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Then, PP-g-PVAc granule was saponified to PP-g-PVOH by heterogeneous saponification technique with NaOH/KOH as catalyst in alcohol dispersing medium. During our investigation, some methods to prepare PP-g-PVOH with high saponification percentage were explored.

本文又以PP-g-PVAc为原料，NaOH/KOH为催化剂，探讨并系统研究了利用非均相皂化反应制备高醇解率聚丙烯接枝聚乙烯醇的工艺，并对本文制备得到的两种接枝共聚物PP-g-PVAc和PP-g-PVOH的结构和性能进行了表征。

The interaction between MT and AA was expressed by infrared spectra, the functional groups of -SH in MT had lone pair electrons, which could formπ-πwith -C=O in AA. The equilibrium binding experiment and Scatchard analysis showed, at least three kinds of binding sites would exist when MT-imprinted polymer formed, the most adsorption capacities were 3.3896mg/g, 0.9362mg/g, 1.6583mg/g respectively; most terminal thiolate sulfurs in MT were polymerized as binding sites in the process of polymerization, which could observed from TEM, binding capability of other thiolate sulfurs was weak since spatial hindrance existed.

采用红外光谱研究了加入金属硫蛋白后功能单体丙烯酸官能团谱峰的变化，结果表明金属硫蛋白分子中的-SH与丙烯酸中的C=O在氯仿溶液中能形成π-π键，由聚合物的吸附特性和Scatchard分析可以得出，金属硫蛋白印迹聚合物至少存在三种结合位点，其高、中、低的最大吸附量分别为3.3896mg/g、0.9362mg/g、1.6583mg/g；通过透射电镜可以观察到，金属硫蛋白在聚合过程中主要以分子两端的巯基作为结合位点，不同位置的巯基受到的空间位阻不同，导致产生了三种不同的结合位点。

The main results are:In logic system ,G,tautologies can not be get by using upgrade algorithm to non tautologies within finite many times;In logic system G n,tautologies can be get by using upgrade algorithm to an arbitrary formula of F at most n times; Congruence partitions about on F have been given in logi...

主要结果是：在逻辑系统 G，G中，重言式不可能由对非重言式进行有限次升级算法得到；在逻辑系统 Gn 中，对任一公式最多进行 n次升级算法即可得到重言式；利用可达广义重言式概念和α-矛盾式概念分别在 G，G，Gn 中给出了 F的一个关于同余的分划。

By the study of the influence of urea concentration,reaction time and temperature on the dyeing results and washing fastness,the improved conditions were found as(1) for weak acid red: 90 ℃ dyeing for 60 min with urea 225 g/L;(2) for strong acid yellow: dyeing 50 min at 80 ℃ with urea 250 g/L and NaHSO3 8 g/L.

以尿素为基础对羊毛低温染色工艺进行了初步探讨，研究了尿素浓度、反应温度和反应时间对羊毛染色效果及耐洗牢度的影响，找出了较佳的低温染色条件：①弱酸性红，尿素225 g/L，90℃，60 min；②强酸性黄，NaHSO3 8 g/L，尿素250 g/L，80℃，50 min。

A competitive ELISA kit for detect ENR was developed with ENR mAb and its traits were tested.Two hybridoma lines were filtered and the best one was 4G1-B3,which secreted ENR mAb with indirect ELISA titers of 1∶1.024×10~6 in ascites.Isotype of the two mAb was IgG_1.ENR mAb had a high affinity constant with 9×10~(10)L/mol.The ENR-Kit had the linear detection range of 0.05～101.6μg/L,the sensitivity of 0.05 μg/L and a good sensitivity with an IC_(50) of 1.1μg/L to ENR,cross-reactivity to other compounds less than 0.01%.The average recoveres of ENR spiked in chicken,liver,fish and milk were 81.5%,87.6%,84.3% and 95% respectively.The coefficient variation was below 10%.

