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The microstructure of Ti Zr alloy formed under this suitable technologic parameter matching was analyzed by scanning electron microscope. RESULTS: When the ratio of laser power to facular diameter was 2.7 kW/3 mm, the powder feeding speed was 90 r/min and the moving speed of numerical control machine was 5 mm/s, better H (826.61 μm) and W (3504.61 μm) were obtained.

结果: 在激光功率与光斑直径之比为2.7 kW/3 mm,送粉器转速为90 r/min和数控机床的运动速度为5 mm/s等参数下,Ti Zr粉末激光立体成形时具有较好的H和W,分别为826.61 μm和3504.61 μm。

The results showed that the higher peptides yield was 38.96mg/g on the conditions of 1% brown sugar power,initial pH7.5,temperature 30 ℃,rotational speed 180 r/min and the substrate 7%,which was fermented 48 h.The higher yield of free amino acids was 0.344% when ferme...

结果表明,发酵培养基碳源为红糖粉添加量1%,发酵初始pH 7.5,发酵温度30℃,转速180 r/min以及底物浓度7%,发酵48 h时多肽含量达到38.96 mg/g,当发酵时间持续到72 h可得到较多游离氨基酸,含量为0.344%发酵48 h发酵液的香味较好。

Porous TiO2 nanostructures, well-adhered to Ti foil surfaces, were formed at 80 ℃ in 10 min, and then flowerlike and rod nanostructures formed in succession after a longer reaction time.

在80 ℃下反应10 min得到了和Ti片黏附较好的多孔纳米结构,延长反应时间先后得到了类化状和类棒状纳米结构。

A HPLC/ESI-MS method studied on relative compounds of chloramphenicol succinate ;Column:an Agilent ODS column 250×2.1mm;Mobile phase: 0.05M ammonium formicate buffer PH4.0/acetonitrile=80/20 ,flow0.2ml/min, and λ276nm;Mass:trap ion mass;source:ESI;Scan mode:negative ion scan.

液相色谱条件为色谱柱:Agilent C18 2.1mm×250 mm;流动相:流动相0.05M甲酸铵用甲酸调pH至4.0 /乙腈=80/20,流速0.2ml/ min,检测波长276nm;质谱条件为离子肼电喷雾质谱仪,离子源:ESI;检出模式:负离子检测。

The volume ratio of furaldehyde to acetic anhydride is 1∶2; the mole ratio of furaldehyde with anhydrous potassium carbonate is 1.00∶0.54. The best phase transfer catalyst is PEG1000, the mass ratio of PEG1000 with furaldehyde is 4.3%, the reaction time is 11 min, the reaction power of microwave is 260 W. The yield ofα-furanacrylicacid is up to 72.3% under these reaction conditions.

研究结果表明:在微波辐射功率为260 W、微波反应时间为11 min、以聚乙二醇1 000(PEG1000)为相转移催化剂,糠醛与乙酐的体积比为1∶2,糠醛与无水碳酸钾的量比为1.00∶0.55时,α-呋喃丙烯酸的产率为72.3%。

The comparison studies on gossypol of different genetic types of pigment gland in the seeds of cotton newly bred, including the special and common glandless and glanded ones, was conducted through highperformance liquid chromatography on a C18 Column with methanol 0.5% acetic acid aqueous solution, 90∶10 as mobile phase at a flow rate of 0.8mL·min-1 and UV detection at 254 nm.

运用高效液相方法对新近育成的特殊和普通的无腺体陆地棉及特殊和普通的有腺体陆地棉及海岛棉等多种遗传类型品种材料的棉酚含量进行了比较研究。实验以一反向C18色谱柱为固定相,甲醇 0.5%的醋酸90∶10为流动相,流速为0.8mL·min-1,建立了分离度好、准确而快速的棉酚HPLC测定方法:其最低检测限量3×10-6g/mL-1,精密度和准确度均小于10%,回收率为100.4%~103.2%。

C, 200rpm for 5d then placed statically for more than 7d, and addition more than 0.01% Chitosan to Bacillus subtilis suspension provided significant UV protection. The survival spore rate is 90% about 2-2.5 fold better than control for spore exposed to UV radiation for 30 min. Bioassay in against Glomerella cingulata, and the inhibition activity is still 60%.

枯草杆菌於MIY液态培养基中,30°C,200rpm震荡培养五天后静置培养七天以上,以甲壳素添加浓度大於0.01%作为最适宜的紫外保护剂之作用最好,於UVB灯下暴晒30 min,对枯草杆菌孢子的保护效果最好,存活率达90%以上,抗紫外线活性是不添加紫外线保护剂的CK组的2.5-3倍,对檬果炭疽真菌仍有60%的抑菌活性。

When 45% methanol solution containing 0.5 mmol/L hexamethylene tetraamine was used as the pump carrier, the pump flow rate and output pressure achieved 0.58 mL/min and 0.79 MPa at 4950 V, respectively. By using the pump carrier as the mobile phase, benzene and naphthanlene were separated on baseline by the EFA system.

在4950 V的外加电压下,以含0.5 mmol/L六亚甲基四胺的45%甲醇溶液为泵载流,电渗泵的流量和输出压强分别为0.58 mL/min和0.79 MPa,以泵载流为流动相,该系统对苯和萘进行了反相色谱分离。

Methods: Collect the sEMG signals of the middle part of both deltoid muscles when the subjects make both shoulders contract homometrically to the maximum abduction. After 20 min relax, do acupuncture "jian san zhen"(Jianyu/Jianqian/Jianhou) on the left shoulder and collect the signals.

志愿受试者做肩关节最大外展等长收缩,测量双侧三角肌中部肌束sEMG变化数据,两次测量中间间隔20 min,其间针刺左侧&肩三针&。

The result of immobilization showed that hydrophile membranes were more advantageous than hydrophobe ones to act as immobilization carrier. Crosslinking organophosphorus hydrolase by glutaraldehyde on polyethersulfone membrane is a simple and practical immobilization method. An appropriate amount of bovine serum albumin and crosslinker is necessary to get a good result of immobilization. In the biodegradation of methyl-parathion through enzyme membrane reactor, the effect of immobilized enzyme amount, flow rate of peristaltic pump, pH of the feed, and the methyl-parathion concentration on biodegradation rate was studied. It was shown that the biodegradation rate increased with immobilized enzyme amount and substrate concentration. Biodegradation rate didn't increase when the folw rate of the peristaltic pump was larger than 7 ml/min.

然后,研究固定化酶降解甲基对硫磷,从不同材料的膜载体固定有机磷水解酶的比较中,发现亲水膜比疏水膜适合作固定化酶载体;在此基础上,将有机磷水解酶固定在聚醚砜微滤膜上,并制成酶膜生物反应器,用于降解甲基对硫磷;戊二醛化学交联法固定时,酶液与10%牛血清白蛋白溶液的比例在3:1~2:1,与交联剂的比例在7:2~7:4范围内,固定化效果较好,并发现牛血清白蛋白和膜载体有降低酶活损失的作用;将固定化的酶膜装于酶膜反应器降解甲基对硫磷,实验结果表明:反应器的降解速率与固定化酶量呈正比,也随底物浓度的增加而加快,当流速低时,降解速率随流速增大而加快,到7ml/min以上时,降解速率不随流速脑黾佣洌到獾淖畹团ǘ任?

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。