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The structure and morphology of CNTs which have been purified and not yet, were characterized by TEM, SEM, XRD, Raman, TG-DTA, BET, IR. The results indicated that when the stokehole reaction temperature was 1170℃,the decompose temperature of Ferrocene was 150℃,he volatilize temperature of Benzene was 50 ℃, hydric flow rate was 270ml/min, the concentration of thiophene was l% and the reaction time was 20 minutes, the CNTs with single-walled and multi-walled were prepared.
结果表明:炉膛反应温度1170℃、二茂铁的分解温度150℃、苯的挥发温度50℃、氢气的流量270ml/min、噻吩体积分数1.00/100ml苯、反应时间20min时,可以得到碳纳米管,既有单壁管又有多壁管,单壁管的内径分布在0.88~1.15nm之间,多壁管的直径分布在40~120nm之间;纯化后的碳纳米管比表面积增加,管壁光滑,而且产生了大量的含氧官能团,有利于在水溶液中的分散。
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The structure and morphology of CNTs which have been purified and not yet, were characterized by TEM, SEM, XRD, Raman, TG-DTA, BET, IR. The results indicated that when the stokehole reaction temperature was 1170℃,the decompose temperature of Ferrocene was 150℃,he volatilize temperature of Benzene was 50 ℃, hydric flow rate was 270ml/min, the concentration of thiophene was 1% and the reaction time was 20 minutes, the CNTs with single-walled and multi-walled were prepared. The diameters of the single-walled CNTs are in the range of 0.08~1.15nm, and that of the multi-walled CNTs are in the range of 40~120nm.
结果表明:炉膛反应温度1170℃、二茂铁的分解温度150℃、苯的挥发温度50℃、氢气的流量270ml/min、吩体积分数1.00/100ml苯、反应时间20min时,可以得到碳纳米管,既有单壁管又有多壁管,单壁管的内径分布在0.881.15nm之间,多壁管的直径分布在40120nm之间;纯化后的碳纳米管比表面积增加,管壁光滑,而且产生了大量的含氧官能团,有利于在水溶液中的分散。
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Technical parameter: Striation water jet commonly used current capacity: 0.8-1.8L/min, jet velocity
技术参数:线状喷射水流的常用流量:0.8-1.8L/min,喷射速度
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Fig. 5.Intracellular potential changes 30 min after injection of strychnine at indicated stimulus strength.
图5。肌注士的宁后30 min,以如图所示强度刺激迷走神经诱发的M细胞胞内电位变化
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The optimal processing conditions are as follows: roasting temperature at 1 000℃, roasting time for 40 min, the ratio of NbH dosage to theoretic dosage at 1.1. The specific capacity of niobium suboxide of preparation by agate grind procedure is 69.50 mF·V·g-1, the loss is 11.25%, the leakage current is 1.8×10-4A·F-1·V-1, and the electrical properties are better than that of the national standard (GB/T 3136-1995) of FTa16-300 tantalum powder for capacitor.
用正交试验法及方差分析对玛瑙研磨工艺进行优化,得到制备低价铌氧化物最佳条件是:焙烧温度为1 000℃,焙烧时间为40 min, NbH用量与理论量之比为1.1,所制得的产物杂质含量低,比容为69.50mF·V·g-1,损耗为11.25%,漏电流为1.8×10-4A·F-1·V-1,其电性能指标高于FTa16—300电容器钽粉国家标准(GB/T 3136—1995)所规定的值。
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Fig. 3 TG and DTG curves of lignin and paper mill sullage particles pyrolysis in heating rate of 20 'C /min
图3 木质素、造纸废液颗粒在20 9C/min升温速率下的TG, DTG曲线
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Observations on the probing and feeding behaviors of free whiteflies confirmed the EPG results as above: the percentages of whiteflies stayed on leaves within 60 min were 100%, 88% and 28% on cabbage, summer squash and hot pepper, respectively.
在自由状态下,烟粉虱60 min内在甘蓝、西葫芦和辣椒上留存粉虱的百分比分别为100%、88%和28%,这进一步验证了上述依据EPG记录得到的结果。
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Moreover, the hot compressive deformation behavior of the RS/PM AZ91 magnesium alloy and AZ91 alloy matrix composite were also investigated, the conclusions are drawn as follows:1. The processing parameters of the atomization-twin rolls quenching technology were optimized as follows: the diameter of the nozzle 1mm, the wheel velocity 25m/s, the pressure of atomization gas 0.3MPa and Ar gas for melt injection 0.1MPa. The RS AZ91 alloy flakes exhibited fine and uniform microstructures. When the flakes were extruded at 673K, extruded velocity of 0.1mm/min and extrusion ratio of 25:1,the magnesium alloy rods with clean surface, uniform dimension and excellent mechanical properties were obtained.2. The RS AZ91 magnesium alloy powders prepared by atomization-twin rolls quenched technology exhibited fine equiaxed grains with the grain size of 1-3μm, the phase constituent included supersaturate solid solution phaseα-Mg and miner fineβ-Mg_(17)Al_(12) phase. The as-extruded materials also exhibited equiaxed grains with the size of 5-7μm and a large number of fineβ-Al_(12)Mg_(17) and fewer AlMg_2Zn phases were detected in the alloy.
本文还研究了快速凝固/粉末冶金AZ91镁合金热压缩变形流变应力行为,快速凝固/粉末冶金法原位生成Mg_2Si增强AZ91镁基复合材料,经过系统的研究,获得如下结论:1、雾化-双辊急冷法在下列工艺参数组合下:双辊线速度25m/s;喷嘴直径1mm;熔体压射压力0.1MPa;雾化气体压力0.3MPa。,可获得宏观尺寸细小、微观组织均匀细小、综合性能优良的的快速凝固AZ91镁合金细碎箔带,快速凝固箔带在挤压温度为673K、挤压速度为0.1mm/min,挤压比为25:1时,可获得的外表光洁、尺寸均匀、组织性能优异的镁合金棒材。2、雾化-双辊急冷法制备的AZ91镁合金粉末态为细小等轴晶组织,晶粒尺寸1-3μm,组织为α-Mg过饱和固溶体和微量的细小β-Mg_(17)Al_(12)相组成;粉末挤压棒材为等轴晶组织,晶粒尺寸5-7μm,组织中含有大量细小的β-Al_(12)Mg_(17)以及AlMg_2Zn析出相,室温力学性能,抗拉强度383MPa,屈服强度275MPa,断后伸长率7.5%。
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There were 613 breaks of ischemia symptomless in which 504 broke while at rest or sleeping, lasting for 3~5min and 88 breaks were symptomatic in which 53 broke while at rest and 25 broke in daily activities, lasting for 1~3 min and there were significant changes of ischemia on DCG and the ST segment descent for 0.1~0.3 mV.
结果:138例患者24h监测发现在所有ST段下移1mm以上的缺血发作701次,无症状发作613次,其中休息和睡眠时发作504次,持续时间为3~5min;有症状发作88次,其中休息和睡眠53次,日常活动时 25次,持续时间为 1~3 min,DCG检测中有明显的心肌缺血表现,ST段降低幅度0.1~0.3mV。
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The optimum parameters were that the water content in meal was 16.6%,heating time was 32 min and tempera...
豆粕酶活最低的灭酶条件是:豆粕水分含量为16.6%,加热时间为32 min,温度为100.5℃。
- 推荐网络例句
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Do you know, i need you to come back
你知道吗,我需要你回来
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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.
1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。
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Chapter Three: Type classification of DE structure in Sino-Tibetan languages.
第三章汉藏语&的&字结构的类型划分。