查询词典 acid reaction

The effects of technological conditions of different temperatures,sulfuric acid concentration,particle size,liquid/solid ratio and reaction time on levulinic acid yield were investigated,respectively.

分别考查了不同温度、硫酸浓度、原料粒度、液固比和反应时间对小麦秸秆转化乙酰丙酸产率的影响。

The effect of water-carring agents, mole ratio of malonic acid to benzaldehyde, dosage of catalyst and reaction time on the yield of cinamic acid was discussed.

探讨带水剂的种类、原料比、催化剂用量和反应时间等对肉桂酸收率的影响。

Cinnamic acid was synthesized from benzaldehyde and malonic acid by Knoevenagel reaction with pyridine as catalyst.

以苯甲醛和丙二酸为原料，吡啶为催化剂，利用 Knoevenagel 反应合成肉桂酸，从而降低了反应温度，提高了收率和产物纯度，简化了合成工艺。

The decisive influencing factor of viscosity in carboxyl-methylation was cross-linking reaction. Carboxyl-methylation was the main influencing factor of solubility and swelling capacity in modification of high content amylose starch. The structure and gelatinization property of different amylose content were analyzed with an Olympus Vanox BHS-2 multi-function optic microscope, and the results were as follows. The structure of ordinary cornstarch was different from the high amylose; gelatinization temperature and pH value of starch were affected deeply by amylose content, but had little difference between the gelatinization of high content amylose starch contained 50% and 70% amylose; pH value had much more effect than temperature on the gelatinization of high content amylose cross-linked starch. Monochloroacetic acid consumption, alcohol concentration and pH value influenced the starch carboxyl-methylation. When alcohol concentration was 60%, pH value 10, monochloroacetic acid/starch mass ratio 55%, the carboxyl-methylation of high amylose cross-linked cornstarch had the best result. With the In-Vitro digestibility model and biodegradation experiment, the digestibility and biodegradability of high amylose cornstarch and its modified starch were detected.

采用Brabande粘度测定仪和Olympus Vanox BHS-2型多功能光学显微镜等分析手段对链淀粉含量50％和70％的高链玉米淀粉及其交联和交联羧甲基化淀粉的结构和性质进行了表征和分析，结果表明，普通玉米淀粉结构与含链淀粉50％和70％高链玉米淀粉结构不同；高链淀粉比普通淀粉难糊化，高链改性淀粉糊化受pH值影响较大，受温度影响较小；淀粉的冻融稳定性、透光率、溶解度、膨胀度和粘度受链淀粉的含量和改性的影响，但是，链淀粉含量超过50％时，则链淀粉含量对淀粉的膨胀度和溶解度影响不大；改性淀粉性质的影响因素中，影响粘度主要因素是交联反应，影响透明度、溶解度和膨胀度主要因素是羧甲基化改性；一氯乙酸用量、反应时乙醇浓度及碱性条件都会影响高链淀粉及其交联淀粉的羧甲基化改性效果，制备羧甲基化改性淀粉的最佳工艺是在pH值为10的60％的乙醇浓度介质中按一氯乙酸/淀粉质量比为55％进行取代反应。

The myristic-2-hydroxy-3-propane sulfonic acid sodium salt was synthesized from sodium bisulfite, epichlorohydrin, sodium phosphate and myristic acid. The influence factors of temperature, amount of catalyst, reaction time and reactant ratio on conversion were studied.

以亚硫酸氢钠、环氧氯丙烷、磷酸钠和肉豆蒄酸等为原料，合成了肉豆蒄酸－2-羟基－3-磺酸钠丙酯，探索了反应温度、催化剂、反应时间、反应物物质的量比等因素对合成的影响。

A modified γ-Al〓O〓 was prepared by a special precipitation method with aluminum nitrate solution containing a certain amounts of orthosilicic acid and ammonia aqueous solution. Compared with commercial γ-Al〓O〓, the modified γ-Al〓O〓 was an effecient catalyst for dehydration of tetrahydrofurfuryl alcohol to dihydropyran. The results revealed that the strong acid sites on the surface of the catalyst may play a crucial role in this reaction.

并以硝酸铝和氨水为原料，用沉淀法制备出一种高比表面和拥有较多强酸中心的γ-Al〓O〓，它在四氢糠醇开环脱水制备二氢吡喃的反应中有优良的催化活性，通过比较此γ-Al〓O〓和普通商业γ-Al〓O〓的Py-TPD图，发现强酸中心在制备二氢吡喃的反应中可能具有关键的作用。

Five chalcones were synthesized via the aldol condensation reaction of acetophenone or parasubstituted acetophenones with 1-phenyl-3-methyl-5-phenoxyl-pyrazol-4-aldehyde, which reacted with two kinds of hydrazine in glacial acetic acid under refluxing to give a series of bipyrazoline derivatives. In this synthetic course, glacial acetic acid is not only a solvent, but also a catalyzer.

以1-苯基－3-甲基－5-苯氧基－吡唑-4-甲醛为原料，与苯乙酮发生羟醛缩合，生成相应的查尔酮，再在冰醋酸中与不同的肼反应，高产率的合成出10种新的5位含1-苯基－3-甲基－5-苯氧基－吡唑基的吡唑啉类衍生物。

The process of the present invention consists in bringing into contact, on the one hand, gaseous phosphorus pentafluoride or a gaseous mixture comprising phosphorus pentafluoride and hydrochloric acid, and, on the other hand, a solution of lithium fluoride in hydrofluoric acid, in a column (10) having a sufficient number of transfer units to carry out the reaction of PF5 with LiF under the chosen conditions of temperature, of pressure and of molar ratio of the two contrasting reactants and with complete or substantially complete absorption of the PF5 in the column.

本发明方法是让气态五氟化磷或五氟化磷与盐酸的气态混合物与氟化锂的氟氢酸溶液在塔（10）中接触，该塔转化单元数足以在选定温度、压力与两种反应剂摩尔比条件下使PF5与LiF反应，塔中五氟化磷完全或基本完全被吸收。

The paper introduced three processes to prepare isochroman from β-phenethyl alcohol and polyformaldehyde:HCl catalysis,AlCl_3 catalysis and toluene-p-sulfonic acid catalysis,and discussed its reaction mechanism,using toluene-p-sulfonic acid catalysis method to prepare isochroman ,the yield is 46%,purity is 96%.

用β-苯乙醇和多聚甲醛为原料，进行了HC l催化法，三氯化铝催化法和对甲苯磺酸催化法的合成路线的实验，并对其反应机理进行了探讨，应用对甲苯磺酸催化法合成异色满的合成路线，得率46%，纯度96%。

Synthesis and Crystal Structure of a Ternary Complex: [Ni2].8H2O GAO En-Jun YU Ying WANG Ke-Hua SNN Ya-Guang LI Hao-Yang (Laboratory of Coordination Chemistry, Shenyang Institute of Chemical Technology, Shenyang 110142, China) ABSTRACT A new ternary complex .8H2O (phen = 1,10-phenanthroline, Pmal 2－= phenethyl malonic acid) has been synthesized by the reaction of nickel acetate, phen and phenethyl malonic acid.

综合和三部组成的复合体的晶体结构： [Ni 2]。8H2O GAO En6月YU Ying WANG Ke华SNN Ya广李郝杨(实验室协调化学，化工技术沈阳学院，沈阳110142，中国)摘要A新的三部组成的复合体。8H2O (phen = 1，10二氮杂菲， Pmal 2-=苯乙基丙二酸的酸)由镍醋酸盐， phen和苯乙基丙二酸的酸的反应综合了。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。