查询词典 acetonitrile

Lycorine, lycoramine and galanthamine in Lycoris radiata were microwave-assisted extracted and determined by HPLC using triethylamine aqueous solution (pH9.00)-acetonitrile-methanol as the mobile phase.

采用微波辅助提取法提取石蒜中的石蒜碱、力可拉敏和加兰他敏生物碱，建立了微波辅助提取／HPLC测定石蒜中这3种生物碱的分析方法。

Previously,these reactions were performed in dry acetonitrile which was manipulatively complex and environmentally unfriendly.

以前报道的此类反应，都是在有毒的有机溶剂，如乙腈中进行的，而且需要加入分子筛以除去反应体系中的水。

F. Nees and their metabolites by HPLC, the mobile phase was acetonitrile-water (0.1% methanoic acid) for gradient elution, Column temperature was 25℃, flow rate was 1.0mL/min, the detection wavelength was at 254nm..

采用HPLC对穿心莲及其代谢产物进行研究，以乙腈-0.1%甲酸水进行梯度洗脱，柱温为25℃，流速为1.0mL/min，检测波长为254nm。

Methods A LiChrospher RP-C_(18)(250 mm×4.6 mm,i.d.5μm)column was used and the mobile phase was acetonitrile-water (1.0% methanoic acid)for gradient elution.

采用LiChrospher RP- C_(18)(250mm×4.6mm，i.d.5μm)色谱柱，以乙腈-水(1.0%甲酸)为流动相，梯度洗脱，双波长检测。

Using UPLC system,WATERS ACQUITY UPLC BEH C~(18)(2.1 mm×50 mm,1.7μm) column and the mobile phase of 1% methanoic acid solution-acetonitrile with the flow rate of 0.6 mL·min~(-1),the determination wavele...

使用 UPLC 色谱系统，BEH C~(18)色谱柱(2.1mm×50mm，1.7μm)；流动相为1%甲酸溶液—乙腈；流速为0.6mL·min~(-1)；检测波长为280nm。

The separation was achieved within 4 min using a BEH Shield RP18 column (100 mm 2.1 mm, 1.7 μm) with 50 mmol/L monoammonium phosphate solution (pH 6.5) and acetonitrile as the mobile phase.

以BEH Shield RP18柱(100 mm 2.1 mm，1.7 μm)为分析柱，以50 mmol/L的磷酸二氢铵(pH 6.5)和乙腈为流动相进行梯度洗脱，3种磷酸腺苷在4 min内实现了较好的分离。

The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱，以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相，流速1ml/min，检测波长210nm，柱温40℃。

Methods Using Diamonsil ODS1 C18 Column, acetonitrile- 0.033mol/L Potassium Phosphate Monobasic acid(35:65) as the mobile phase,detection wavelength as 265nm and flow rate was 1.0ml/min.

HPLC用外标一点法，Diamonsil ODS1 C18柱，乙腈- 0.033mol/L磷酸二氢钾溶液(35：65)为流动相，流速为1.0ml/min，λ=265nm。

The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱，以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相，流速1ml/min，检测波长210nm，柱温40℃。结果阿奇霉素的线性范围为50.3～1006μg/ml，平均回收率100.1%，r=1.0000，RSD=0.8%(n=9)。

Hypersil of ODS-C18 was used with acetonitrile-0.01mol/L monobasic potassium phosphate-triethylamine phosphoric acid8:92:0.4:0.3） as mobile phase.

色谱柱：依利特 Hypersil ODS柱4.6 mm×250mm，5μm），流动相：乙腈-0.01mol/L磷酸二氢钾溶液－三乙胺－磷酸（8 ： 92 ： 0.4 ： 0.3）。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。