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All the compounds are characterized by IR and elemental analysis.we design and prepare a bipyridinium supramolecular compound and six coordination compounds, which are also characterized by IR, elemental analysis and X-ray structure analysis. According to X-ray structure analysis, hydrogen bonds and n-n stocking interactions participate in the architecture of three-dimensional framework [H2L1 (NO3)2 (H2O)2]n; one-dimensional zigzag coordination polymer [Hgl21.5CH3OH]n; binuclear metallamacrocycle (HgI2L2)2 3H2O; helical double-stranded one-dimensional coordination polymer [Co2(L2)2-2CH3OH]n; double-stranded one-dimensional coordination polymer [Co2(L3)2-CH3OH-CH3CN]n; and three-dimensional compound [Cu(C5H4NCOO)2(H2O)2]-H2O with hydrogen bonds, three-dimensional coordination polymer {[Cd(C5H6NCOO)2H2O]-DMF}n, which are indirectly obtained from the precursor ligand L3 through metal ion induced the hydrolysis of diamide and self-assembled with the hydrolyzate.

我们首次合成了一个双吡啶鎓超分子化合物和六个过渡金属配合物，并通过IR谱，元素分析和X-ray晶体衍射分析对它们进行了表征。X-ray晶体结构分析表明：超分子化合物[H_2L1·(NO_3)_2·(H_2O)_2]_n是由多种氢键和芳香环间的π-π堆积作用构建的三维无限结构；[HgI_2(L1)·1.5CH_3OH]_n是一维锯齿状配位聚合物；(HgI_2L2)_2·3H_2O是双核金属大环化合物；[Co_2(L2)_2·2CH_3OH]_n是具有一维双螺旋结构的配位聚合物；[Co_2(L3)_2·CH_3OH·CH_3CN]_n为一维双链结构的配位聚合物；以及由非直线形配体L3在金属离子Cu和Cd的诱导作用下发生水解，并且金属离子与水解产物——异烟酸根离子自组装，形成了三维氢键超分子化合物[Cu(C_5H_4NCOO)_2(H_2O)_2]·H_2O和三维配位聚合物{[Cd(C_5H_6NCOO)_2H_2O]·DMF}_n。

Furthermore, a strong linear correlation exists between radio-luminosity and γ-ray lurninosity〓 The possible upper limit relation suggests that the contribution to γ-ray background of AGNs may be less than other authors' prediction.

另外，光度——光度之间存在显著的线性相关〓可能的上限关系表明AGNs对γ-ray背景的整体贡献比以前认为的要少。

We find a strong correlation between VLBI core flux and γ-ray flux in EGRET AGNs statistically. This correlation is possibly an upper limit relation.

通过对EGRET AGNs VLBI射电核流量和γ-ray流量的相关性分析，我们得出射电核流量与γ-ray流量间存在一显著相关，这种相关性可能表现为一上限关系。

Since all γ-ray AGNs have strong radio emission, the relationship between γ-ray and radio emission is worthy to study.

由于所有的γ-ray AGNs都具有强的射电辐射，所以人们一直在努力研究γ-ray辐射和射电辐射之间的联系。

As the modern astronomical observational technique with the highest resolution, VLBI can provide key contribution to the study of relativistic jets structure, superluminal motion and bending jet of γ-ray AGNs. It is helpful to discover the relationship between γ-ray and radio emission of them.

VLBI技术是现代天文观测中能获得最高分辨本领的观测手段，利用VLBI技术对γ-ray AGNs的相对论射电喷流结构、视超光速运动和喷流的弯曲进行研究，将有助于我们探索该类源的γ-ray和射电辐射的关系。

The X-Ray is vacuum bagged in ?berglass and infusion-molded in kevlar/carbon with fibreglass/vinylester deck. Equipped as standard with a deep retractable skeg, The X-Ray is available with an optional ingenious retractable rudder and an optional day hatch.

