查询词典 a column of water

For determination the content of isomaltooligosaccharide in beverage, a high performance liquid chromatography method was established by using 300 mm×4 6 mm, 5 μm Hypersil NH 2 column, acetonitrile+water=78+22 as mobile phase, detector was diffeential refractometer with 40℃ internal temprature.

为测定饮料中异麦芽低聚糖的含量，建立了使用 30 0mm× 4 6mm ，5 μmHypersil NH2 柱，乙腈+水=78+ 2 2为流动相，内部温度为 4 0℃的示差检测器的高效液相色谱法。

The whole analysis was completed on a C〓 column in 18min at a flow rate of 0.5 ml/min, with the mobile phase of methanol-water (93: 7, v: v) containing 75 mmol/L TEOLA and 200 mmol/L HAc, or with the mobile phase of ethanol-water (90: 10, v: v) containing 25 mmol/L TEOLA and 200mmol/L HAc pumped at 0.25ml/min. Compared with the methanol system, the ethanol system was a better candidate for the separation of thulium porphyrin complexes in view of selectivity.

在C〓分析柱（5μm，2.5×150mm）上，流动相为：甲醇：水＝93：7（v/v内含75mmol/L三乙醇胺和200mmol/LHAc），流速为0.5ml/min和流动相为：乙醇：水＝90：10（v/v，内含25mmol/L三乙醇胺和200mmol/L HAc），流速为0.25ml/min，均能使六个铥卟啉配合物在18min内得到有效的分离，相比之下，乙醇体系对铥卟啉配合物更具有分离选择性。

A determination method of ursolic acid in Callicarpa macrophylla Vahl leaves by reversed- phase high performance liquid chromtograph was established. The chromatographic column (Symmetry Shield RP18), methanol-water mobile phase(88:12, V/V) with 1.0 ml/min flow rate, the detection wavelength (210nm) and the column temperature (25℃) were adopted.

建立反相高效液相色谱测定其含量的方法，色谱柱为Symmetry Shield RP18柱，流动相为甲醇-水（体积比88∶12），流速1.0 ml/min，检测波长210 nm，柱温25℃。

A determination method of ursolic acid in Callicarpa macrophylla Vahl leaves by reversed- phase high performance liquid chromtograph was established. The chromatographic column (Symmetry Shield RP18), methanol-water mobile phase(88:12, V/V) with 1.0 ml/min flow rate, the detection wavelength (210nm) and the column temperature (25℃) were adopted.

建立反相高效液相色谱测定其含量的方法，色谱柱 Symmetry Shield RP18柱，流动相为甲醇-水（体积比88∶12），流速1.0 ml/min，检测波长210 nm，柱温25℃。

Different chromatographic parameters including elution profiles, column temperature were investigated in order to optimize separation conditions of different fatty acid phenacyl ester derivatives. A gradient elution using methanol/acetonitrile (90:10, V/V)-water as mobile phase at 0.35 mL/min, detection wavelength at 246 nm, and column temperature of 35℃ were chosen.

经优化确定以(90：10)-水为流动相梯度洗脱，在检测波长246 nm，柱温35℃，流速0.35 mL/min的色谱条件下，18 min内能完成对13种脂肪酸衍生物的分离检测。

The determination of quercitin was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using methanol-water-phosphoric acid (V:V:V=60.00:40.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 360 nm. The determination of gallic acid was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using acetonitrile-water-phosphoric acid (V:V:V=5.00:95.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 272 nm.

槲皮素的测定条件为：Century SIL C18， BDS(250.0mm×4.6mm， 5μm)色谱柱，流动相为甲醇－水－磷酸（体积比为60.00：40.00：0.02），流速为0.8mLmin^(-1)，检测波长为360nm；没食子酸的测定条件为：Century SIL C18 BDS (250.0mm×4.6mm， 5μm)色谱柱，流动相为乙腈－水－磷酸（体积比为5.00：95.00：0.02），流速为0.80mLmin^(-1)，检测波长为272nm。

The HPLC method has been used to investigate the stability of etimicin in 0.9% sodium chloride, 5% glucose, 10% glucose, compound sodium chloride, glucose sodium chloride and so on. In the experiment, the ODS-C18 column (4.6mm×250mm), mobile phase: methanol/water/acetic acid=80/16/4 (containing heptane sulfonic sodium 0.02mol/L), UV detection with wavelength of 330nm were employed. After integrating each of the menstruums with etimicin, the content and pH value were measured after 1h, 2h, 4h, 6h and 8h at a temperature of 17, 25 and 35℃, respectively.

实验采用HPLC法，以C18柱为色谱柱，CH3OH：H2O：HAc=80：16：4（含0.02mol/L庚烷磺酸钠）为流动相，检测波长330nm；对依替米星在生理盐水，5%葡萄糖，10%葡萄糖，复方氯化钠，葡萄糖氯化钠等溶媒中进行了稳定性研究，在室温(17℃)，25℃，35℃情况下，将依替米星与不同的溶媒配伍后，在1h，2h，4h，6h，8h分别测定它们的含量及pH值。

Sample matrix are discharged by the pre-column. The mobile phases applied consisted of 0.1% HOAc (pH3.0) acetonitrile-water on extraction column with UV detection at 225nm. Then, coupled-column liquid chromatographic methods for the direct analysis of atrazine and simazine in urine was established. As a result, the system showed good chromatographic property in the on-line analysis of atrazine and simazine in urine.

使用该系统对尿中的莠去净和西玛津残留进行了分离分析，以含有0.1%乙酸的酸性水缓冲液对加标尿液中莠去净类化合物保留在预柱上，干扰分析的大分子被排阻而无保留通过，其它干扰分子保留小而通过，再切换六通阀，以乙腈和0.1%乙酸水溶液进行梯度洗脱，进而在下一级ODS分析柱上进行分离（紫外检测225nm），两种除草剂的分离分析取得了良好的定性定量结果

In the first cultivation stage,as relatively high concentration of phosphorus,phosphorus from water column was removed to a certain extent by periphyton.The end of the incubation,as low concentration of phosphorus periphyton releases phosphorus to water column instead of removal phosphorus from water,this may closely relate to the alkaline phosphatase secreted by periphyton in water body.

从培养过程中水体磷的浓度变化来说，培养初期，水体中磷的浓度比较高，附着生物对其有一定的去除作用；培养后期，水柱中磷的浓度比较低，附着生物不但不去除水中的磷，而且还向水柱中释放磷，这可能与附着生物向水体分泌碱性磷酸酶密切相关。

The new process gets the feed to low-pressure column from a side stream of high-pressure column, which balanced better the separation duties of the high- and low-pressure columns and implemented the integration of extracting soft-water.

该流程用加压塔侧线采出作为常压塔进料，更合理地分配了高、低压塔之间的分离负荷，并实现了萃取软水的集成利用。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。