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The mole fractions of unsubstituted, monosubstituted, disubstituted, and trisubstituted anhydroglucose units are in very good agreement with Spurlin model during the determined range.

在测量的范围内，未取代、一取代、二取代和三取代无水葡萄糖单元的摩尔分数分布和Spurlin模型非常吻合。

The sodium dithiobenzoic acid was oxidized with potassium ferricyanide to obtain di disulfide.The influences of raw materials mole ratio,stirring method and reaction time on the yield were studied with orthogonal test.

用铁氰化钾溶液氧化二硫代苯甲酸钠，得双二硫代苯甲酰，采用正交实验探讨了4，4'-偶氮双(4-氰基戊酸)与双二硫代苯甲酰反应的投料比、搅拌方式、反应时间对反应收率的影响。

The reaction conditions of synthesizingcyclohexyl acetate catalyzed with ammonium ferric sulfate dodecahydrate NH4Fe(SO42.12H2Oare studied .The yield of cyclohexyl acetate can reach 87.2% under mole ratio of aceticacid,cyclohexyl alcohol and ammonium ferric sulfate is 1∶0.44∶0.02,cyclohexane as solvent ,refluxing and segregating water for 60min.

研究了NH4Fe(SO4)2.12H2O催化合成乙酸环己酯的反应条件，当乙酸、环己醇和硫酸铁铵的摩尔比为1∶0.44∶0.02，以环己烷为溶剂，回流分水60min，乙酸环己酯收率达87.2%，在相同反应条件下，合成了甲酸环己酯(收率为68.5%)、丙酸环己酯(收率为59.4%)和丁酸环己酯(收率为21.6%)。

Polymerization was carried out between dimethyl adipate and triamine with the same mole ratio in the reactor. Acid dyeable additive can be obtained under the conditions of transesterification temperature 180~220℃, polycondensation temperature 240~270℃,pressure40~50Pa, The infrared analysis results showed that at the position of 1639cm^(-1), there was an obvious characterisitc peak of amide bond.

己二酸二甲酯与三胺按等量比在反应釜中进行聚合，在酯交换温度180~220℃，缩聚温度240~270℃，压力40~50Pa条件下即可获得酸性染料可染添加剂。

To improve the selectivity, the Co/Mn/Br catalyst system with ethanal as an additive was studied and the reaction conditions were also optimized, which were as follows:the amount of ethanal 10%(mole ration base on the substrate), reaction temperature 100℃,reaction time 30min,the oxygen pressure 0.2MPa, the amount of the composite catalyst Co/Mn/Br 7%,the mass ration of different ingredients 2:2:1. Under these conditions, the yield comes to 24.10% and the selectivity reaches 75.03%.

为了提高反应的选择性，论文初步研究了以乙醛作为添加剂条件下各工艺参数的影响，并进行正交优化，得出最佳条件为：乙醛加入量1：10，反应温度100℃，反应时间30min，氧气压力0.2MPa， Co/Mn/Br混合催化剂加入量7%，质量比2：2：1，在此条件下，反应产率为24.10%，选择性可达75.03%。

The results show that among the acetoacetonate complexes,Co_3 has the best catalytic activity.The optimum reaction conditions were as follows:0.764 mmol of Co_3,mole fraction of ethanal 10%based on the substrate,room temperature,oxygen pressure 2 MPa,reaction time 11h and solvent acetonitrile.Under these conditions,13.3%p-chlorobenzaldehyde was obtained with 15.3%conversion and 87.2%selectivity.The oxidation can also be carried out without solvent with 8.1%conversion,89.1%selectivity and 7.2%yield respectively.

在金属配合物中Co_3的催化性能最好，在其用量为0.764 mmol、乙醛用量为反应物物质的量的10%、氧气压力为2MPa时，以乙腈为反应介质，室温下反应11h，反应的转化率和选择性可达15.3%，87.2%，对氯苯甲醛收率可达13.3%；反应也可在无溶剂时进行，此时反应的转化率、选择性及醛的收率分别为：8.1%，89.1%，7.2%。

The influences of mole ratio of ethanediol and naphthenic acid,a mount of catalyst,reation time,reation temperature etc.on est erification were discussed and the suitable processing conditions were found.

介绍了用氧化亚锡非酸性催化剂催化合成环烷酸季戊四醇脂的方法，通过讨论醇酸摩尔比、催化剂用量、反应时间、反应温度等因素对该脂化反应的影响，从而确定了适宜的工艺条件。

The influences of mole ratio of ethanediol and naphthenic acid,a mount of catalyst,reation time,reation temperature etc.on est erification were discussed and the suitable processing conditions were found.

文摘：介绍了用氧化亚锡非酸性催化剂催化合成环烷酸季戊四醇脂的方法，通过讨论醇酸摩尔比、催化剂用量、反应时间、反应温度等因素对该脂化反应的影响，从而确定了适宜的工艺条件。

Ethyl 4,4,4-trifluoroacetoacetate was synthesized from ethyl acetate and 4,4,4-trifluoroacetate(mole ratio 3:1) with sodium ethoxide.

乙酸乙酯与三氟乙酸乙酯(摩尔比为3∶1)在乙醇钠作用下进行克莱森酯缩合反应，得到三氟乙酰乙酸乙酯。

In this paper, the electroplating of bright Zn-Ni alloy process was studied, the effect of (1-hydroxy ethylidene diphosphonate acid coordinating agent, chloride content, [Zn2+]/[Ni2+] mole ratio, cathode current density, temperature, a class of aldehyde compound (abbreviated as ZNP additive agent) and supplementary coordinating agent on Ni content, and brightness of plating layer was discussed, the physical phase of alloy plating layer and stability of plating solution were determined.

研究了用有机多膦酸盐作络合剂，ZNP作添加剂电镀光亮锌镍合金，探讨了络合剂、氯化物含量、[Zn2+]/[Ni2+]比、阳极电流密度、温度、辅助络合剂对合金中镍含量的影响，测定了合金镀层中物相组成及镀液稳定性，通过筛选得出最佳最镀光亮锌镍合金的镀液组成及工艺条件，并讨论了锌镍合金的异常共沉积机理。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！