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In the preparation method, zirconium is mixed with benzenephosphonic acid according to the molar ratio of 1:2 to 1:4, and Alpha-zirconium phenyl phosphonate is produced by centrifugal washing after one to five days of crystallization under the temperature of 50 DEG C to 100 DEG C; deionized water is added in order to prepare Alpha-zirconium serosity, the solid content of which is 4 percent to 8 percent; the Alpha-zirconium serosity is granulated and dried by a rotary spray dryer, the feeding speed of the Alpha-zirconium serosity imported into an atomizer is controlled between 20ml/min and 80ml/min, and the temperature of a hot air inlet is controlled between 120 DEG C and 200 DEG C.

本发明涉及一种大比孔容微球α-苯膦酸锆及其制备方法，其颗粒尺寸为10～100μm，比孔容为0.908cc/g，比表面积为125.8m 2 /g；其制备方法是将锆和苯膦酸以摩尔比1∶2～1∶4混合，在50～100℃温度条件下晶化1～5天，离心洗涤得到α-苯膦酸锆；加入去离子水配制α-苯膦酸锆浆液，其固含量为4-8％；将α-苯膦酸锆浆液用旋转式喷雾干燥器进行造粒、干燥，控制α-苯膦酸锆浆液输入雾化器的进料速度为20～80ml/min，控制热风进风口温度为120～200℃；该方法具有操作简单、合成条件温和，对环境污染小等特点，该材料应用于催化、催化剂载体、吸附、离子交换等方面。

Methods A lamellar flap was produced in the rabbit cornea with a microkeratome. The flap interface in whole corneas and corneal beds were soaked in the rAAV –EGFP solution for 10 min, BSS solution was applied in the control group. The corneas were harvested at day 1, 3, 14, and 21 after application for the structure analysis of cornea by HE staining. Expression of the transferred gene was monitored by fluorescence stereoscope and laser confocal microscope. Results After 3d of infection with rAAV-EGFP ,slight fluorescence was detected in rabbit cornea by fluorescence stereoscope .

微型角膜刀制作兔角膜基质瓣；转染组用含rAAV－EGFP转染液浸泡角膜瓣和角膜基质床10 min，对照组用等量BSS液浸泡角膜瓣和角膜基质床10 min，不同时间点(1、3、7、14、21d)通过荧光体视镜观察角膜出现EGFP荧光的起始时间及分布情况，收集角膜，其中一半用激光共聚焦显微镜观察、照相，另一半固定后行HE染色。

By superfusion of ET-1, the hypoxiainduced decrease in RPF was remarkably potentiated (from 136±9 to 48±27 bpm) and the occurrence of pacemaker arrest was shifted to 20±6 min.

在缺氧的条件下持续灌流ET-1（1 nmol／L）20 min时，可显著加重缺氧所致的RPF降低，使起搏细胞的RPF由对照的136±9 bpm降至48±27 bpm（p.01），起搏细胞的停跳时间前移至20±6 min。

Moreover, the protein level of pERK in the ACC was transiently increased after LTP induction, starting at 5 min and returning to basal at 1 h after tetanic stimulation.

取高频刺激后不同时间点的脑片进行免疫组化检测，结果显示，高频刺激后5 min时，pERK 表达显著升高，在10 min达到最高峰，1 h后回复到基础表达水平。

The optimization of heat shock conditions for producing tetraploidy loach was treated the fertilized eggs for 4 min with 41℃ water after fertilization about 20 minutes.

采用热休克抑制受精卵第一次卵裂、Ag-NOR计数鉴定四倍体胚胎的方法，探索了诱发四倍体泥鳅的最佳条件是：在受精后20 min左右采用41℃热水持续处理泥鳅受精卵4 min。

The filtration velocity could be chosen between 1m/min to 8m/min, which is as several times as the normal baghouse.

过滤风速可在1～8m/min之间选取，达常规袋式除尘器的数倍，除尘效率达到99.99％以上。

The results showed that the carbon membranes preoxidized at 460℃,30min,and carbonized at 650℃reached the highest permeability.The permeabilities of H_2,CO_2,O_2,N_2 were 1016.4、710.3、187.8、14.0 Barrer1 Barrer=10~(-10cm~3·cm·cm~2·s~(-1)·cmHg~(-1),respectively.The carbon membranes preoxidized at 460℃,30 min,and carbonized at 850℃reached the highest selectivity.The ideal separation factors of H_2/N_2、CO_2/N_2,O_2/N_2 were 129.2、93.1、21.9、respectively.

结果表明：PPESK前驱体经460℃，30 min预氧化处理，650℃炭化得到的炭膜气体渗透性最佳，H_2、CO_2、O_2、N_2的渗透系数分别达到了1016.4、710.3、187.8、14.0 Barrer1 Barrer=10~(-10cm~3·cm·cm~(-2)·s~(-1)·cmHg~(-1)；经460℃，30 min预氧化处理，850℃炭化得到的炭膜气体选择性最佳，H_2/N_2、CO_2/N_2、O_2/N_2的分离系数分别达到了129.2、93.1、21.9。

METHODS: 10 mL bone marrow was extracted from dog posterior superior iliac spine, heparin anticoagulation, diluted using Hanks juice, treated with 1.077 g/mL Ficoll solution 3 mL, and centrifuged at 2 000 r/min for 20 minutes. Karyocytes were absorbed to form white cloudlike layering interface, and then centrifuged twice using DMEM supplemented with fetal bovine serum, incubated at 12×104/cm2 at 37 ℃ in a 5% CO2 incubator.

于犬髂后上棘抽取骨髓液10 mL，肝素抗凝，Hanks液稀释后，加入1.077 g/mL Ficoll液3 mL，2 000 r/min离心20 min，吸取有核细胞形成白色云雾状的分层界面，用含胎牛血清的DMEM离心2遍，按12×104/cm2密度接种，于37 ℃、体积分数为5%的CO2培养箱内培养。

MethodsSeparation was performed on an Agilent ZORBAX SBC18 (4.6 mm×250 mm, 5 μm) analytical column with mobile phase consisting of acetonitrile and water with gradient elute at the flow rate of 1.0 ml/min and the column temperature 40℃.

色谱柱： Zorbax SBC18柱（250 mm×4.6 mm，5 μm），流动相∶乙腈水，检测波长：203 nm，柱温：40℃，流速：1.0 ml/min，分析时间：90 min。

The tribological behavior of the fluoborate nanoparticles as lubricating oil additive was evaluated by four-ball test machine,where test conditions are following: load 100～ 700 N,rotating speed 1 200 r/min,testing time 10 min.

借助TEM、XRD对表面修饰纳米氟硼酸盐微粒进行了表征，并利用四球摩擦试验机对其用作润滑油添加剂的摩擦学性能进行了评价，试验条件为载荷100~700N，转速1200r/min，时间10min。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。