查询词典 acid reaction

It is the most important solid-liquid reaction that sulfuric acid decomposes phosphate rock in phosphate fertilizer production. By contrast with conventional reaction of acid decomposing phosphate rock, the effects of ultrasonic power, reaction time, and temperature are discussed.

硫酸分解磷酸是磷肥工业中最重要的液固分解反应，本研究从磷矿酸解液—固反应着手，通过对比的方法，探讨常规的液—固反应体系施加超声波后，超声的声强、时间、温度对磷矿酸解的影响。

Alkylamine reaction with dialkyl cyanodithioiminocarbonate was catalyzed by quaternary ammonium salts at room temperature to yield 3-alkylamine-5-amino-1,2,4-triazole in good quality and high yields. After imidization and reaction with an α,β-unsaturated acid derivative, the reaction intermediate was hydrolyzed in the presence of a Lewis acid to obtain the target product.

烷基胺与氰基亚胺硫代二甲酯在季氨盐催化作用下得到质量好、收率高的3-烷氨基-5-氨基-1，2，4-三氮唑，进一步经过亚胺中间体并与α，β-不饱和酸酯作用后，中间产物在Lewis酸催化作用下水解得到三唑嘧啶酮。

In order to obtain 3-methoxy-4-hydroxymandelic acid with high quality and high yield, guaiacol was condensed with glyoxylic acid in an alkaline aqueous solution using solid acid as catalyst. The reaction temperature and reaction time was 15℃ and 18 hours respectively.

为了得到高质量和高收率的3-甲氧基－4-羟基苯乙醇酸，使愈创木酚和乙醛酸在碱性水溶液中在固体酸催化剂存在下进行缩合反应，反应温度15℃，反应时间18h。

By using a fracture simulation unit,the regularity that temperature,flow rate and fracture width influence on HCl/dolomite reaction rate is investigated.The sequence of temperature,flow rate,acid concentration and fracture width influence to the acidic rock reaction rate is also studied in a four factors and four levels orthonormal test,and the sequence that acid concentration＞flow rate＞temperature＞fracture width is found.At the last,the possible HCl/dolomite reaction mechanism model which can explain the influence factors is derived.

文中利用人工模拟裂缝装置，研究了温度、注酸排量、裂缝宽度等因素对盐酸/白云岩反应速率的影响规律；并采用四因素四水平的正交试验，综合考察了温度、排量、酸浓度、缝宽四种因素对酸岩反应速率的影响的主次顺序，发现对酸岩反应速率影响力的大小次序为：酸浓度＞排量＞温度＞缝宽；最后，提出了盐酸/白云岩反应可能的机理模式，并根据这一模式对诸因素的影响进行了合理的解释。

Under basic conditions p-nitrotoluene was oxidized to p-nitrobenzoic acid with oxygen or air. The reaction parameters, such as reaction temperature, reaction time, substrate concentration were optimized and 75% of p-nitrobenzoic acid was obtained under proper conditions.

论文探讨了在碱性条件下，用空气／氧气氧化对硝基甲苯的反应，得出了温度、时间、底物浓度、催化剂用量等工艺参数对反应的影响，在较佳的工艺条件下，对硝基苯甲酸的收率可达到75％左右。

The key steps involved Friedel-Crafts reaction of o-cresol and the Wittig reaction for construction the skeleton of amine moiety,at the same time, using the synthesis of E,(7S)-7-methoxytetradec-4-enoic acid in chapter 2,and Johnson-Clainsen rearrangement as a key step for construction the fatty acid part,the corresponding acid was prepared in 23%and 50%overall yield,respectively.

随后将手性不饱和脂肪酸和氨片段进行酰胺化反应构筑了malyngamide M的基本骨架，再将Z-烯氯转化为E-烯氯完成了目标分子的全合成，高立体选择性地构筑了末端烯氯结构，为制备其它含有类似烯氯结构的malyngamides探索出行之有效的合成路线。

The optimum reaction conditions were as follows: rosin 5 g, m: in: m 1:2:2, palladium chloride 0.090 %, n: n1:10, hydrogen pressure 5 MPa, reaction temperature 160℃ reaction time 3 h, mass fraction of abietic acid could be under 1%, mass fraction of dehydroabietic acid was 5.6%, which conforms to the national standards. The regeneration of catalyst was investigated. After cycling five times, the product of hydrogenated rosin still conforms to the national standards without any treatment of catalyst.

在松香5g、m：m：m1：2：2、氯化钯0.090%、n：nl：10、氢气压力5MPa，反应温度160℃，反应时间3h的较佳工艺条件下，产物氢化松香中极酸的质量分数小于1%，去氢枞酸的质量分数5.6%，符合GB/T 14020-2006国家标准；并对催化剂的重复使用性能进行了考察，催化剂相不经过处理直接重复使用5次后，产品氢化松香仍然符合国家标准中关于枞酸和去氢枞酸的指标要求。

The proper synthetic technology are as follows: molar ratio of P-aminobenzene sulfonic acid/phenol/formaldehyde is 1∶2∶9, concentration of P-aminobenzene sulfonic acid is 0.4mol·L~-1 , pH of reaction system is 8.0, reaction temperature is 95℃ and reaction time is 3.5h. aminobenzene sulfonate ; dispersant ; ceramic grind additives

国外在磨矿行业已大量使用高效减水剂助磨并取得了显著效果，国内关于这方面的研究起步较晚，主要采用如碳酸钠、硅酸钠、磷酸钠等无机盐，而且也主要是用于有色金属选矿方面，在硅酸盐工业原料加工中有部分采

To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

Isoamyl isovalerate was synthesized through esterification reaction by using isovaleric acid and isoamyl alcohol as raw materials and nano-H4SiW12O40/SiO2 as catalyst, the influencing factors in the reaction were studied, and the results showed that the esterification rate could reach 98.6 % under the conditions of the ratio of alcohol-acid 1.4∶1, the use level of catalyst 5 %, and the reaction time 1.5 h.

以纳米复合钨硅杂多酸为催化剂，异戊酸和异戊醇为原料，通过酯化反应合成苹果油，对酯化反应的影响因素进行了研究，结果表明，在醇酸物质的量比为1.4∶1，催化剂用量5%，反应时间1.5h的条件下，酯化率可达98.6%。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。