mineral effectively, and determing the first-order reaction dynamical equation of each mineral.5 Revealing rock mechanics property chage as a result of acid flooding in different condition by sandstone traumata experiment in different temperatures which combined with rock mechanics triaxial stress experiment.6 Associating damage mechanics with sandstone acidizing, established sandstone damage mechanics model in the foundation of the recognition on the rock mechanics parametric variation which is caused by acid-rock reaction in both macroscopic view and microscopic view ,also demonstrated those processes and quantitative estimated the acid busrt pressure to direct the site operation.

本文针对目前异常破裂压力储层降低破裂压力的主要问题展开较为系统和深入的研究,取得了以下主要成果:1形成了利用测井资料,结合室内岩芯测试结果,获取静动岩石力学参数的相关性特征,从而获得纵向上大量静态力学参数的方法。2在获取了岩石力学参数的此基础上,利用弯曲薄板作为力学模型,结合区块实际地质特征对背斜构造进行曲率分析,通过曲率与应力的关系,利用背斜构造不同部位的主曲率求得相应的构造应力值,从而建立起背斜储层的分层应力模型;对已有压裂资料的区块分层,形成了综合利用测试、室内实验、压裂资料反演获得该区块构造应力系数,建立起分层地应力的力学模型的方法。3综合考虑储层地质、油藏、岩石力学特性和储层伤害等因素,分析造成高破裂压力的主要原因,综合利用岩石力学、弹性力学等知识,建立了裸眼完井、射孔完井条件下以及储层受到伤害后的储层破裂压力定量预测模型,为降低施工风险和优化施工工艺提供了依据。4完成了物性、岩性影响岩石力学参数的因素分析,找出了各影响因素和岩石力学参数之间的关系,为从机理上解释酸化预处理降低破裂压力提供了理论基础;从微观元素的角度阐述了单矿物与酸反应的机理;并在此基础上,有效评价了各种矿物的酸敏感性,定量确定了岩石中各矿物的一级反应动力学方程。5完成了不同温度下的酸液类型、酸液浓度、注酸量等一系列砂岩损伤实验,结合岩石力学三轴应力实验,系统揭示了在不同条件下注酸而引起的岩石力学性质变化。6将损伤力学与砂岩酸化相结合,在宏观、微观两个方面认识酸岩反应引起岩石力学参数变化基础上,建立了砂岩损伤力学模型,并对其进行验证,在此基础上定量计算酸化后的破裂压力,有效指导现场施工

First design a reasonable XML Schema structure and under the restriction of XML Schema use XML to describe the UML class diagram and the related specification, and then extract the test specification of method from XML test script. Test specification refers to predicate sequences in the form of conjunctive normal form, extracted from basic constraint conditions of variables included in test scripts and expected outputs. Each conjunctive normal form can be transformed to an inequation set, and adopt 1×1 domain test strategy to every inequation set to produce the domain test matrix, which in turn produce the test case.

首先设计合理的XML Schema结构,并在该XML Schema的有效性约束下,用XML对UML类图及相关性约束进行脚本描述;其次对XML测试脚本进行分析,提取方法的测试规约说明,所谓测试规约说明就是从测试脚本中包含的变量的基本约束条件以及期望输出中抽取得到的以合取范式形式存在的谓词序列;每一合取范式对应一个不等式组,对每一个不等式组采用1×1域测试策略,生成域测试矩阵,最终得到测试用例。

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