查询词典 acid reaction

The composition and solubility of the main impurities in crude azelaic acid ,which was the reaction product of ozonolysis of oleic acid,were analyzed in detail.

以油酸臭氧氧化法制备的纯度为88.37%的壬二酸粗品为原料，用固液萃取法分离提纯，得到了纯度为98.73%的壬二酸。

In the first section, the effect of sodium houttuyfonate on the level of lysozyme secreted by macrophages was first tested by bacteriolytic method; then the effect of sodium houttuyfonate on the level of tartaric acid resistant acid phosphatase produced in macrophages was investigated by analyzing the phenol generated in the reaction that was catalyzed by the enzyme; the third, the effect of sodium houttuyfonate on the phagocytic activity of macrophages was observed by microscopy; the forth, the effect of sodium houttuyfonate on the production of complement C4 from macrophages was tested by hemolytic method; the fifth, the effect of sodium houttuyfonate on the expression of C3b receptors on the surface of macrophages was analyzed by observing the formation percentage of zymosan wreath; the sixth, the effect of sodium houttuyfonate on the respiratory burst in macrophages was tested by flow cytometry; the seventh, the effect of sodium houttuyfonate on the production of IL-1α and IL-1β from macrophages was tested by ELISA method.

在这一章中，首先，采用溶菌法考察合成鱼腥草素对巨噬细胞分泌溶菌酶水平的影响；其次，采用游离酚法研究合成鱼腥草素对巨噬细胞产生的耐酒石酸酸性磷酸酶水平的影响；第三，采用显微镜观察法考察合成鱼腥草素对巨噬细胞吞噬功能的影响；第四，采用溶血法测定合成鱼腥草素对巨噬细胞产生的补体C4水平的影响；第五，采用酵母花环法检测合成鱼腥草素对巨噬细胞表面C3b受体水平的影响；第六，采用流式细胞术法观察合成鱼腥草素对巨噬细胞呼吸爆发的影响；第七，采用ELISA法探讨合成鱼腥草素对巨噬细胞产生IL-1α及IL-1β水平的影响。

The method is based on a diazotion-coupling reaction between benzidine and hydrochloric acid naphthyl ethylenediamine in a hydrochloric acid medium.

在酸性条件下，亚硝酸盐与联苯胺重氮化，再与盐酸萘乙二胺偶联生成蓝色产物，该产物在578 nm处有最大吸收值，并由此建立了一种简单、快速、灵敏的亚硝酸盐测定方法。

Objective: To use p-toluene sulfonic acid as the catalyst for the esterification reaction of cinnamic acid with isoamyl alcohol in liquid phase.

目的：以对甲苯磺酸为催化剂对肉桂酸与异戊醇的液相酯化反应进行研究。

In acetic acid and using cobaltous acetate as catalyst m-chlorobenzoic acid was synthesized by the reaction of m-chlorotoluene with oxygen.

在醋酸溶液中，醋酸钴为催化剂，以间氯甲苯、氧气为原料合成间氯苯甲酸，分别研究了反应温度、反应时间、原料配比、催化剂的用量等条件对合成反应的影响，确定了最佳工艺条件。

The invention uses the method of the fusion and direct polymerization to prepare the carboxyl-terminated lactic acid prepolymer and then copolymerize with the aliphatic polycarbonate; then the reaction is done in the twin-screw extruder to screw out the extension chain and the good polylactic acid copolymer is made.

本发明采用熔融直接缩聚的方法制备出羧基封端的乳酸预聚物，接着再与脂肪族聚碳酸酯二元醇进行共聚，然后再在双螺杆挤出机中进行反应挤出扩链，制备性能良好的聚乳酸共聚物。

The orthogonal experimental result showed that the optimum reaction conditions were as follows: citric acid 7.7 g, isoamyl alcohol 21.7 mL(the molar ratio of citric acid to isoamyl alcohol, 1:5); 1.0 g (4% of the total weight of raw material) NaHSO4H2O as catalyst; 25 mL dimethyl benzene as deaquation reagent; microwave irradiation time 15 mm; the yield of product was 83.2%(the rate of esterification was 95.1%).

通过正交实验，得到最佳的工艺条件如下：柠檬酸7.7g，异戊醇21.7mL（酸醇摩尔比为1：5）；一水合硫酸氢钠作催化剂，用量为1.0 g（为原料总质量的4%）；带水剂为二甲苯，用量为25mL；微波辐射时间为15min。

Factors of esterfication of mixed dibasic acid were studied: alcohol acid mol ratios, the content of the catalysts, the reaction time and the content of water carrier.

实验考察了混合二元酸酯化的影响因素：醇酸摩尔比、催化剂用量、反应时间以及带水剂的种类和用量对酯化率的影响。

The metalorganic complex NaEu4 is prepared by europium and Dibenzoyl Methane. The coordination polymers Eu-DBM-PAA and NaEu-DBM-PSAA are synthesized by the reaction of NaEu4 with polyacrylic acid M(subscript r=5000and copolymer of acrylic acid and styrene M(subscript r=3000.

研究了铕和二苯甲醯甲烷形成的有机配体NaEu4与聚丙烯酸M(下标 r=5000）、聚M(下标 r=3000发生配位反应分别得到配合物Eu-DBM-PAA和NaEu-DBM-PSAA，得率分别为89.7%和87.3%。

Three aspects were included here:The derivatives of dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid were synthesized via three different routes:(1) four new compounds were synthesized via the reaction bet ween dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid, thionyl chloride and corresponding alcohol ;(2) first ,dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate wer e synthesized, then ,another four new compounds were obtained t hrough the alcoholysis under the catalyst ;(3) three acylamines were got through the ammonolysis betw een dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate and amines.

本论文分别通过三条不同的路线合成了1，4-二氢-3，6-二甲酸-s-四嗪的衍生物：(1)通过1，4-二氢-3，6-二甲酸-s-四嗪与氯化亚砜和相应的醇反应，制备了四个新化合物；(2)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪，在催化剂的作用下，与高沸点的醇进行酯交换反应，合成了四个新化合物；(3)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪后，与胺进行氨解反应，合成三个新的1，4-二氢-3，6-二甲酰胺-s-四嗪化合物。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。