查询词典 N-phenylaniline

Excitations from localized states to the conduction band account for the absorption edge shift toward lower energies observed in the case of N/TiO_2 with respect to pure TiO_2.Mixture of visible light absorption of nitrogen doping and oxygen defect gave no obvious onset in the whole range between 400 and 800nm were observed of the samples N/TiO_(2-)A and N/TiO_(2-)M.

UV-VIS-DRS分析掺杂N/TiO_2结果表明，N/TiO_2-H和N/TiO_2-T两种催化剂在490nm处有吸收带边，可见光激发途径是掺杂的N以填隙方式形成的杂质能级吸收电子发生的跃迁引起的；而N/TiO_2-A和N/TiO_2-M两种方法得到的N/TiO_2在整个可见光区域内具有可见光吸收，没有显著的可见光吸收带边，其对可见光的激发途径是掺杂N和氧空缺共同作用的结果。

Results show that 4-oxo-β-ionone is the major product with yield of 53.5% under the conditions as follows: reaction temperature 45℃, reaction time 24 h, the molar ratio of n: n(NaClO3): n 20: 100: 3, and pH value of solution in 1-3; on the other hand, 5,6-epoxy-β-ionone is major product with yield of 25.4% when reaction temperature is 40℃, reaction time is 24 h, the molar ratio of n: n(NaClO3): n is 20: 120: 5, and pH values of solution is 3. The excessive β-ionone can be recovered by vacuum distillation for reusing again. 4-oxo-β-ionone and 5,6-epoxy-3-ionone were purified by recrystallization and silica gel column chromatograph respectively with the purity over 98%.

研究结果表明：氯酸钠氧化β-紫罗兰酮的反应主要生成4-氧代－β-紫罗兰酮和5，6-环氧－β-紫罗兰酮，经重结晶和硅胶柱层析分离，纯度高于98%；4-氧代－β-紫罗兰酮的有利合成条件是反应温度为45℃，反应时间为24h，溶液的pH值为1~3，反应物配比n：n(NaClO3)：n为20：100：3，最佳收率为53.5%；5，6-环氧－β-紫罗兰酮有利的合成条件是反应温度为40℃，反应时间为24h，溶液的pH值为3，反应物配比n：n(NaClO3)：n为20：120：5，其收率为25.4%；未反应的β-紫罗兰酮经减压蒸馏回收后可重复使用。

A process for reducing nitryl with unstable guanyl on para-position of benzene ring into azyl features that active metal reacts on organic acid and solvent at ordinary temp. and pressure to reduce N-(2 or 3-M, 5 or 6-M',4-nitrophenyl)-N',N'-dimethyl acetamidine into N-(2 or 3-m, 5 or 6-M', 4-aminophenyl)-N',N'-dimethyl acetamidine, where M=H,-R,-OR,-COOR (R=H, C1-C6); and M'=H,-R,-OR,-COOR (R=H, C1-C6). Its advantages include reduced by-reaction and high reducting rate up to 80%-95%.

本发明是将苯环上对位带有不稳定脒基的硝基还原为氨基的方法，采用活泼金属，如：锌或锡，与有机酸和适当的溶剂，在常温、常压下发生反应，将N－（2或3－M，5或6－M＇，4－硝基苯基）－N＇，N＇－二甲基乙脒还原为N－（2或3－M，5或6－M＇，4－氨基苯基）－N＇，N＇－二甲基乙脒，其中M＝H，－R，－OR，－COOR（R＝H，C1－C6），M＇＝H，－R，－OR，－COOR（R＝H，C1－C6），减少了副反应，使还原收率达到80％以上，最高可达95％以上，更适用于工业化生产。

The invention discloses the anti-fake method by using the 3D stereoscopic icon, which can show 3D stereoscopic icons and hide the confidential image information in the 3D stereoscopic icons, comprising the following steps of: obtaining parameters, inputting confidential images and grey images; then using a visual divided storage method to build n visual divided storage images, using a 3D stereograph method to build n 3D stereoscopic images, adjusting the sizes of the n visual divided storage images and the n 3D stereoscopic images and dividing the n visual divided storage images and the n 3D stereoscopic images into a plurality of basic blocks; finally random choosing the basic blocks in the corresponding positions in the visual divided storage images or the 3D stereoscopic images to build n 3D stereoscopic and visual divided storage icons, etc.

