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The best decoloring conditions for 40 ° c:, adjust pH = 3.5 percent, add 20 min, mixing carbon.

最佳脱色条件为: 40℃下,调节pH = 3.5,加入2%活性炭,搅拌20 min。

The results showed that the reaction condition was mild (70℃, 60 min). The derivatives could be directly detected by MALDI-TOF-MS without desalted procedure, avoiding lose of sample.

结果显示:衍生化方法反应条件温和(70℃反应60 min),衍生物不用脱盐处理即可直接进行质谱分析,检测灵敏度高,避免了微量样品的损失。

Under the optimum conditions, the lactobacillus bulgaricus microcapsule was madeby single agglomerate, and precipitated the wall with located in rapeseed oil with 50%ammonium sulfate solution; The preliminary micro-emulsion filtrated, then drawsome microcapsule from the micro-emulsion and progressing the second emul-sification, injecting a mixture with 3% CAP and 1.5% gelatin into the micro-emulsion,and keep the stirring speed 200r/min for 5 minutes, adjusting pH as 3.0 with aceticacid, then desiccating with the spray drier after 30 minutes. At last, got the prodtictof microcapsule powder.

通过最佳乳化条件制备的乳液,采用单凝聚法制备保加利亚乳酸杆菌微胶囊,用50%硫酸铵溶液,使菜籽油中的壁材CAP析出,形成初步的微胶囊,过滤,取上层微胶囊油液,缓慢注入3%CAP和1.5%明胶混合液中,进行第二次乳化,在200r/min的搅拌速度下乳化5min,用冰醋酸调节乳液的pH值至3.0,固化30min,取乳液置于喷雾干燥机中进行喷雾干燥。

This catalyst can cause discoloring of MY10 under the condition of pH 6.0 in 60 min.

在pH6.0条件下,60 min内可使200 mg/L媒介黄完全脱色。

In order to get the microcapsule which enwraps high success ratio of lactobacil-lus, we need developed a new emulsification method which can protect the activity oflactobacillus during the spray drying process. Firstly, rapeseed oil was used as adispersion medium when water was emulsified in the initial period, the concen-tration of emulsification were: CAP:3%, Tween-20:0.05%, Span-80:2%, glutin: 1.5%,mechanical stirring speed:900r/min,and the emulsification temperature was 37.5℃.

在制备用于微胶囊的保加利亚乳酸杆菌中,首先以菜籽油为分散介质,在初步的乳化条件中,最佳的乳化条件为:邻苯二甲酸醋酸纤维素的浓度为3%、表面活性剂Span-80的浓度为2%、Tween-20的浓度为0.05%、明胶的浓度为3%、搅拌速度为900 r/min、乳化温度为37.5℃。

Finally, local effects of CPZ were confirmed in the formalin test and it was shown that the formalin-induced paw flinches were strongly suppressed by CPZ in phase 1 but with phase 2 being significantly suppressed only during 25-55 min.

利用行为学技术方法证明足底注射CPZ可以明显抑制福尔马林溶液所致的第一相全程和第二相内仅第25~55 min的自发缩足反射。

According to the Box-Benhnken design principle,the method of response surface method with 3 factors and 3 levels was used. The factors influencing the technological parameters were determined by means of regression analysis. Response surfaces were finally graphed with the yield as the response value. The synthesis conditions were optimized as follows:reaction reagent was NBS,stoichiometric proportion between NBS and anhydrovinblastine was 1.07; the dosage of TFA was 22 mL/L; reaction temperature was -68 ℃ and duration was 90 min.

在单因素实验基础上,根据Box-Benhnken实验设计原理,采用三因素三水平的响应面分析法,研究了各个因素及其交互作用后,得到了合成7′-Br-脱水长春碱的最佳工艺条件:以二氯甲烷为溶剂,采用NBS为溴代剂,其用量与底物的物质的量比为1.07∶1,TFA的加入量22 mL/L,在-68 ℃下反应90 min,终止反应后,得到卤代产物。

It is a MAX-MIN ant system hybridized with tabu search, which is implemented in the hyper-cube framework.

该算法主体是一个在超立方框架下执行的MAX-MIN蚂蚁系统,算法混合了禁忌搜索算法作为局部优化算法,同时集成了一个后优化过程来进一步优化最优解。

The xylanase displayed about 50% retained acitivity after incubating at 80℃ for 30 min.

在pH 2.4~5.4范围内,酶的相对活性都在75%以上,重组酶在80℃保温30 min还有近50%的残余酶活。

According to the physiochemical properties of anthocyanin, methanol solution containing 0.1 mol/L HCl was selected as the extraction solution, then grape pomace lixiviated for 30~40 min with pH=3.0~4.0 and temperature at 60~70 ℃, and then the liquid or paste extract was prepared after a series of technical procedures including extraction, centrifugation, filtration and vacuum concentration.

本课题根据花色素苷的理化性质,选择了用0.1 mol/L 的HCl的甲醇溶液作提取剂,在pH值为3.0~4.0及60~70 ℃温度下浸提30~40 min,再经萃取、离心、过滤、减压浓缩,可得到液态或膏状提取物,并通过了分析检测;还对花色素苷在食品工业中的应用作了研究。

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The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作:对伸臂位于顶部的单层框架—筒体模型进行分析,提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。

Its advantage is that it can be used in smaller units.

其优点在于可以在较小的单位中应用。