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The quantity of catalyst was equal to 0.6% of feedstocks,the reaction temperature was 78~110 ℃,and the reaction time was 45 min. The test results have shown thatH_4SiW_(12-O_(40)/MCM-48 is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal with its yield reaching over 91.9%.

实验表明:H4SiW12O40/MCM-48是合成丁酮-1,2-丙二醇缩酮的良好催化剂,在n∶n(1,2-丙二醇)=1∶1.6,催化剂用量为反应物料总质量的0.6%,环己烷为带水剂,反应时间45 min的优化条件下,丁酮-1,2-丙二醇缩酮的收率可达91.9%。

D limonene was distributed among the culture flasks (200 mg/L). The flasks were incubated at 28oC on a rotary shaker (r/min=120) for 5 days. On completion, the culture broth were successively extracted with EtOAc. The extract was quantitatively measured by gas chromatography mass spectrometry analysis, The results showed that biocatalytic reactions were comprised of oxidation, including hydroxylation and ketonization which occurred at different positions of the D limonene, as well as hydrogenation, hydrolyzation, esterification and cyclic cleavage. These bacteria strains possess the distinctive biocatalytic capacities towards the D limonene. A series of terpenoids, including sesqui , di and tri terpernoids were also observed,which was accounted for D limonene had influence on the metabolites of marine bacteria.

以2216E为培养基,添加200mg/L的柠檬烯,在28℃,以120 r/min摇瓶培养5 d,用乙酸乙酯提取培养液,经GC MS分析其转化产物,结果显示,这些细菌能在柠檬烯的不同位置进行羟基化、羰基化等,并伴随有还原、水解、酯化、开环等反应,但转化能力和转化程度不同;在产物中,还检测到系列结构不同的其它萜类:包括倍半萜、二萜以及三萜等,这些萜类化合物的产生跟柠檬烯的加入有关,说明柠檬烯能影响细菌代谢产物的产生。

The optimal technological parameters of oil transesterification from Kosteletzkya virginica oil should be as follows: the rate of rotation 1800r.min-1, catalyst dosage 0.6%, mole ratio of methanol to Kosteletzkya virginica oil 6/1,reaction time 60min and reaction temperature 65℃, and under such conditions, the total oil transesterification ratio after transesterification three times is 97.8%.

海滨锦葵油制备生物柴油的最佳工艺参数为:搅拌强度为1800r.min-1,催化剂KOH用量为海滨锦葵油质量的1%,醇油摩尔比6/1,反应时间60min,反应温度65℃,在该工艺条件下,酯交换反应三次,酯交换率达到97.8%。

The LMA removal was consideredsuccessful when there was no coughing, clenching of teeth, orgross purposeful movements during or within 1 min after removaland also if there was no breath holding, laryngospasm, or desaturationafter removal.

当拔除过程中或拔除后1 min 内无咳嗽、牙关紧闭或有目的的大体动,且如果拔除后无屏气、喉痉挛或氧饱和度下降,则认为 LMA 拔除成功。

The max-min composition indicates the strength of lation between the element of X and Z.

max-min组合是指在元素X和Z之间的平移长度。

The results show that the optimal parameters of esterification are as follows: 4% of SO42-/ZrO2, molar ratio of methanol to litsea cubeba kernel oil 101, 68 ℃ of reaction temperature and 4 h of reaction time, the acid value decreases to 2.52 mg/g. Compared with the traditional acidic-catalyzed method, this method has the advantages of no acid proof equipment, easy to recycle catalyst and no acidic waste water emission. The optimal parameters of transesterification are as follows: 25 ℃ of reaction temperature, 0.5% of hexadecyl-trimethyl-ammonium bromide, 1% of NaOH, molar ratio of methanol to the oil 61 and 15 min of reaction time. The ester exchanging rate is 97.6%. This method adopts phase transfer catalyst and produces industry prospect, which has many advantages such as energy-saving and time-saving under room temperature.

研究结果表明,固体酸SO42-/ZrO2催化酯化反应的最佳条件为:油重4%的SO42-/ZrO2,醇油摩尔比为101,温度为68 ℃,反应时间为4 h,原油酸值降到2.52 mg/g;该法相对浓硫酸催化酯化法具有不需耐酸设备、催化剂易回收、无废水排放等优点;相转移催化酯交换反应的最佳条件为:温度为 25 ℃,0.5%的十六烷基三甲基溴化铵,油重1%的NaOH,醇油摩尔比为61,反应15 min,原油酯交换率达到97.6%;采用相转移催化技术,反应在常温下进行,大大减少了能耗,缩短了反应时间,具有的产业化前景。

Ethanol yield could reach 20.52 g/L (74.5 %of theoretical yield) under the following conditions: fermentation temperature at 28 ℃, initial pH value as 5.0, 150 mL liquid loadage in 250 mL rotating flask, and rotating speed at 160 r /min, and 0.5 % corn steep liquor and 0.024 % urea. Tran. by YUE Yang

在28 ℃,初始pH值5.0,160 r/min,250 mL三角瓶装液量150 mL,木糖浓度60 g/L,玉米浆0.5 %,含尿素0.024 %的条件下,休哈塔假丝酵母发酵木糖能产乙醇20.52 g/L,得率达到理论值的74.5 %。

Ethanol yield could reach 20.52g/L (74.5%of theoretical yield) under the following conditions: fermentation temperature at 28 ℃, initial pH value a 5.0, 150mL liquid loadage in 250mL rotating flack, and rotating speed at 160r/min, and 0.5% corn steep liquor and 0.024% urea.

在28℃,初始pH值5.0,160r/min,250mL三角瓶装液量150mL,木糖浓度60g/L,玉米浆0.5%,含尿素0.024%的条件下,休哈塔假丝酵母发酵木糖能产乙醇20.52g/L,得率达到理论值的74.5%。

METHODS: Patients in the aerobic exercise group were given aerobic exercise four times a week, 30 min/time for 12 weeks on the basis of the medicative therapy.

有氧训练组在接受以甲氨蝶呤为主的药物治疗基础上,进行4次/周的有氧运动训练,30 min/次,共12周。

The application of low pressure boiling technique could increase wort boiling temperature to 100.5 ℃ and advance protein agglomeration and reduce solidifiable nitrogen content to 0.5 mg/100 mL. Maillard reaction and Brown reaction were strengthened in the boiling, melanoidin and melanoid compound contents increased, wort chromaticity improved, and the oxidation resistance of wort strengthened. Besides, the boiling intensity dropped from 9 %~12 % to 7 %~8 % and boiling time shortened to 10~20 min, which improved production efficiency and saved 20 % energy and improved beer non-biological stability.

采用低压煮沸工艺,可提高煮沸麦汁温度至100.5 ℃,加强蛋白质凝聚,麦汁可凝固氮下降0.5 mg/100 mL;煮沸过程加强了美拉德反应、&棕色反应&,类黑精、类黑素化合物增加,麦汁色度增加,麦汁的抗氧化能力增强;煮沸强度从9 %~12 %降至7 %~8 %,煮沸时间缩短10~20 min,提高生产效率,节约能源20 %;改善啤酒非生物稳定性。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。