X-Ray 是用袋子抽真空，并通过玻璃纤维/乙烯基塑料甲板，向模具中注入凯夫拉尔合成纤维/碳， X-Ray 可选择性配置灵巧的可收回的舵，以及可选择的仓口。

The biomechanical tests showed that two kinds of artificial bones had not significant difference on compressive strength and Young\'s modulus(P＞0.05),while the flexural strength of nano-nacre artificial bone was less than the control group(P＜0.05).3.The results of CCK-8 showed that the difference were not significant in each group,the proliferation of osteoblast reached the peak at the 5th day;7 days after being co-cultured,the total protein content of study group was higher than control group and blank group(P＜0.05),while the difference between control group and blank group was not significantP＞0.05The difference of alkaline phosphatase activities among three groups was not significant(P＞0.05The SEM view showed that osteoblast attached and grew well in two kinds of artificial bone.4.X-ray photography showed that two kinds of powder started to degrade in 2 weeks;this phenomenon became more appear in 4 weeks,nano-nacre powder degraded faster than micron-nacre powder,while the hole shadow was easy to be found;in 8 weeks,all the femoral holes recovered and returned to normal bone mineral density in all groups.Analysis of tetracycline fluorescent double marks in the hard tissue grinding slices indicated that new bone grew fastest around the bone defect area in study group,while most slowly in blank groupP＜0.05 SEM(scanning electron microscope observation showed that nano-nacre powder degraded more quickly.The same result can be found through the demineralized sections morphometric analysis,and both of the composite artificial bones made from those two kinds of nacre powder had the good connection with the adjacent tissue in rats body without apparent inflammatory response.5.X-ray photography showed that rabbit\'s bone defects healed faster in study group since NNAB implanted than in control group since MNAB implanted.At 24 weeks after operation,bone density in radial defects had nearly accessed to the normal area,while lower in control group,and turned up nonunion in blank group;The checking of BMD showed that results in study group were higher than those in control group at 8,16 and 24 week(P＜0.05), and the difference between the BMD values in study group at 24 week and those in blank group was not significant(P＞0.05).The gross specimens showed satisfactory histocompatibility both in study group and in control group,with bone tissue growing from two sides into the center of implanted materials; Normal slices in HE stain and hard tissue grinding slices in Stevenel\'s blue/Van Geison\'s picro-fuchsin stain showed that the bone growth tendency was better in study group than that in control group,and the medullary cavity had been penetrated to the implanted materials in study group at 24 week;Analysis of tetracycline fluorescent double marks in the hard tissue grinding slices indicated that new bone in both groups grew fastest 8 weeks after surgery,while slow down at 16 week.

纳米珍珠层/消旋聚乳酸复合人工骨与微米珍珠层/消旋聚乳酸复合人工骨分别与成骨细胞共培养后，其各时间点CCK-8法检测值与空白对照无显著差异(P＞0.05)，成骨细胞均在第5天达到增殖高峰期；培养7天后，实验组细胞蛋白含量高于对照组及空白组(P＜0.05)，后两者之间则无显著差异P＞0.05碱性磷酸酶活性在三组间均无显著差异(P＞0.05电镜下可见成骨细胞在两种人工骨上都有良好生长贴附能力。4.X-ray显示两种粉体在大鼠股骨骨洞植入第2周时都开始出现了降解，第4周时更为明显，纳米珍珠层粉较之微米珍珠层粉降解更快，而空白对照组骨洞阴影仍可见，至8周时，则所有组骨洞均己闭合修复，X-ray下已不可见原钻孔痕迹，恢复正常骨质密度；硬组织磨片四环素荧光双标记结果显示纳米珍珠层粉植入组较其余两组在骨缺损区周围新骨生长速度更快，空白组速度最慢P＜0.05电镜观察及常规脱钙切片亦可见到纳米粉体降解较快；由以上两种原材料制得的纳米珍珠层/消旋聚乳酸复合人工骨与微米珍珠层/消旋聚乳酸复合人工骨在大鼠体内均与周围组织结合良好，无明显炎症反应。5.X-ray显示纳米珍珠层/消旋聚乳酸复合人工骨植入兔桡骨缺损区后其骨愈合速度较对照组微米珍珠层/消旋聚乳酸复合人工骨植入的快，至植入术后24周，实验组骨缺损区接近正常骨密度，对照组骨缺损区密度较低，空白组则呈现骨不连状态；骨密度测量结果显示术后8周、16周、24周实验组的骨密度值高于对照组(P＜0.05，24周实验组的骨密度值与术前所测得的正常值无显著性差异P＞0.05动物取材大体所见均显示组织相容性良好，骨组织逐渐由植入材料两端向中央生长；常规切片HE染色及硬组织磨片Stevenel\'s blue/Van Geison\'s picro-fuchsin联合染色均可见实验组骨缺损区长势优于对照组，至术后24周，实验组骨髓腔与材料已呈相交通状；硬组织磨片荧光显微镜下观察，两组材料在术后8周处于骨生长最快速时期，16周时速度开始减慢，术后4、8、16周时实验组的新骨生长速度均较对照组的快

