查询词典 acid ratio

The decisive influencing factor of viscosity in carboxyl-methylation was cross-linking reaction. Carboxyl-methylation was the main influencing factor of solubility and swelling capacity in modification of high content amylose starch. The structure and gelatinization property of different amylose content were analyzed with an Olympus Vanox BHS-2 multi-function optic microscope, and the results were as follows. The structure of ordinary cornstarch was different from the high amylose; gelatinization temperature and pH value of starch were affected deeply by amylose content, but had little difference between the gelatinization of high content amylose starch contained 50% and 70% amylose; pH value had much more effect than temperature on the gelatinization of high content amylose cross-linked starch. Monochloroacetic acid consumption, alcohol concentration and pH value influenced the starch carboxyl-methylation. When alcohol concentration was 60%, pH value 10, monochloroacetic acid/starch mass ratio 55%, the carboxyl-methylation of high amylose cross-linked cornstarch had the best result. With the In-Vitro digestibility model and biodegradation experiment, the digestibility and biodegradability of high amylose cornstarch and its modified starch were detected.

采用Brabande粘度测定仪和Olympus Vanox BHS-2型多功能光学显微镜等分析手段对链淀粉含量50％和70％的高链玉米淀粉及其交联和交联羧甲基化淀粉的结构和性质进行了表征和分析，结果表明，普通玉米淀粉结构与含链淀粉50％和70％高链玉米淀粉结构不同；高链淀粉比普通淀粉难糊化，高链改性淀粉糊化受pH值影响较大，受温度影响较小；淀粉的冻融稳定性、透光率、溶解度、膨胀度和粘度受链淀粉的含量和改性的影响，但是，链淀粉含量超过50％时，则链淀粉含量对淀粉的膨胀度和溶解度影响不大；改性淀粉性质的影响因素中，影响粘度主要因素是交联反应，影响透明度、溶解度和膨胀度主要因素是羧甲基化改性；一氯乙酸用量、反应时乙醇浓度及碱性条件都会影响高链淀粉及其交联淀粉的羧甲基化改性效果，制备羧甲基化改性淀粉的最佳工艺是在pH值为10的60％的乙醇浓度介质中按一氯乙酸/淀粉质量比为55％进行取代反应。

First of all, a monophase microemulsion was prepared with Triton X-100 as surfactant, and the nitration of phenols by concentrated nitric acid in the systems was studied. The influence of the mass fraction of nitric acid, oil/water volume ratio, reaction temperature and other factors on the reaction conversion and selectivity was examined.

首先在非离子表面活性剂Triton X-100形成的单相微乳体系中，用浓硝酸对苯酚进行选择性硝化反应，研究了硝酸的质量分数、微乳中油/水比、反应温度等因素对反应转化率及硝化选择性的影响。

The myristic-2-hydroxy-3-propane sulfonic acid sodium salt was synthesized from sodium bisulfite, epichlorohydrin, sodium phosphate and myristic acid. The influence factors of temperature, amount of catalyst, reaction time and reactant ratio on conversion were studied.

以亚硫酸氢钠、环氧氯丙烷、磷酸钠和肉豆蒄酸等为原料，合成了肉豆蒄酸－2-羟基－3-磺酸钠丙酯，探索了反应温度、催化剂、反应时间、反应物物质的量比等因素对合成的影响。

The experiment results showed that the optimum reaction condition were as follow: the molar ratio of acrylic acid to octadecyl alcohol was 1.2:1, the amounts of solid super acid and hydroquinonone were 6.0% and 0.8% respectively, reaction temperature and time were 120℃ and 3h. In this condition, the percentage of esterification of octadecyl acrylate was 97%.

由实验得出的最佳合成条件是：丙烯酸与十八醇的摩尔比为1.2：1，固体超强酸及对苯二酚的质量分数分别为6%，0.8%，反应温度为120℃，反应时间为3 h，在此反应条件下，酯的产率可达97%。

The result indicated that: the amount of the excess HF formed direct ratio to the yield of phosphorus pentafluoride and the optimum amount of the excess HF used is about 35%; the trickling rate of oleum shouldnt make the temperature of hexafluorophosphoric acid exceed 25 ℃ and the amount of oleum is 110% to 125% that of stoichiometry so that the content of phosphorus pentafluoride can be achieved 90%; the time and temperature of heating hexafluorophosphoric acid influenced both the yield and the content of phosphorus pentafluoride, and the optimum time should be about 30 minutes and the proper temperature was 148 to 153℃; when alcohol used asrefrigerant, the content of phosphorus pentafluoride was 94.03%, and the content can be up to 97.38%, provided that using liquid nitrogen as refrigerant.