为了既能三维立体显示图标，又能在三维显示的图标中隐藏秘密图像信息，本发明公开了利用三维立体图标防伪的方法，包括获取参数，输入秘密图像和灰度图像；然后利用可视分存方法构造n幅可视分存图，利用三维立体画方法构造n幅三维立体图，调整所述n幅可视分存图和所述n幅三维立体图大小并分成多个基本块；最后随机选取可视分存图或三维立体图中相应位置处的基本块，构造n幅三维立体可视分存图标等步骤。

N,N′-Disubstituted ureas,used as intermediates for synthesis of pesticides,resin precursors and carbamates,were synthesized from carbon dioxide and primary amines(namely n-propylamine, n-butylamine ,n-amylamine,n-hexylamine,benzylamine and aniline) over organic base catalysts.

以正丁胺为反应基质、TBD为催化剂，合成N，N′-二丁脲的最佳反应条件为：反应温度180℃，CO2压力10.0M Pa，反应时间10h，TBD摩尔分数5.0%；在此条件下，N，N′-二丁脲的收率为81.8%；红外光谱表征结果表明，合成的产物为N，N′-二丁脲。

The results indicated that when initial NO3--N was not leached, soil initial NO3--N and mineral N extracted by CaCl2 before aerobic incubation were closely related with raygrass nitrogen uptake, the correlation coefficients were 0.856 and 0.862, respectively, both reached at 1% significant level. When initial NO3--N was leached, it was no good relationship between mineralizable N extracted by aerobic incubation, soil initial mineral N and mineralizable N extracted by aerobic incubation, N0 and soil initial mineral N and N0 with raygrass nitrogrn uptake, the correlation coefficients were 0.410, 0.553, 0.492 and 0.419, respectively, indicating that the poor effects of mineralizable N on reflecting soil N capacity were influenced and disturbed by initial nitrate.

以包括土壤起始NO3--N盆栽试验植物吸氮量为参比，通气培养前CaCl2所淋洗起始NO3--N和起始矿质氮与5期黑麦草地上部氮素累积量密切相关，相关系数分别为0.856和0.862，达1%显著水平；与此相反，通气培养30周所矿化氮素、土壤起始矿质氮+通气培养30周矿化氮素、氮素矿化势(N0)及N0+起始矿质氮与5期黑麦草地上部氮素累积量间无显著相关关系，相关系数分别仅为0.410、0.553、0.492和0.419。

The influence factors such as n/ n,n(H_2O_2)/n,the concentration of hydrogen peroxide,reaction temperature and time were studied to find how they affected the synthesizing of accelerant NOBS adopting hydrogen peroxide oxidation method.

研究了n/n、n(H2O2)/n、双氧水浓度、反应温度和时间对双氧水氧化法合成促进剂 NOBS的影响，通过L16(45)正交实验确定出的最佳合成配方及工艺条件：n/n为7；n(H2O2)/n为1.6；双氧水浓度为12%；反应温度为40℃；反应时间为3h。

Study the bioactivity of the n-HA/PA66 composite and the effects it would be to body's metabolism of calcium and phosphorus ion in vivo.(3) Study the osteo-conductivity and the ability to repair bone defect of the porous n-HA/PA66 composite and the feasibility use it as the scaffold of bone tissue engineering. Objects and Methods as follows: 1.To evaluate the biocompatability of nano-hydroxyapatite crystals and polyamide composite (n-HA/PA66) with the L929 cells.To proceed the morphological observation and take pictures of L929 cells after 1d,2d,4d,and 7d of co-cultured with extract of n-HA/PA66 ,and direct contact with n-HA/PA66.To determine light absorbtion value of every hole under 500 nm with enzyme linked immunity instrument after 1 d,2 d,4 d,and 7 d of contact of n-HA/PA66 extract with L929 cells,and direct contact with n-HA/PA66.In the meanwhile calculate the relative multiplication rate of cells,and evaluate them by six degree tests for cytotoxicity. To investigate the acute and chronic toxic reaction on the whole body induced by the new nano-hydroapatite crystals and polyamide composite(n-HA/PA66)after implanting in vivo and its effects on partial constitution of animal organs after implanting in vivo,and evaluate the potential and degree of subcuticular stimulation reaction.

