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The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱，以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相，流速1ml/min，检测波长210nm，柱温40℃。结果阿奇霉素的线范围为50.3～1006μg/ml，平均回收率100.1%，r=1.0000，RSD=0.8%(n=9)。

In the CMKGM preparation section,with the indicators of DS andη, the optimum laboratory conditions preparation of a certain molecular weight of the high DS of CMKGM: reaction time (5～6) h, the theory of the degree of substitution (2～3), the molar ratio of monochloroacetic acid to Sodium hydroxide (2:1～3:1),the reaction temperature (55～65)℃, liquid ratio (10:1～12:1)mL/g, containing enthanol (50～70)%.

CM(来源：5e60ABC论文网www.abclunwen.com)KGM制备工艺研究中，以取代度、表观粘度为指标，建立了制备一定摩尔质量的高DS的CMKGM的实验室制备条件：反应时间(5～6)h、理论取代度(2～3)、氢氧化钠与氯乙酸摩尔比(2：1～3：1)、反应温度(55～65)℃、液料比(10：1～12：1)mL/g、乙醇体积分数(50～70)%。

Inosine -5'- monophosphate (5'-IMP) and guanosine-5'-monophosphate (5'-GMP) in samples were separated successfully using an Inertsil ODS-3 column (250 mm×4.6 mm, 5 μm) when 0.02 mol/L monopotassium phosphate (pH 4.5) was employed as the mobile phase with a flow rate of 1.0 ml/min at 250 nm and 25℃.

采用Inertsil ODS-3色谱柱(250 mm×4.6 mm， 5μm)；以0.02 moL/L磷酸二氢钾溶液(pH 4.5)为流动相，流速1.0 mL/min，柱温25℃，检测波长250 nm，同时分离了样品中5'-鸟苷酸二钠和5'-肌苷酸二钠。

When sterilized with 1 000 mg/L chlorine dioxide in finial concentration of 10 ml/m3 for 30 minutes,the dissolution ratio of the total bacterial count was 94.6% and 93.5% while mycetes was 92.1% and 89.6% using the method of knock-on and settling process.

用ClO2 1 000 mg/L浓度10 ml/m3消毒30 min，撞击法及沉降法检测细菌总数消亡率为94.6%、93.5%，真菌消亡率为92.1%、89.6%。

Results showed that urokinase at 20U/ml was the optimal concentration used. Fibrinolysis kinetics and plasma plasminogen concentration of 27 normal persons and 27 patients with acute myeloblastic leukemia were detected, a significant difference was observed between the two groups. Repetition test showed that the coefficience of variation was 5.24±1.51%. This method could also be used to detect the concentration of plasma fibrinogen.

结果 初步建立了正常人纤溶动力学分析参数，确定了20U/ml尿激酶为最适试验浓度，检测22例正常人，27例急性髓细胞白血病患者纤溶动力学及纤溶酶原含量，显示患病组较正常组差异有显著意义(P.05， P.01)，重复性试验显示该方法的变异系数为(5.42±1.51)%，并可同步测定血浆纤维蛋白原浓度。

The molecularly imprinted solid-phase extraction columns were prepared from a 1.0 mL glass syringe packed with 150 mg of the molecularly polymer. The MISPE procedure performed in an off-line mode coupled with reversed-phase high performance liquid chromatography was developed to extract domoic acid from Mytilus edulis and seawater samples.

用150 mg印迹聚合物填充于1.0 mL玻璃注射器制成的分子印迹固相萃取柱，采用离线模式，并结合高效液相色谱实现紫贻贝和海水中软骨藻酸的分离与检测。

Healthy SD male rats were given DEG with the dose of 8 mL/kg body weight (intraperitoneal injection I.P.). The level of the serum Cr, BUN and CO2CP(CO2 Combining Power CO2CP)were tested before and after the injection the 2nd , 5th , 7th, and 14th day. The nephridial tissue of all the rats was taken for pathological examinations.

选用健康雄性SD(Sprague-Dawley)大鼠，腹腔注射8 mL/kg的DEG，于注射前和注射后第2天、5天、7天以及14天尾静脉采血检测血肌酐、尿素氮和CO2结合率(CO2CP)，收集死亡大鼠及第7天和14天处死大鼠的肾组织进行病理检查。

Sixteen patients with terminal cancerous pain received epidural, sacral or neuroplexus administration of MMC 4-8mg(concentration:1-2mg/ml) once a day or every other day, lasting 3-4times and degree of pain relief was evaluated.In different concentration solutions of MMC and normal saline, the pathologic changes of separated nerve of live body in sharp dissection ,immersed for 1-24hours (37℃),was observed under microscope.

16例晚期癌痛病人以1～2mg/ml浓度使用4～8mgMMC行椎管内、骶管、神径丛注射，每日或隔日一次，3～4次，观察止痛效果；采取人离体坐骨神经锐性分段后分别浸泡于生理盐水及不同浓度MMC溶液中1～24小时作切片对比观察其病理损伤程度。

The studies showed that the optimum conditions of the reaction were the amount of the 75% gathers the phosphoric acid 30 mL,the mole ratio ofhexamethylene tetramine to nitrophenol was 2∶1,the reaction time was about 3.0 hours,the reaction temperature was about 105℃.

结果表明较佳反应条件是：在对硝基苯酚为3.5 g的情况下，75%的多聚磷酸用量为30 mL，n∶n=2∶1，反应时间为3.0 h，反应温度105℃，5-硝基水杨醛的产率可达68.1%。

On this basis,a noncircular planetary gear mechanism of 50 mL/r displacement was designed and manufactured.

在此基础上，设计制造了50 mL/r排量的非圆行星齿轮机构。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。