查询词典 acetone

Chemiluminescent immunoassay is one of the advanced immunoassay ofnon-radioisotopic immunoassay because of its high sensitivity, wide dynamic range,high accuracy, stable labeled protein, full automation and extensive application field.CLIA using acridinium ester derivatives as chemiluminescent label has advantages oflow background, high signal-to-noise ratio, no need of catalyst and simpleluminescence system. Different aspects associating the DMAE·NHS-based CLIA were studied in thisthesis, including synthesis of acridinium ester, chemiluminescentcharacteristics of DMAE·NHS, labelling antibody or streptavidin with DMAE·NHS,two-site sandwich chemiluminescent immunoassay for TSH, two-sitesandwich chemiluminescent immunoassay involved biotin-streptavidinsystem for TSH, and competitive chemiluminescent immunoassay usingbiotin-streptavidin system for TT〓. The desired acridinium ester, DMAE·NHS, was synthesized according to thereference method with some modifications. The products were identified by IR, NMR,MS and elemental analysis. In our method, KOH was used in place of NaOH tosynthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate waspurified on a silica gel column with chloroform/ethylacetate(4:1, v/v) as eluent andfurther purified by triturating with hexane/acetone(2:1, v/v).

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-二甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿／乙酸乙酯(4∶1，V∶V)作溶剂和淋洗剂，第二次柱层析用己烷／丙酮(2∶1，V∶V)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷／丙酮(2∶1，V∶V)进行研磨，过滤，洗涤，除去溶于己烷／丙酮(2∶1，V∶V)的部分，得到所需要的产品。

The results of analysis have indicated that, in comparison with the direct dehydrogenation reaction, the coverage of alkoxide is decreased with the increase of the adsorption of acetone.

在直接脱氢反应动力学分析的基础上，将这一方法扩展到更为复杂的氧化脱氢反应中，采用如下的机理对担载银催化剂上异丙醇氧化反应动力学进行了拟合分析。

The result indicated that the reacting mixture containing dioxane 11.3mL/g HDCA which had been added ethyl chloroformate drop wise should be keep at 10℃ for 30min, then, rising to 15℃ for another 20min in the step of forming mixed anhydride ,and 1.5mol/L NaOH was used to dissolve taurine before aminolysis, and crude product was recrystalled by acetone in purifying process.

结果表明，形成混酐时，二氧六环用量为11.3ml/g HDCA，滴加氯甲酸乙酯后先在10℃反应30min，再在15℃下反应20min；用1.5mol/L的NaOH水溶液溶解牛磺酸后再进行氨解；粗产品用丙酮重结晶。

Caffeic acid tetramers was extracted and separated from acetone water extraction of Arnebia echroma.

目的从新疆软紫草的丙酮水提取物中分离制备了咖啡酸四聚体对照品。

The hydroxyl and carboxyl, belonging to auxochromic groups, were oxidized into the carbonyl and ester groups, belonging to chromophoric groups, during inducing discoloration under the pretreatment conditions, which makes the wood color deeper. There were plenty of auxochromic groups and chromophoric groups in the acetone extractives of silver chain. The interaction between the auxochromic groups and the chromophoric groups made the wood color deeper.

结论］羟基、羧基等助色基团在预处理条件下氧化成羰基、酯基等发色基团，使木材的颜色加深；刺槐木材丙酮抽出物的主要成分中含有大量发色基团和助色基团，这些基团间的相互作用使木材颜色加深。

Compared with the absorption positions of chlorophyll in acetone, a bathochromic shift was observed at the absorption peaks of chlorophyll in DMF and DMSO.

与叶绿素在丙酮溶剂中的光谱特性吸收峰位置相比较，叶绿素的光谱特性吸收峰在DMF与DMSO两种溶剂中显现了向红位移。

Chapter 4: Synthesis of 1,5-diary 1-1,4-pentadien-3-ones from acetone or benzalacetone with aromatic aldehydes results in 86-97% yield with potassium hydroxide as catalyst under ultrasound irradiation in 5-60min.

为合成氰基环己醇找到一条方便高效的合成方法。第四章：研究了超声辐射下，以氢氧化钾为催化剂，芳香醛与丙酮及亚苄基丙酮之间反应合成1，5-双苄基-1，4-戊二烯-3-酮。

This paper studies that TLC technology is applied to synthesis of benzylidene acetone .

将薄层色谱技术应用于苄叉丙酮的合成实验，通过薄层色谱对合成反应过程的监控，增加了实验的探究性，提高了学生分析问题、解决问题的能力

Test of electrochemical methods Benzylidene acetone, formaldehyde, compound additive D, ammonium metavanadate solution of acid sulfate tin polarization curves, test ammonium metavanadate on the open circuit potential acid sulfate solution of tin.

用电化学工作站测试分析苄叉丙酮、甲醛、复合添加剂D、偏钒酸铵对酸性硫酸盐镀锡溶液的极化曲线的影响，测试偏钒酸铵对酸性硫酸盐镀锡溶液开路电位的影响。

The results showed that in acetone and ethanol, solubilities of 3, 28-di-O-glutaryl-betulin were 33.52 and 22.65 times of those of betulin respectively; In water, solubility of 3, 28-di-O-glutaryl-betulin was 0.0021 g (100 mL water), and in PBS, solubility of 3, 28-di-O-glutary-betulin was 0.0015 g (100 mL PBS), the hydrophilicity of 3, 28-di-O-glutaryl-betulin was significantly increase.

结果表明，在丙酮和无水乙醇中，桦木酐戊二酸酯的溶解度是桦木醇的33.52和22.65倍；在水中，桦木醇戊二酸酯的溶解度为0.0021g（100mL水）；在PBS中，桦木醇戊二酸酯的溶解度约为0.0015g(100mL PBS)，目标产物的亲水性有了显著的改善。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。