查询词典 N-phenylaniline

Naphthalene acetyl chloride was prepared firstly by the reaction betweenα-naphthylacetic acid and SOCl2 in anhydrous benzene, then reacted with potassium thiocyanate to obtainα-naphthalene acetyl isosulfocyanate, as taking an addition reaction with p-chloro benzoyl hydrazine the novel compound N-naphthalene acetyl-N'-p-chloro benzoylamino thiocarbamide was finally synthesized.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯，然后与硫氰酸钾反应生成α-萘乙酸基异硫氰酸酯，再与对氯苯甲酰肼进行加成反应，生成新型化合物N-萘乙酰基－N'-对氯苯甲酰氨基硫脲。

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酸为原料，经盐酸化、氯代等反应合成了Z-2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酰氯盐酸盐；氯代时以用亚硫酰氯和N，N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂，并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下，以异丙醇作溶剂，苯硒酚与化合物2不反应。在氢氧化钾存在下，以异丙醇／水作溶剂（体积比20：1，在室温下，硒酚可以有效地进攻中化合物2中1，3，2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件，顺利实现了硒酚对N^1-（2-呋喃基）-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环，生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

Themethod combines the deterministic optimization technique with the orthogonaloptimal experiment method to change the 2￣n vertices of the tolerance region into(n+1)constraint conditions,and uses nondifferent...

该方法应用确定性方法和正交最优化方法相结合，将容差域的2￣n个顶点离散为n＋1个约束条件，并利用不可微规划直接得到DCTT问题的最优解。

It is proved that any n-dimensional(n≥4)compact manifold with totally geodesic boundary which satisfies a pinching condition can be deformed to a space form with totally geodesic boundary.

证明了对于任意一个具有全测地边界的n维紧致流形(n≥4)满足一定的拼挤条件可以形变为具有全测地边界的空间形式。

The different factors'n (V / n molar ratio, precipitation pH and calcination temperature effects on the characterization of FeVO4 were discussed and the optimum preparation conditions of triclinic FeVO4 was concluded.

以硝酸铁和偏钒酸铵为原料，在不同n/n摩尔比，不同pH值和不同温度条件下制备了系列样品，优化了三斜型FeVO4的工艺制备条件。

Treatment of N-p-tolylsulfonylindole 1 with acetyl chloride in dried dichloromethane gave the title compound, N-p-tolylsulfonyl-3-acetyl-indole 2 C17H15NO3S, M(subscript r=313.36 in 89% yield. Single-crystal structure of 2 was determined by X-ray crystallography.2 crystallizes in the triclinic system, space group P-1 with a=10.0264(13), b=12.5913(16), c=14.1621(18)?

N-对－甲苯磺酰－吲哚(1)在二氯甲烷中与乙酰基氯反应得到产率为89%的N-对－甲苯磺酰－3-乙酰基－吲哚(2)（分子式：C17H15NO3S，分子量：313.36），用单晶X-射线衍射方法测定了2的晶体结构并表明：属三斜晶系，空间群为P-1，单胞参数为a=10.0264(13)，b=12.5913(16)，c=14.1621(18)？

Trivial Solution conception is put forwarded based on the theorem of K〓nig and forbidden node----for the n×n 0-1 degeneracy matrix, the solution under the condition that all element 1 can not be covered completely by n lines that must have intersects or can be covered completely by n lines that must have cross, without forbidden node, are called TS matrix.

本文在K〓nig定理和禁点定理的基础上，提出了平凡解的概念，即对于n×n阶的退化矩阵，全部1元素不可能被n条有交叉的直线全部覆盖或能用n条直线覆盖全部1元素，但无禁点的情况称为平凡解。并证明了如下的平凡解产生的充分必要条件：对退化矩阵A〓，若

When u lost the R'n'R password, simply uninstall R'n'R and reinstall it.

当u失去了r'n'r密码，只需卸载r'n'r并重新安装它。

Results The identification method for ursolic acid was established; The calibration curves of unarm showed a good linearity in the range of 0.0448-0.448 μg (r=0.9999, n=6), the average recovery was 99.7%(n=6), with RSD of 1.2%.

结果 夏枯草的薄层鉴别方法快速、灵敏，阴性无干扰；蒙花苷在0.044 8~0.448 μg范围内呈良好线性(r=0.999 9， n=5)，平均回收率为99.7%(n=6)，RSD为1.2%。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。