查询词典 ML

objective to determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of edaravone, by gas chromatography.methods sample solution was injected on a gdx column (0.18 mm～0.25 mm) with nitrogen as the carrier gas.the residue was calculated by the external standard method.results the linearity was good over the range of 25 μg/ml～400 μg/ml,with the correlation coefficient of acetone being 0.996 and the average recovery 96.8%.conclusions the method was proved to be simple,rapid,practical and highly sensitive.it is an efficient method for the quality control of acetoacetic ester.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。方法：采用固定相为二乙烯苯乙基乙烯苯型高分子多孔小球（直径为0.18 mm～0.25 mm），氮气为载气，用外标法测定乙酰乙酸乙酯中残留丙酮的含量。结果：该方法在丙酮浓度范围在25 μg/ml～400 μg/ml内呈良好的线性关系，响应曲线相关系数为0.996，平均回收率为96.8%。结论：本法简便，快速、实用，灵敏度高，可有效地用于乙酰乙酸乙酯的质量控制。

The result showed that the methane tank sludge was execellent, with 25338.16 mL of the total aerogenesis tolerance, 844.61 mL of day aerogenesis tolerance.

通过对沼气池污泥的接种量设置不同的梯度，研究接种量对产气效果的影响。

The results showed that under 8% of raw total solids concentration, 6.8-7.4 of pH, the methane tank sludge, 20% of them inoculated, after 30 days of fermentation, it was 9 days of period that the effect was execellent. The total aerogenesis tolerance was 42490.70 mL, the day aerogenesis tolerance was 1416.36 mL, the pit held aerogenesis rate was 0.217 m~3/m~3·d , the stuff held aerogenesis rate was 0.241 m~3/m~3·d, the raw material aerogenesis rate was 0.090 m~3/kg·TS.

结果表明，在原料的总固体浓度为8％、pH值介于6.8～7.4、接种沼气池污泥量为原料干物质重量的20％、发酵周期为30d时，对发酵系统间隔9d换料的效果最好，其在总产气量、日均产气量、池容产气率、料容产气率和原料产气率分别达到了42490.70mL、1416.36mL、0.217m~3／m~3·d、0.241m~3／m~3·d和0.090m~3／kg·TS，都比不换料的对照处理有很大提高，分别提高了153.41％、153.41％、152.33％、153.68％和150％，沼气中的甲烷含量也在70％以上。

Result According to the result of identification, TF413 belonged to Alcaligenes faecalis. The optimum temperature for it degrading triazophos was 32℃, and the optimum primary pH value was 7.0, the optimum liquid volume in flask was 50 ml medium in 100 ml erlenmeyer flask, the optimum medium was nutrient broth, the inoculation amount had no obvious effect on degradation effect of TF413 on triazophos.

结果］经鉴定，TF413菌株为粪产碱杆菌，其降解三唑磷的最适温度为32℃、最适初始pH值为7.0，最适装液量为100m1三角瓶中装50ml培养基，最佳培养基为营养肉汤，接种量对TF413降解三唑磷的效果无明显影响。

The BMSCs were divided into six groups after repeatedly passaged: A,the BMSCs were cultured with conventional culture fluid(DMEM culture fluid+20%fetal bovine serum+2 mmol/L aminoglutaric acid amine) all the time;B,the BMSCs were cultured with conventional culture fluid+HGF(25ng/ml)+dexamethasone10~(-7M;C(HGF and Zuoguiwan induced group), the BMSCs were cultured with conventional culture fluid+ HGF(25ng/ml)+ dexamethasone10~(-7M+ 10%Zuoguiwan drug serum;D(conditioned medium and contrast serum induced group), the BMSCs were cultured with conventional culture fluid+50 % conditioned medium+10 % normal rat serum;E(conditioned medium and Bazhentang drug serum induced group), the BMSCs were cultured with conventional culture fluid+50 % conditioned medium+10 % Bazhentang drug serum;F(conditioned medium and Zuoguiwan drug serum induced group), the BMSCs were cultured with conventional culture fluid+50 % conditioned medium+10% Zuoguiwan drug serum.

