查询词典 acetonitrile

Its electroosmotic flow property is investigated in a variety of nonaqueous media (methanol, formamide and N, N-dimethylformamide and mixtures of methanol and acetonitrile).

在相同条件下与非涂层毛细管上的分离做了比较。4。利用溶胶凝胶法和化学键合法制备了非高聚物有机磺酸基涂层毛细管。

Methods: It was used with acetonitrile-0.5%phosphoric acid solution(42∶58) as a mobile phase by HPLC. The detecting wavelength was 266nm. The flow rate was 1.0 mLmin^(-1). Results: When Gaoliangjian and Xiangfu are extracted together by alcohol, the content of galangin is the highest.

采用HPLC法，以乙腈-0.5%磷酸(42：58)为流动相，检测波长：266nm，流速：1.0mlmin^(-1)；结果：高良姜与香附的提取方法为乙醇合并提取时，高良姜素的含量高于其他提取方法。

A new process was proposed to get musk ketone and musk xylene from the eutectics by adding acetonitrile and heptane, which was verified by experiments.

提出采用乙腈和庚烷从低共熔组成的酮麝香、二甲苯麝香混合物中得到两种产品的过程，实验结果表明该过程是可行的。

Methods: The chromatographic separation was performed on a Hypersil ODS2 column(250 mm×4.6 mm, 5 μm) with mobile phases of potassium dihydrogen phosphate hexyl amine solution-acetonitrile(74∶26) for the determination of its related substances and methanol-0.05 mol/L potassium dihydrogen phosphate solution(1∶1) for the determination of dexbetamethasone sodium phosphate. The flow rate was 0.8 ml/min, the detection wavelength was 254 nm, the column temperature was 25℃ and the sample size was 20 μl.

色谱柱为Hypersil ODS2柱(250 mm×4.6 mm，5 μm)；有关物质测定的流动相为磷酸二氢钾己胺溶液-乙腈(74∶26)，含量测定的流动相为甲醇-0.05 mol/L磷酸二氢钾溶液(1∶1)；流速为0.8 ml/min，检测波长为254 nm，柱温为25℃，进样量为20 μl。

Hot gases from the neutralizer next are water washed at ambient temperature to absorb acrylonitrile ,acetonitrile hydrogen cyanide and other by products .

热气体从中和剂明年是水清洗常温吸收丙烯腈，乙腈氰化氢和其他的产品。

Was packed electrokinetically and the separation performance of basic compounds was investigated in the pressurized capillary electrochromatography system using 1 μm nonporous bare silica spheres as stationary phase and acetonitrile-water as mobile phase. The effects of the composition of the mobile phase, the concentration of the buffer, pH value, applied voltage and so on on the separation performance were investigated.

以乙腈-水体系作为流动相，详细考察了碱性化合物在该色谱柱上的加压电色谱分离性能，讨论了流动相比例、缓冲液浓度、pH值及操作电压等因素对分离的影响。

The Pictet-Spengler reaction of D-tryptophan methyl ester hydrochloride II-42 with piperonal II-34 in various solvents was extensively studied. The best stereoselectivity (cis/trans=99:1) was obtained using nitromethane or acetonitrile as the solvent.

我们研究了在不同溶剂中，D-色氨酸甲酯盐酸盐II-42和胡椒醛II-34发生的Pictet-Spengler反应的立体选择性，发现当分别用硝基甲烷和乙腈做溶剂时反应的立体选择性达到最高， cis：trans的比例为99： 1。

The effect of various solvents such as water, ethanol and acetonitrile on the title reaction was assessed by the polarizable continuum model.

采用自洽反应场极化连续模型研究了反应体系在水、乙醇和乙腈溶液中反应的溶剂化效应。

The solvent effects were studied with the conductor-like polarizable continuum model respectively in the solvents acetonitrile and water, and we found that the solvent effects reduce the activation energy, but the reduction is small, these reactions are not sensitive to the solvent polarity.

采用导电极化连续介质模型分别研究了在乙腈与水溶液中反应的溶剂化效应，发现这些溶剂可降低反应的活化能，但降低的程度比较小，反应速率变化不大。

The better labeling conditions are as follows:dry acetonitrile as solvent, the mole ratio of K/222 to K 2CO 3 is 1∶1, reaction time is 5 min at 80 ℃. The radiochemical yield is about 57% which is about 3 times higher than the published data.

得出较佳标记条件：以无水乙腈为溶剂，K/ 2 2 2与K2 CO3 摩尔比为1，80℃下反应 5min ，标记率为 5 7%，比文献值提高了 3倍以上。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。