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The composition of Fe-Co and Fe-Co-Mn alloy is analyzed by using Electron Probe Micro Analysis and the magnetic properties of porous alumite film in which Fe-Co and Fe-Co-Mn alloy electrodeposited are measured by a Vibrating Sample Magnetometer .

本论文通过使用多种现代测试技术，如：扫描电镜、透射电镜、电子探针X射线能谱、X射线衍射、电子衍射分析和振动样品磁强测试等，对铝阳极氧化膜的形貌、纳米级微孔内Fe—Co和Fe—Co—Mn合金的晶体结构、Fe—Co和Fe—Co—Mn合金在纳米级微孔内的电沉积工艺以及纳米级微孔内Fe—Co和Fe—Co—Mn合金的磁性进行了系统的研究。

Hot corrosion behavior of Na2SO_4 coated B-1900 alloy was studied in air at 827 and 750℃.Corrosion kinetics of the coated alloy was gravimetrically measured,and contents of water soluble ions in the reaction products were chemically analyzed.X-ray diffraction and EMP techniques were employed to determine the components and morphology of the corrosion product scale.

用涂 Na_2SO_4盐膜法研究高温合金 B-1900在827℃和750℃于空气中的热腐蚀行为，测定其腐蚀动力学曲线，用 X -射线衍射和电子探针元素面扫描方法分析腐蚀产物的相组成和成份，还对其中的水溶性离子进行化学定量分析。

The microstructure evolution and composition distribution of the 7A55 cast and homogenized alloy were studied by optical microscopy, scanning electron microcopy, energy dispersive spectrometer, transmission electron microscopy and X-ray diffractometry. The homogenizing and overburnt temperatures of the alloy were determined. Meanwhile, the diffusion kinetics of the alloy elements during homogenizing treatment was investigated and the homogenizing kinetic equation was deduced according to Fick's First Law of diffusion. The diffusion of alloy elements, precipitation of Al3Zr particles and the conglomeration and globe of the insoluble phases were explained by the equation during homogenization.

摘 要：采用光学显微镜、扫描电镜、能谱分析、透射电镜和X射线衍射分析等研究了7A55合金铸态与均匀化显微组织演化与成分分布，确定了该合金的均匀化处理温度与过烧温度，研究了铸锭均匀化动力学过程，利用菲克定理导出了均匀化动力学方程，利用动力学方程对均匀化过程中合金元素的扩散、 Al3Zr的析出、难熔相的聚集和球化现象进行了解释。

Based on the failure analysis of hot roll, this paper optimizedly adjusts alloy system and summarizes the experience of rolling wiresand improves ail processing properties. Then, it analyses the effects on some natural parameters such as alloy transfer coefficient, surfacing layers, welding current and arc voltage etc.. It confirms the fitting ageing technique. Also, it discusses the microscopic structural transformation back and forth ageing and the effects on hardness change of overlaying metal by some alloying elements including C, Cr, V, W, Mo, Ni, Mn, B, Re through OM, SEM and X-ray diffraction analyses. Finally the abrasive resistance, red hardness, thermal fatigue property and anti-high temperature oxidability are investigated in experimentation.

全文在热轧辊失效分析的基础上优化调整合金体系，总结了焊丝轧制的经验，改善各种工艺性能，分析了几个特性参数的影响，确定了适宜的时效工艺，并通过光学显微镜、扫描电镜和X-射线衍射对时效前后的显微组织转变以及部分合金元素如C、Cr、V、W、Mo、Ni、Mn、B、Re对堆焊层硬度变化的影响进行分析，最后通过试验考察了堆焊层金属的耐磨粒磨损性能、红硬性、耐热疲劳性和抗高温氧化性。

La-Mg-Ni system La0.83Mg0.17Ni Mn0.1 (x=3.4, 3.6) hydrogen storage, alloy electrode has been explored. Different time annealing treatment at 1173K has been applied to the alloy. XRD and Rietveld refinement method and Scanning Electron Microscopy analysis showed that the alloy annealed at 1173K for 8h singler type A2B7 and A5B19 phase composition can be obtained.

以La-Mg-Ni系La0.83Mg0.17NiMn0.1(x=3.4， 3.6)为研究对象，合金在1173K进行不同时间退火处理，通过XRD及Rietveld全谱拟合方法和扫描电镜背散射分析表明，在1173K退火8h分别可得到较单一的A2B7与A5B19型相结构合金。

The microstructure of the magnesium alloy before and after ECAP were examined by means of OM and TEM. The hardness of the as-extruded and unextruded Mg-6Zn-1Gd-0.6Zr magnesium alloy was examined by vickers hardness tester. The rolling of the crystal plane in the process of ECAP was analyzed by X-ray diffraction.

