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In addition, the activties of different catalyst were compered. The test proved the chloroplatinic acid– ethanol catalyst provides high yields of addition products without the formation of undesirable by-products, to provide the possibility of using less rigorous reaction condition, to provide a catalyst material, which is effective at low concentrations.

实验过程中特别对不同催化剂进行了比较,其中氯铂酸—乙醇催化剂提高了加成反应的产率,没有副产物生成,不需要苛刻的反应条件,在低浓度时有很好的催化效果。

Polyether modified polysiloxane was synthesized by the hydrosilation reaction of hydrogen containing silicone fluidand allyl polyether, using chloroplatinic acid as the catalyst.

以氯铂酸为催化剂,利用含氢硅油与烯丙基聚醚的硅氢加成反应,合成出聚醚改性硅油;然后用乙醇胺进行胺化反应,制成纸张用氨基改性聚醚硅油柔软剂。

Five new polysiloxane-platinum complexes ("Si-Pt-1"-"Si-Pt-5") have been prepared by reaction of chloroplatinic acid with various silica-supported polysiloxanes(1-5) bearing ligand group CHC6H4N(CH3)2, CHC6H4OH,- N(OC-CH3)2,-CN and - COOH.

以二氧化硅为载体的侧链上含有配位基团和-COOH的聚硅氧烷(1-5)分别与氯铂酸反应制备了五种聚硅氧烷-铂络合物(&St-Pt-l&—&St-Pt-5&)。

The sodium sulphonate of ethoxylated acrylic modified rosin can be obtained from acrylic modified rosin after the reaction with ethylene oxide and then be sulphonated with chlorosulphonic acid.

以松香为原料,用丙烯酸进行改性后再与环氧乙烷聚合,然后用氯磺酸进行磺化处理制得丙烯酸改性松香聚氧乙烯醚磺酸钠阴离子表面活性剂。

The reaction between 3, 4 cinnamic acid and 〓 has also been investigated as an evidence for the electron transfer mechanism.

以〓为过氧自由基模型,研究了羟基肉桂酸衍生物对该自由基的清除作用,发现这类化合物,特别是芥子酸,能够通过电子转移反应有效地还原过氧自由基。3,4-亚甲二氧基肉桂酸与〓的反应的动力学研究为电子转移机制提供了证据。

Application of organic acid catalysis to the polymerization of pyrroles and pentafluorobenzaldehydes, with the xylene as reaction medium instead of expensive collidine used in the conventional methodology, resulted in a relatively high yield of TPFPPH〓.

本研究利用有机酸如氯乙酸催化吡咯和五氟化苯甲醛聚合,并以二甲苯替代传统方法所用的昂贵溶剂2,4,6-三甲基吡啶,获得了产率较高的TPFPPH〓。

R-1,c-2, t-3, t-4-1,3-bis(4-biphenyl)-2,4-di(4-pyridyl)cyclobutane was obtained in diluted sulfuric acid by photodimerization reaction.

通过反-1-(4-联苯基)-2-(4-吡啶基)乙烯在稀硫酸中的光二聚反应合成了r-1,c-2,t-3,t-4-1,3-双(4-联苯基)-2,4-二(4-吡啶基)环丁烷。

Ketoheptamethylenimine was prepared by one-pot reaction of cycloheptanone with concentrated sulfuric acid. In this step, oximation and rearrangement occurred .

制备庚内酰胺时,我们采用了&一锅反应&的方法,环庚酮、浓硫酸和硫酸羟胺混合在一起,经过肟化、重排一次得到庚内酰胺。

The catalytic activity of iodine in the esterification reaction was studied by synthesis cyclohexyl acetate from acetic anhydride,cyclohexano and acetic acid,cyclohexano.

以单质碘为催化剂,通过乙酸酐、环己醇及乙酸、环己醇为原料合成乙酸环己酯,对碘的催化活性进行了研究。

In the second part of the thesis, we discussed a L-proline-catalyzed direct Aldol reaction between L-amino acid-derived N,N-dibenzyl -amino aldehydes 15 and acetone, cyclopentanone or hydroxyacetone, which afforded (-amino--hydroxy- or (-amino-,(-dihydroxy-ketones in good to excellent yields (up to 94%) and diastereoseletivities (up to 94.9%).

发现许多情况下,反应的产率和de值超过90%。接着,在碱性条件下,我们将L-亮氨酸衍生的N,N-二苄基--氨基醛15g与羟基丙酮反应得到的主要产物(,-二羟基-γ-氨基酮171d与次溴酸钠反应,得到了具有抗肿瘤活性的天然产物PM-94128的氨基酸片断184。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。