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SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.

并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析，结果显示SM6中主要为具有香气成分的不饱和脂肪醛，其中含量较高的依次为：-2，4-癸二烯醛(58％)、十四烷酸(55.78％)、2-癸烯醛(50％)、邻苯二甲酸异丁基十一烷酯(47％)、2，4-癸二烯(41％)、2-十一碳烯醛(31％)、2-甲基-Z，Z-3，13-十八碳二烯酸(18.45％)等；SM7中主要为饱和直链烷烃，其中含量较高的依次为：1，2-苯二羧酸丁基环己酯(23.90％)、三十烷(22.63％)、二十九烷(21.04％)、十七烷(18.84％)、二十八烷(13.58％)。

The structures of the target compounds were confirmed by MS, IR, 1H NMR spectra, and elemental analysis. The preliminary biological tests show that some of the target compounds have certain herbicidal activities.

通过元素分析， 1H NMR， IR 和MS确定化合物的结构，初步生物活性测试表明标题化合物具有一定的除草活性。

Five new heterocyclic compounds were synthesized and characterized by elemental analysis, IR, 1HNMR and MS.

总共合成5个新的化合物，并用元素分析，IR，~1HNMR，和MS进行了鉴定。

He fatty acid composition of grass carp was analyzed using GS-MS and more than 18 fatty acids were identified, including hexadecanoic acid, 9-hexadecenoic acid, 9-octadecenoic acid, 6,9-octadecadienoic acid, 9,12,15-octadecatrienoic acid, octadecanoic acid, 5,8,11,14-eicosatetraenoic acid, 4,7,10,13,16,19-docosahexaenoic acid, 5,8,11,14,17-eicosapentaenoic acid, pentadecanoic acid, heptadecanoic acid, and 5,8,11-heptadecatrienoic acid. There were some fatty acids with odd carbon atoms besides the fatty acids with even carbon atoms common in animals and plants.

P能改善蛋白质的乳化性和凝胶性。3、利用GC-MS对草鱼鱼肉中的脂肪酸进行分析，鉴定出草鱼中含有棕榈酸、十六碳烯酸、油酸、亚油酸、亚麻酸、硬脂酸、花生四烯酸、DHA、EPA、十五烷酸、十七烷酸、十七碳三烯酸等十八种以上脂肪酸，除含有动植物中常见的偶数碳脂肪酸外，还含有一定量的奇数碳脂肪酸。

According to the structure-activity relationships of actinonin and the theory that drug binds with acceptor, we designed and synthesized three series of novel hydroxamic acid derivatives in which the isoxazole ring were contained. Their structures have been confirmed by 1HNMR, MS and other analytic methods.

本文就是以天然放线菌素为先导化合物，根据放线菌素的构效关系和与PDF受体结合的原理，以易得的氨基酸为起始化合物，采用了不同的合成路线设计合成了三类新的含有异噁唑杂环的异羟肟酸衍生物，并通过1HNMR，MS及其他分析方法验证了它们的结构。

LC-ESI/MS is proved to be a simple, rapid, sensitive and specific technique for identification of the hydroxylate metabolites and its sulfate conjugates of daidzein in rat urine.

LC-ESI/MS法可以快速、简捷、准确地鉴定大豆黄素在大鼠体内羟基化及其结合形代谢产物。

Investigation of major metabolic pathways of SFZ-47 in animals The metabolites of SFZ-47 in rabbit urine following oral administration were separated and detected with HPLC and LC-MS methods. On the basis of the chromatographic behavior and mass spectra of the metabolites as well as biotransformation pathways of drugs with the partial structure of SFZ-47, the hydroxylic derivative 4-(3H-1, 2- dihydro-1-pyrrolizinone-2-methylamino benzyl alcohol and the carboxylic derivative 4-(3H-1, 2-dihydro-1-pyrrolizinone-2-methylamino benzoic acid of SFZ-47 were proposed as two potential metabolites and were synthesized.

在动物体内主要代谢途径的确定用HPLC和LC-MS对家兔口服SFZ-47后尿中的代谢物进行了分离、检测，根据代谢产物的色谱和质谱行为以及与SFZ-47有类似结构部分的其它药物的代谢途径，推测其羟基衍生物[4-（3H-1，2-二氢-1-吡咯里嗪酮-2-甲基胺基）苯甲醇]与羧基衍生物[4-（3H-1，2-二氢-1-吡咯里嗪酮-2-甲基胺基）苯甲酸]是两种可能的代谢产物，遂用化学方法合成了这两种衍生物。

The chemical composition of th essential oil from Illicium verum Hook.f.was determined by the means of GC-MS.

采用GC-MS对八角茴香挥发油的化学成分进行分析，其中反式茴香醚的含量最高。

Particles from burning of incense, rice stalk, cigarettes, generator, and diesel engines were collected by an impactor (Harvard Impactor 2.5) and an impinger (AGI-30). ED-XRF and ICP-MS were used to measure particle element component on filters and in suspension, respectively.

本研究以二种不同之采样方式，包括Harvard Impactor PM2.5冲击器及AGI-30冲击瓶（Harvard Impactor及Impinger）分别采集数种特定污染源所产生之微粒（PM2.5），并以ED-XRF及ICP-MS分别分析滤纸及悬浮液中微粒之元素组成。

F. based on gas chromatography-mass spectrometer method. Essential oil from cultivated variety Inula racemosa Hook. f. was extracted by steam distillation and analyzed by applying GC-MS.

方法］采用水蒸气蒸馏法从藏木香栽培品种中提取挥发油，并用GC-MS联用仪对其挥发油的化学成分进行研究。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。