通过实验发现，氟化氢用量与五氟化磷的产率成正比，最佳过量百分率宜在35％左右；发烟硫酸的滴加速度不能使中间产物温度大于25℃，发烟硫酸用量大于理论量10％～25％时，得到的五氟化磷纯度高于90％；六氟磷酸的加热温度对五氟化磷的产率和纯度均有影响，宜在148～153℃的范围内，加热时间应在30分钟左右；用工业酒精做冷凝介质得到的五氟化磷纯度最高只能到达94.03％，使用液氮做冷凝介质可以使五氟化磷的纯度达97.38％以上。

The process of the present invention consists in bringing into contact, on the one hand, gaseous phosphorus pentafluoride or a gaseous mixture comprising phosphorus pentafluoride and hydrochloric acid, and, on the other hand, a solution of lithium fluoride in hydrofluoric acid, in a column (10) having a sufficient number of transfer units to carry out the reaction of PF5 with LiF under the chosen conditions of temperature, of pressure and of molar ratio of the two contrasting reactants and with complete or substantially complete absorption of the PF5 in the column.

本发明方法是让气态五氟化磷或五氟化磷与盐酸的气态混合物与氟化锂的氟氢酸溶液在塔（10）中接触，该塔转化单元数足以在选定温度、压力与两种反应剂摩尔比条件下使PF5与LiF反应，塔中五氟化磷完全或基本完全被吸收。

The reaction between 2-hydroxy benzoic acid and 3-methyl-1-butanol using phosphotungstic acid as catalyst were studied and the best catayst amount, react'ratio and reaction time were also discussed.

研究以磷钨酸为催化剂，由水杨酸与异戊醇制备水杨酸异戊酯的工艺条件，找到最佳催化剂用量，最佳反应时间及醇酸摩尔比，并研究了带水剂对反应收率的影响。

Cyclization: cyclization occurs at 100℃in polyphosphoric acid for 4h in the mass ratio of 3-(4-methoxyanilino) propionic acid to PPA with 1:8, and 6-methoxy-2,3-dihydro-4-quinolone is formed in 50.5% yield with a method of rapid chromatographic column, c.

成环反应：质量比[3-(4-甲氧苯氨基)丙酸∶多聚磷酸]=1∶8，反应温度为100℃，反应时间4h，柱层析纯化后6-甲氧基-2，3-二氢-4-喹啉酮的收率为50.5％；c。

METHODS: 15 g/L silk fibroin solution was made by degumming, salvation and dialysis. Chitosan was dissolved in 2% acetic acid solution to prepare 25 g/L chitosan-acetic acid solution. Two solutions were mixed to prepare six silk fibroin/chitosan solutions, and mass ratio was 10: 0, 5: 5, 4: 6, 3: 7, 2: 8, 0: 10. These solutions were separately sucked in a 24-well plate. Following exhausting gas vacuole at 4 ℃, precooling was performed at -20 ℃ for 12 hours, followed by cryodesiccate for 30 hours.

通过脱胶、溶解、透析这3个主要步骤制成质量浓度为15 g/L的丝素溶液，将壳聚糖溶解在2%的醋酸溶液中制成25 g/L的壳聚糖-乙酸溶液，然后将两者混合，配制成丝素/壳聚糖质量比分别为10∶0，5∶5，4∶6，3∶7，2∶8，0∶10的6种溶液，分别吸入24孔板中，4 ℃排出气泡后，-20 ℃预冷冻12 h，再冷冻干燥30 h。

The influences of ratio of liquid to solid, concentration of ethanol in solvent and leaching time on recovery of phenol and caustic soda and yield of fatty acid and sebacic acid were investigated.

在癸二酸传统生产工艺中的裂解工序后增加浸取工序回收游离碱和苯酚，通过正交试验，考察了液固比、浸取剂浓度和浸取时间对氢氧化钠和苯酚回收及对脂肪酸和癸二酸产率的影响，确定最佳回收工艺条件为：液固比2.5，浸取剂为95％的乙醇水溶液，浸取时间为15min。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。