结果表明：筛选出的2株杂交瘤细胞，单抗亚类均为IgG1型，其中4G1-B3株的ENR mAb间接ELISA效价为1：1.024×106，亲和常数为9×1010L/mol；竞争ELISA试剂盒的线性检测范围为0.05~101.6μg/L、灵敏度0.05μg/L、半数抑制浓度(IC50)1.1μg/L，与其他化合物的交叉反应率均小于0.01%，鸡肉样、鸡肝样、鱼肉样和牛奶样的平均添加回收率分别为81.5%8、7.6%、84.3%和95%，不同基质添加恩诺沙星标准品做竞争ELISA对ENR-Kit检测结果影响小，试剂盒保存期6个月以上。

The average peak time values of berberine nanoemulsion (4.205 h) enhance 2.826 h,3.088 h than tablet(1.379 h) and capsule(1.117 h).The average highest plasma concentration of its (113.699μg/L)is 1.820,1.894 times of ablet (62.466μg/L)and capsule(60.021μg/L), The relative bioavailability is339% and 332% that of tablet and capsule.

黄连素纳米乳的平均达峰时间Tmax(4.205 h)比黄连素片剂(1.379 h)和黄连素胶囊(1.117 h)延长2.826 h和3.088 h；其理论的平均最高血药浓度Cmax(113.699μg/L)是黄连素片剂(62.466μg/L)和黄连素胶囊(60.021μg/L)的1.820倍和1.894倍；其相对生物利用度是黄连素片剂和黄连素胶囊的339%和332%。

Results The observation from HE stain showed the most toxic effect of HCT-8 cells at 800μg/ml for 8h. The toxicity of HCT-8 cels in each experiment group(25~800μg/ml)was higher than that of matched control except 12.5%μg/ml.

结果 HE染色显示，当ABF浓度为800μg/ml时，HCT-8细胞的毒性作用最大，除浓度为12.5μg/ml的实验组，各实验组(25~800μg/ml)的毒性均高于对照组。

Results:Compared with the oil group, the concents of serum MDA were decreased significantly in 0.4 g/ group, and the energy of serum SA was increased significantly in 0.134 g/ and 0.4 g/ groups.

肝组织中脂褐质含量？结果：0.4 g/组大鼠血清中MDA含量显著低于对照组， 0.134 g/？0.400 g/组大鼠血清中SOD活力显著高于对照组？

Difference of cell-free DNA concentrations was analyzed by one-way analysis of variance using SPSS 10.0 software. There is a significant difference if p value was less than 0.05. The results showed that: 1 DNA concentrations in cell-free lavages supernatants in central lung cancer, peripheral lung cancer and pulmonary benign lesions are (0.83±0.34)μg/ml,(0.66±0.31)μg/ml and (0.59±0.37)μg/ml, respectively.

研究结果如下： 1中心型肺癌支气管灌洗液上清游离DNA量为(0.83±0.34)μg/ml，周围型肺癌为(0.66±0.31)μg/ml，肺部良性病变为(0.59±0.37)μg/ml，经单因素方差分析发现三者支气管灌洗液游离DNA量没有显著差异。

Sowe selected the colchicine optimum parameters were 0.6μg/ml and 6 hour culturedduration.The second, there were no significantly differences between the four groupsin 2 hour groups; and there were significantly differences between 0.2μg/ml groups and other three groups in 4 hour groups; and there were no significantlydifferences between the four groups in 6 hour groups; and there were significantlydifferences between 0.4μg/ml groups and other three groups in 8 hour groups onthe metaphases (P＜0.05), in the experiment of the effect on the mouse 8-cellembryo stage single blastomere of colchicine with different concentrations andduration by x~2 statistical analysis.

根据实验的实际情况，适宜制备小鼠4-细胞期胚胎单卵裂球染色体标本的秋水仙素的处理浓度和时间是0.6μg／ml和6小时。2、在确定秋水仙素不同处理浓度和时间对小鼠8-细胞期胚胎单卵裂球中期分裂相数影响的实验中，经统计分析，阻断培养2小时组中四个浓度组差异均不显著；阻断培养4小时组中0.2μg／ml浓度组与其他三组差异显著；阻断培养6小时组中四个浓度组差异均不显著；阻断培养8小时组中0.4μg／ml浓度组与其他三组差异显著(P＜0.05)。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。