采用光学显微镜和透射电子显微镜分析了试样ECAP变形前后的显微组织变化，采用显维硬度计对Mg-6Zn-1Gd-0.6Zr合金ECAP变形前后进行了硬度测试，采用X-射线分析法分析了ECAP变形过程中晶面的转动。

In this thesis, the phase diagram of Zn-Al binary system on 10~69.5 w% was reinvestigated by using differential scanning calorimeter, X-ray diffraction and pushrod dilatometer. The process of isothermal transformation during the aging of high-Aluminum-Zinc-based alloy was studied by using differential scanning calorimetry, and the aging behavior of the alloy was analyzed at the aspect of thermal analysis kinetics. The change of microstructure which the alloy was being heated was observed on high-temperature metallurgical microscope. The microstructure and wear-friction properties were compared among the alloys treated with several different heat treatment processes, and a model for heat treatment processes was proposed based on artificial neural network,so as to predict the relationship between friction coefficient and parameters of aging treatment such as aging temperature and time.

本文采用高温X射线衍射、示差扫描量热分析、热膨胀等方法重新测定含锌量范围为10％～69.5％的Zn-Al系二元相图，利用示差扫描量热分析法，研究高铝锌基合金时效等温转变过程，并从热分析动力学的角度分析高铝锌基合金合金时效行为；使用高温金相显微镜观察合金加热时的组织变化；比较几种不同热处理工艺对高铝锌基合金显微组织与耐磨性能的影响并利用人工神经网络建立高铝锌基合金热处理工艺模型，预测合金摩擦系数随时效温度及时间变化规律。

The tensile properties of under-aged 3J21 alloy at room and low temperatures were studied on a universal tensile teat machine. Moreover, a metallographic microscope and X-ray diffractometer were used to analyze the metallographic structure and physical phase of the alloy in a cold rolled and under-aged state. By employing a transmission electron microscope the structure of the alloy under the above-cited two states was observed and the X-ray diffraction results being verified.

在万能拉伸机上对欠时效态3J21合金室温及低温条件下的拉伸性能进行研究，并采用金相显微镜、X射线衍射仪对冷轧状态和欠时效态的金相组织及物相进行分析，采用TEM观察两种状态的组织和结构，验证了X射线衍射结果。

In order to explore the influence of the bath composition on Ni-W-P alloy coating structure and properties, to find the right ratio, so as to lay the foundation for follow-up experiments, SEM/EDS, X-ray diffraction, and metallographic analysis and other methods were adopted to study the composition and structure of different chemical deposition of Ni-W-P alloy. And the hardness of different components of the sediment layers plated state and the hardness after heat treatment were measured.

为了探索镀液组分对Ni-W-P合金镀层结构与性能的影响规律，寻求合适的镀液配比，为后续实验莫定基础，采用扫描电镜／包谱、X射线衍射以及金相分析等方法，研究了不同成分和结构的化学沉积Ni-W-P合金层，测量了不同成分沉积层的镀态与热处理后的硬度。

In order to disclosure the reason why the electrocatalysis activeness and selectivity droped after being used several hundred hours continuously, the x-ray diffraction, scanning electron microscopy and energy dispersive spectroscope have been used to characterize the surface condition variations of Monel metal. The results indicated: Monel metal belongs to the Cu-Ni alloy around the electrolysis experiment.And after being used for 600hr, the surface layer element composition and geometry distribution of the alloy changed, namely in the alloy the Cu element /which superficial free enthalpy was smaller,"concentrated" to the alloy surface,and formed one kind of marble structure microcrystallite.Thus the electrode surface becamed rough a

为了揭示蒙乃尔合金阴极在连续使用数百个小时后电催化活性剂选择性下降的原因，采用X射线衍射仪、电子扫描电镜和电子能谱分析仪对电解实验所用的蒙乃尔阴极材料在电解实验前后的表面状态进行了表征，结果表明：所使用的蒙乃尔合金阴极材料在电解实验前后均属于Cu-Ni合金，使用600hr后，由于表面层元素组成和几何排布发生了变化，即合金中表面自由焓较小的Cu元素向合金表面&富集&，形成一种大理石结构的微晶，表面粗糙、不均一，这是造成其对硝基苯电还原的催化活性及选择性随着使用时间延长而逐渐下降的主要原因，同时也为此类电极的修饰改进提供了方向。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。