查询词典 acetonitrile

Methods: The sample that pass through handled to be abstracted twice by acetonitrile, evaporate the organic phase to dryness following defecated through the Na2SO4, cleaned-up by norm alhexalle, then analysed by HPLC (C18 column) with a gradient system of methanol-water as a mobile phase.

经处理过的样品用乙腈提取两次，将乙腈过无水硫酸钠层后挥千乙腈，正己烷洗涤净化，经过净化后进行高效液相色谱仪测定（C18柱），本方法以甲醇、水为流动相梯度洗脱，柱温35℃，在波长275 nm处测定。

The sample was extracted by acetonitrile plus water, degreased by n-hexane, and purified by adsorption.

样品用乙腈水提取，正己烷除脂，提取液经液液萃取和反萃取，电子捕获检测器检测，外标法定量。

Another system employs acetonitrile electrolyte with an activated carbon doublelayer storage electrode coupled with a graphitic carbon that intercalates Li ions.

另外一个体系采用乙腈电解质和活性炭双电层储能电极但是采用石墨电极来作为嵌锂电极。

For the determination of five carbamate pesticide residues by high performance liquid chromatography with gel permeation chromatography purification, sample was extracted with acetonitrile and purified with gel permeation chromatography. Methanol-water was used as the mobile phase by gradient elution, flow rate of 1.0mL/min, using a fluorescence detector and quantitating with external standard method.

凝胶渗透色谱-液相色谱法测定5种氨基甲酸酯类农药残留中，实验采用乙腈提取，凝胶渗透色谱柱对样品进行净化，以甲醇-水为流动相，进行梯度洗脱，流速1.0mL／min，荧光检测器检测，外标定量测定。

The extract was dried under nitrogen stream, redissolved in the mobile phase and defatted with n-hexane saturated by acetonitrile.

利用超高压液相色谱－电喷雾串联四极杆质谱联用技术，建立了一种能在10 min内快速分离和测定牛奶中24种磺胺类药物残留的方法。

The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water（10∶60∶30）（including 0.14%n-butyamine 0.1%acetic acid）at a flow rate of 1 mL*min-1 and detected at 220 nm during 1～7 min and at 273 nm during 7～16 min.

氮气吹干有机层，残留物用流动相重新溶解后，用Hypersil BDS C18柱分析，流动相为乙腈-甲醇-水(10∶60∶30)，内含正丁胺0.14%和冰醋酸0.1%，流速为1 mL*min-1，检测波长：1～7 min用220 nm，7～16 min用273 nm。

The combined extract was concentrated to dryness and redissolved in acetonitrile, then cleaned up by dispersive solid-phase extraction with sorbents of N-propyl ethylene diamine, graphited carbon black, and C18, and determined and confirmed by GC-NCI/MS.

样品经乙腈提取并浓缩后加入N-丙基乙二胺、石墨化碳黑和C183种填料进行分散固相萃取净化，气相色谱-负化学离子源质谱分时段选择离子监测技术测定与确证，外标法定量。

The sample was redissolved in the acetonitrilved in the acetonitrile-water (3:2, v/v), then analyzed using LC-MS/MS in multiple reaction monitoring mode via positive electrospray ionization with an Agilent ZORBAX SB-C18 column as the analytical column.

样品用1%醋酸乙腈溶液萃取，经Waters Sep-Pak Vac固相萃取柱净化，乙腈－甲苯（体积比为3：1）洗脱，旋转蒸发浓缩，用乙腈－水（体积比为3：2）溶解，以Agilent ZORBAX SB-C18色谱柱分离，以电喷雾电离串联质谱在正离子多反应监测模式下进行测定。

Samples were saponified with 20 g/L sodium hydroxide. The sexual hormones were then extracted with dichloromethane-acetic acetate (40∶1, v/v) under acidic conditions (pH 3, adjusted with 1 mol/L HCl ). An XTerraTMRP18 column was employed and a mixture of water-methanol-acetonitrile (50∶32∶18, v/v) was used as mobile phase. The seven sexual hormones were detected at 230 nm. The average spiked recoveries for the seven sexual hormones ranged from 75.6% to 97.8% with relative standard deviations of 1.9% to 7.2%. The linear ranges of determination were from 5 to 50 mg/L with correlation coefficients of 0.9999, and the limits of detection were from 3.7 to 12 ng.

先在试样中加入20 g/L氢氧化钠溶液与油脂进行皂化反应，然后用二氯甲烷-乙酸乙酯(体积比为40∶1)混合液在酸性条件下(pH 3)萃取，选择XTerraTMRP18色谱柱，以水-甲醇-乙腈(体积比为50∶32∶18)混合液为流动相，在波长230 nm处检测。7种性激素分离良好并排除了样品中杂质峰的干扰，低、高浓度平均回收率范围为75.6%~97.8%；相对标准偏差为1.9%~7.2%；检出限为3.7~12 ng。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂，与毛蚶抗贫血口服液中的氨基酸柱前定量衍生，用WatersHPLC仪，AccQ-TagTM专用C18柱(3.9mm×15cm)，以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A，乙腈为溶剂B，超纯水为溶剂C，进行梯度洗脱，检测波长为248nm，35min测试完毕。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。