常规培养组始终使用常规培养液(DMEM培养液+体积分数20％胎牛血清+2mmol／L谷氨酸胺)进行培养；HGF诱导组以常规培养液+促肝细胞生长因子(HGF，25ng／ml)和地塞米松10~(-7M进行培养；HGF加左归丸组以常规培养液+促肝细胞生长因子(HGF，25ng／ml)和地塞米松10~(-7／M+10％的左归丸含药血清进行培养；条件培养液加对照血清组以常规培养液+50％的条件培养液+10％正常大鼠血清进行培养；条件培养液加八珍汤组以常规培养液+50％的条件培养液+10％八珍汤含药血清进行培养；条件培养液加左归丸组以常规培养液+50％的条件培养液+10％左归丸含药血清进行培养。

ML nonionic contrast agent was administered with a constant flow rate of 8 mL/s via the antecubital vein by using a power injector.

动态CT检查方法为在启动高压注射器经肘静脉快速注入对比剂的同时对感兴趣层面进行连续快速扫描。

By using a power injector,60 ml of 75% contrast material was injected at a speed of 3 ml/sec via a 17-guage antecubital vein catheter,14 s after start of bolus the dual-phase dynamic CT scans were performed 7 times at the single level.

48例肝肿瘤患者平扫发现并定位病灶后，用压力注射器以3ml／s速度从肘静脉经17号塑料套管针注入造影剂60ml，开始注射后14s行双期动态CT，同层共扫7次。

METHODS : Twenty－five relapsed APL patients were enrolled (M 15, F 10, 3 4 a±s 12 a), 10 mL of 0.1% arsenous acid solution+5% glucos e 500 mL was injected iv, dr ip, daily for 28－56 d.

复发的急性早幼粒细胞白血病25例(男性15例，女性10例；年龄34a±s 12 a)以亚砷酸10mg/d+5%葡萄糖注射液500 mL静脉滴注，28～56 d为一个疗程。

METHODS:We recorded the cardiogram by perfusing garlicin injection and garlic preparation to the isolated heart of rabbits by Langendorff method,examined the minimum dose of asystole. RESULTS:The minimum fungistatic concentration of garlicin injection was 3～6.2 times lower than that of garlic preparation. The minimum dose of garlic preparation is 0.1736 u/ml, and that of garlicin injection is 3.919 u/ml.

采用Langendorff法对兔离体心脏分别灌流大蒜素注射液、大蒜注射液、大蒜实验液，分别记录心搏图，求出致心脏停搏的最小剂量，结果：大蒜素注射液的抑菌浓度为大蒜实验液的1/6.2～1/3，而致心脏停搏的最小浓度分别为0.1736 u/ml和3.919 u/ml。

Methods Ovarian GC DNA fragments of both atretic and developing follicles before and after estrogen (1 μg/ml), androgen (1 μg/ml) treatments were analysed by agarose gel electrophoresis. The expression of bcl-2 mRNA was also determined by northern blotting in GC of developing follicle after sex steroids addition. Results Internucleosomal DNA cleavage occurred in granulosa cells in atretic follicles and after androgen treatment.

应用细胞培养、选择性DNA抽提和琼脂糖凝胶电泳技术分析闭锁卵泡和发育中卵泡颗粒细胞的凋亡状况，及雌激素(1 μg/ml)、雄激素(1 μg/ml)对体外培养发育中的卵泡颗粒细胞凋亡的作用；用Northern印迹杂交技术检测经雌、雄激素刺激后发育中的卵泡颗粒细胞bcl-2基因mRNA表达的变化。

The work of this paper is as follows: 1. Looking back the progressing history of the linear motor, introducing the features of the elevator driven by linear induction motor, radicating the topic of this paper "the digital frequency variable control of the elevator bi-side direct driven by linear induction motor". The research of this paper covers the conventional VVVF control, space vector based VVVF control, vector control and DTC.

本文主要开展了以下几个方面的工作： 1 回顾了直线电机发展历史，电机的驱动技术演变，特别是针对直线电机的驱动，简要介绍了直线感应电机驱动电梯的优点和不同结构类型，对传统的v／f控制，基于空间矢量法的v／f控制，矢量控制，和基于电压空间矢量的直接转矩控制进行了比较，确立了本课题的研究主题：直线感应电机双边直推式驱动电梯的全数字变频控制。

The article combines with the treatment of a superficial civil air defense work to introduce how the grouting method to improve the performance of the backfill soil.

文章从治理漂浮人防工事的角度提出了注浆技术在改善回填土性质方面的应用，并详细阐述了注浆技术的施工流程。