Millisecond time scales in the X-ray light curve of Scorpius X-1. The estimated sizes of these occulting TNOs are about or less than 100 m. This is the first time that TNOs of such a small size are detected. Our discovery of the X-ray occultation demonstrates a new method to study smaller TNOs.

所以，我们在这里介绍了我们利用X-ray波段的掩星方法，藉由利用RXTE卫星观测天蝎座X-1的数据，在毫秒尺度找到了一些可能的X-ray掩星事件，而这方法将可让我们了解一些大小在100公尺左右或更小的物体的分布情形，而这也是我们第一次在X-ray波段所发现掩星事件，而这方法的持续研究将能让我们对於太阳系的形成会有更多的帮助，因次在此提出来和大家分享。

Co-firing characteristics of corn stalk and stone coal in different proportion were investigated by thermal gravimetric analysis. The results showed that corn stalk can improve the ignition and combustion of stone coal. The agglomeration experiments on corn stalk were made in a bench-scale bubbling fluidized bed with quartz sand as bed material and stone coal ash as additive. The results indicate that stone coal ash can inhibit agglomeration of bed material particles at temperature of 900℃. Agglomerate of blends was analyzed by means of scanning electron microscopy, energy-dispersive X-ray, and the bed materials were analyzed by means of X-ray fluorescence. Analysis showed that aluminum element and iron element in stone coal ash can react with alkali compounds and eutectics with low melting point, form a covering layer with high melting point on the surface of biomass and quart sand particles, thus inhibit the forming and transfer of low melting compounds.

以玉米秸秆与石煤按不同比例组成的混合物为研究对象，在TG-DTG热分析仪上进行了燃烧特性分析，结果表明玉米秸秆有利于石煤的着火和稳定燃烧，对石煤有一定的助燃作用；在小型鼓泡流化床实验装置上，以石英砂为床料、石煤灰为添加剂，进行了玉米秸秆成型燃料流化床燃烧的床料黏结实验，结果表明：石煤灰能够在生物质流态化燃烧过程中有效地抑制流化床床料黏结现象的发生；通过对实验中形成的结团进行扫描电子显微镜X射线能谱(scanning electron microscopy/Energy-dispersive X-ray- SEM/EDX)，对床料进行X射线荧光光谱(X-ray fluorescence，XRF)分析，结果表明石煤灰中的Al和Fe能够与生物质灰中的碱金属化合物以及低熔点共熔物发生化学反应生成高熔点物质，并且覆盖在生物质碳颗粒与石英砂颗粒表面形成隔绝层，从而阻止低熔点物质的生成与迁移。

The author prepared bulk SmBaCuO single crystals with 5×5×5mm〓 by MTG method. The SmBaCuO crystals were proved by X-ray diffraction and X-ray back-reflection Laue technique. SmBaCuO crytal became 90K zero resistance superconductor by the study of the relation of transition temperatures and heat treatment conditions.

采用MTG法及其它类似的方法制备的YBCO超导体的小样品具有很好的超导电性能，但要使YBCO超导体获得实际应用，必须制备超导电性能优异的大块YBCO超导材料，采用籽晶诱导技术是制备高性能大块YBCO超导体的有效方法，因此，制备较大尺寸高质量的〓〓单晶是籽晶诱导技术成败的关键，作者用MTG工艺制备了尺寸达5×5×5mm〓的大块〓单晶，X-ray衍射及X-ray劳埃像法证明MTG法制备的〓晶体具有很好的单晶特性。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了