查询词典 acid anhydride

Star polymer ; 1; 1-Trihydroxymethylpropane ; Sebacic acid diacetic anhydride ; PEG

星型聚合物； 1； 1-三羟甲基丙烷；癸二酸二乙酸酐；聚乙二醇

The results indicate that there are strong dipole or ionic pairs interactions between carboxylic acid or anhydride and dimethylamino groups in reactive blends, so reactive compatibilizers are formed at the interphase, which can reduce the interfacial tension and improve interfacial adhesion between the component polymers, meanwhile the morphologies of the reactive blends become more fine and uniform, the dispersed domain size decreases remarkable.

研究结果表明：在PS/PE-g-MAH/St-Co-DMA和PS/EPDM-g-DMA/St-Co-MAH反应性共混体系中，反应性聚合物所含的酸酐基团与叔胺基团存在离子对间的相互作用；在PS/Surlyn/St-Co-DMA和PS/EPDM/Surlyn/St-Co-DMA反应性共混体系中，反应性聚合物所含的羧酸基团与叔胺基团间存在偶极相互作用。

Then the fiber was transferred to a 4 mL vial which was filled with 100 μL of trifluoroacetic anhydride and stood 30 sec for headspace extraction. Afterward the fiber was transferred again to another blank 4 mL vial and stood 10 min for on-fiber derivatization before the analysis with GC/MS. The absorption-time profiles for both furoic acid and creatinine were examined.

有关尿中肌酸酐的量测，首先亦使用65μm PDMS/DVB纤维，在电磁搅拌转速1200rpm下以直接样本接触方式吸附60秒后，将已吸附肌酸酐的纤维挪至装有100μL无水三氟醋酸的4mL样本瓶中顶空吸附30 sec，再将纤维挪至另一个空白的样本瓶并静置10min（以利衍生物trifluoroacetamide的生成），最后再以气相层析质谱仪进行分析。

The diisoamyl glutarate in catalysis of silicotungsticacid was preparated by esterification of isoamyl alcohol and glutaric anhydride seperated from dicarboxylic acid.

用硅钨杂多酸为催化剂，以从二羧酸中分离出的戊二酸酐和异戊醇为原料合成了戊二酸二异戊酯。

Tert-Butyldimethylsilyloxy) glutaric anhydride, as an important drug intermediate, is synthesized from citric acid by decarboxylation, reduction, hydroxyl protection, esterolysis, cyclization, with the total yield of 30.3%.

介绍了以柠檬酸为起始原料合成3-戊二酸酐的方法。该路线经脱羧反应、加氢还原、羟基保护、酯水解和再闭环，以总收率为30.3%得到目的产物。

The optimum reaction conditions were that the molar ratio of maleic anhydride and p-nitroaniline was 1.2:1, the volume ratio of toluene and DMF was 10:1, the amination temperature was 20~30℃ the cyclization temperature was 145~150℃ and the cyclization time was 6 h over; the amount of p-toluene sulfonic acid was 12% of total reactant mass, the amount of copper sulfate was 0.1~0.5% of total reactant mass, the amount of hydroquinol was 0.1% of total reactant mass.

得到的最佳工艺条件是：n：n为1.2：1，V：V为10：1；胺化反应温度为20~30℃，环化反应温度为140~150℃，环化反应时间为6h以上；对甲基苯磺酸用量为反应物总质量的1%~2%；硫酸铜用量为反应物总质量的0.1%~0.5%；对苯二酚用量为反应物总质量的0.1%。

In 1903, D. Vorlander and co-workers found that treatment of dibenzylideneacetone with concentrated sulfuric acid and acetic anhydride followed by hydrolysis by sodium hydroxide yielded a cyclic ketol, the structure of which was unknown at the time.

1903年，D。 Vorlander和合作者发现，二苄基丙酮与浓硫酸及醋酸酐经过氢氧化钠水解后产生了当时还不知结构的环状酮醇。

The result fights allergic experiment to show, dispel the wind stops land of can different level restrains urticant Ding allergy of akin and passive skin mixes the bandicoot that antiserum causes 2, the sex of small rat late hair of chloric benzene be caused by exceeds 2 nitro- of 4- quick the thymus index that reaction; still can increase small rat when dosage greatly and lienal index; stop urticant experiment shows, dispel the wind stops urticant Ding can reduce the time of fit of small rat itching with dextrose lead anhydride and itching duration apparently, can increase Guinea pig to be able to bear or endure those who suffer phosphoric acid histamine send urticant threshold.

结果抗过敏试验显示，祛风止痒酊能不同程度地抑制抗血清诱发的大鼠同种被动皮肤过敏和2，4-二硝基氯苯所致的小鼠迟发性超敏反应；大剂量时还可增加小鼠的胸腺指数及脾指数；止痒试验显示，祛风止痒酊能明显降低右旋糖酐诱导的小鼠搔痒发作次数及搔痒持续时间，并能增加豚鼠耐受磷酸组胺的致痒阈。

The synthesis of dimethyl fumarate was studied from maleic anhydride and methanol with phospho molybdic acid as the catalyst and bromate as the isomerization catalyst by one-step in this short paper.

采用固体杂多酸磷钼酸为催化剂，溴酸盐为异构化剂，经顺酐一步合成了富马酸二甲酯，探讨了醇酐比、反应时间、催化剂的量、异构化剂的量以及异构化时间对合成DMF收率的影响，并确立了最佳反应条件。

Norbornene-2,3-dicarboxylic acid monomethyl ester was prepared by using 5-norbornene-2,3- anhydride and methanol as raw materials and toluene as solvent.

以5-降冰片烯-2，3-二酸酐和甲醇为原料，正交试验法合成了5-降冰片烯-2，3-二羧酸单甲酯，并对产物结构进行了表征。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。