本实验主要由以下三部分组成：一、n-HA/PA66 复合材料在动物体内、体外的生物相容性及生物安全性评价二、n-HA/PA66 复合材料植入动物体内的生物活性及近期对机体钙、磷代谢影响的实验研究三、网孔 n-HA/PA66 复合材料作为支架修复兔桡骨节段缺损的动物实验研究主要研究目标及方法如下：参照 GB/T16886.5-1997-ISO 10993-5：1992《医疗器械生物学评价细胞毒性试验体外法》之评价标准和要求，采用规定的 L929 细胞(小鼠结缔组织成纤维细胞)，分别经直接接触和材料浸提液与细胞共培养等方式对 n-HA/PA66 复合材料进行细胞毒性测试，采用细胞形态观察法观察两种细胞各组在 24h、48h、72h、5 天后各时相点的细胞形态学变化，并在显微镜下照相，从而对细胞与材料的生物相容性进行定性评价；同时采用细胞生长抑制法，以酶标仪定量测定评价各组 1，2，4，7 天 L929 细胞的相对增殖率，以定量测定并判别材料对细胞的毒性程度。

The invention discloses a high-voltage P-type metal oxide semiconductor, including a P-type substrate, a deep N-well is arranged on the P-type substrate, an N-well drift region and a P-type drift region are arranged on the deep N-well, an N-type contact hole, a P-type source and a field oxide layer are arranged on the N-well, a P-type drain and the field oxide layer are arranged on the P-type drift region; the invention is characterized in that the thickness a grid oxide layer part which is positioned above the N-well is smaller than the grid oxide layer part which is positioned above the P-type drift region and a thin grid oxide layer and a thick thin grid oxide layer are respectively formed accordingly.

本发明公开一种高压P型金属氧化物半导体管，包括P型衬底，在P型衬底上设有深N型阱，在深N型阱上设有N型阱和P型漂移区，在N型阱上设有N型接触孔、P型源及场氧化层，在P型漂移区上设有P型漏及场氧化层，其特征在于位于N型阱上方的栅氧化层部分的厚度小于位于P型漂移区上方的栅氧化层部分并由此分别形成薄栅氧化层和厚薄栅氧化层。

The invention discloses a high-voltage N-type metal oxide semiconductor, including a P-type substrate, a P-well drift region and an N-type drift region are arranged on the P-type substrate, a P-type contact hole, an N-type source and a field oxide layer are arranged on the P-well, an N-type drain and the filed oxide layer are arranged on the N-type drift region; the invention is characterized in that the thickness a grid oxide layer part which is positioned above the P-well is smaller than the grid oxide layer part which is positioned above the N-type drift region and a thin grid oxide layer and a thick thin grid oxide layer are respectively formed accordingly, a P-type impurity injection region is arranged in the P-well, and the P-type impurity injection region is positioned below the thin grid oxide layer.

本发明公开一种高压N型金属氧化物半导体管，包括P型衬底，在P型衬底上设有P型阱和N型漂移区，在P型阱上设有P型接触孔、N型源及场氧化层，在N型漂移区上设有N型漏及场氧化层，其特征在于位于P型阱上方的栅氧化层部分的厚度小于位于N型漂移区上方的栅氧化层部分并由此分别形成薄栅氧化层和厚薄栅氧化层，在P型阱内设有P型杂质注入区且该P型杂质注入区位于薄栅氧化层的下面。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新