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In addition ,nine new O,O-dialkyl-[α-(1,3,4,6-tetraacetyl-2-deoxy-β-D-glucoamino)-p-methyl benzlidene] phosphonatesand eight O,O-dialkyl-α-(2-deoxy-D-glucoamino)-p-methyl benzylidene phosphonates were prepared. The 〓 and〓 spectra of Ⅰ-Ⅴ compounds indicated clearly that each of Ⅰ-Ⅴ compounds contains two diastereo-isomers.

我们对非对映异构体的分离方法进行了研究，并分离得到了五个单一构型的异构体〓、〓、〓、〓和〓，培养出了〓、〓和〓三个异构体的单晶，通过X-射线衍射分析，确定了〓、〓和〓三个异构体的绝对构型，反应过程中引入的手性原子的构型均为R构型。

Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.

本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法，合成了4种苯并咪唑-2-羧酸衍生物并进行了表征；培养了2个化合物d、e的晶体并测定和讨论了晶体结构；制备了3种未见报道的苯并咪唑金属配合物，对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。

Ausiello: You had me at "pretty." BBT just tape d geek god Stan Lee's guest appearance, so I have lotsa deets from the eppy : In it, Sheldon learns that he was photographed driving Penny to the hospital the night she dislocate d her arm and, thus, has been ticket ed.

答：就冲这个&尊的&，我可以很负责任的告诉你－－这部剧刚刚录完＂宅男之神＂Stan Lee的戏码（介位大神可是奇迹漫画的创始人，美国超级英雄&蜘蛛侠&、&神奇四侠&、&X战警&、&绿巨人&、《钢铁侠》，都是老人家的大作，想象一下四个宅男遇到大神会有多激动吧~）。

0 D; X8 K富阳论坛 Prof Bonthron, Dr Chris Bennett of the Yorkshire Regional Genetics Service and their colleagues studied a group of patients suffering from inherited primary hypertrophic osteoarthropathy, a genetic disorder in which the finger clubbing is accompanied by painful joint enlargement and a thickening of the bone.

Bonthron教授以及约克郡基因所得Chris Bennett博士和他们的同事们研究了一组罹患原发性肥大性骨关节病的病人，这种病是一种发生杵状指并伴随着进行性股关节痛及骨肥厚的遗传病。3 p1 _6 c O k* d： b+ z1 e富阳论坛，富阳新闻，富阳民声，富阳交友，富阳旅游，富阳美食，富阳房产，富阳商贸 B！ j。 A！ S4 z$ X， c5

Guo L X. Studies on robotization to boom system of concrete pump car［D］.

郭立新。泵车布料机构机器人化若干问题的研究［D］。

RESULTS: A germacrane sesquiterpenoid, incaspitolide D (1), along with-N-benzoylphenylalanine--2-benzamido-3-phenyl- propyl ester (2), indole-3-carboxylic acid (3), apigenin (4), diosmetin (5) and luteolin (6) was isolated. CONCLUSION: Compounds 1-5 were isolated for the first time from Vernonia patula.

结果：分离到1个牻牛烷型倍半萜内酯， 1个苯丙氨酸衍生物、1个生物碱和3个黄酮化合物，根据波谱数据和X-衍射分析分别鉴定为：incaspitolide D (1)，-N-苯甲酰基苯基丙氨酸–-2-苯甲酰氨基–3-苯基丙酯(S-N-benzoylalanine-–2-benzamido-3-phenylpropyl ester， 2；吲哚-3-羧酸(indole-3-carboxylic acid， 3)；香叶木素(diosmetin， 4)，芹菜素(apigenin， 5)和木犀草素(luteolin， 6)。

A tomograph that constructs a 3-D model of an object by combining parallel planes.

通过联合平行位面建立物体-d模型的断层 x光摄影术。

G/ l8 F% d!}1 D4 e1 :} Wang, who was blitzed twice by Cleveland in the playoff loss last fall, was shaky in spring training as he developed his slider and changeup. But he was sharp on Tuesday, using the slider for his two strikeouts and his usual sinker for most of the rest.

X， R W ^0 d O' N 去年季后赛被印第安人狂电两次的王小民(看来，这个印象会跟著小民一阵子T__T，春训期间练习滑球和变速球的时候，表现也是抖抖的，但是星期二他运用滑球取得两次三振，以及其余时间运用伸卡球时，表现得很锐利。

X-ray crystal structure analysis for complex 1 reveals that the copper ion is penta-coordinated by a D-and a L-diamine ligand, and two copper ions are bridge-connected by two cyanides from [Fe6](superscript 3-) in axial position.

晶体结构分析表明，化合物1中Cu离子处于五配位的配位环境，分别和1个D-La，1个吞L-La及[Fe6](上标 3-)中的l个氰基配位，2个Cu离子通过[Fe6](上标 3-)桥联。

The results suggested that chitinhad a good solubility in the new solvent when its at -30℃and below, but the solubilityof chitin no longer increasesd notable as the temperature reduced; The joined of urea, incertain degree, strengthened the solvency of alkali solvent to chitin. When theconcentration of sodium hydroxide is 8%～12%, Chitin had a good solubility, and theapparent viscosity of chitin solution could up to 4000 mpa·s～5000mpa·s at roomtemperature; In addition,the solubility of chitin in new solvent was high when therefrigerated time was three days and above, but the refrigerated time could not too long,otherwise, the deacetylize degree of chitin got more bigger. The properties of chitin solution were tested by revolving viscosimeter, FT-IR,X-RD and so on.

结果表明，在-30℃及以下甲壳素能很好的溶解于新溶剂中，但甲壳素的溶解度不再随温度的下降而有所增大，而是基本保持不变；尿素的加入，在一定程度上强化了强碱溶剂对甲壳素的溶解，当新溶剂中NaOH浓度为8％～12％时，甲壳素在试验温度下可以获得较好的溶解度，所得溶液在室温下的表观黏度达4000 mpa·s～5000mp·s；冷冻时间为3 d及以上时，有利于甲壳素的溶解，超过3 d，甲壳素的溶解度变化不大，另外，冷冻条件下，甲壳素在强碱溶剂中仍会发生脱乙酰化反应，冷冻时间不宜太长。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。