查询词典 Ehrlich preparation

First, a chlorinator was self-designed in this paper, and dichloride of 2-methyl-1-propene was synthesized by 2-methyl-1-propene reacted with chlorine fast in this reactor. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield and selectivity of dichloride of 2-methyl-1-prop-ene were more than 65% and 80% respectively. Second, the preparation of 2-methylene-1, 3-propanediol, which dichloride of 2-methyl-1-propene reacted with alkali was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the conversion of dichloride of 2-methyl-1-propene was 100%. Moreover the preparation of MPO, which 2-methylene-1, 3-propanediol reacted with hydrogen, in presence of Al_2O_3-Pd catalyst, was gotten, and the product was appraised.

本文在氯化反应过程中，自行设计制作出了氯化管式反应器，在该反应器中异丁烯和氯气迅速混合反应生成二氯异丁烯，根据该氯化反应特征利用正交试验和单因素试验考察了有关因素的影响并优化得到了最佳工艺条件，二氯异丁烯的总收率达65％以上，选择性达80％；接着，对二氯异丁烯进行水解反应制得了2-甲烯-1，3-丙二醇，讨论了相关因素对水解反应的影响，并通过正交试验和单因素试验得到了较佳工艺条件，二氯异丁烯的转化率达100％；同时还对制备的2-甲烯-1，3-丙二醇在常压下采用三氧化二铝负载钯催化剂催化加氢得目的产物MPO，并对产品进行了鉴定，从而打通了整个工艺路线。

The combinatorial preparation method based on wet impregnating was validated an effective and precise tool for preparation of supported catalysts.

论文将多相催化剂的组合制备和高通量筛选作为整体进行考虑，并且建立了相应的方法。

Ft Interior Volume Rear: 38.0 cu. ft Luggage capacity: 13.7 cu. ft Performance 0-50 mph (0-80 kmh): n/a 0-60 mph (Manual / Auto): 7.8 / 9.0 sec (7.8 sec / 9.6 sec. quattro) 1/4 Mile: n/a Top estimated speed: 130 mph (203 kmh)- Electronically limited for North America Fuel Economy City (Manual/Auto): 19 / 18 mpg (19 / 18 mpg quattro) Highway (Manual/Auto): 27 / 28 mpg (26 / 27 mpg quattro) Combined (Manual/Auto): 23 / 23 mpg (22 / 21 mpg quattro) Standard Features Comfort/Convenience:· Electronic automatic climate control system, including air conditioning · Power steel sunroof · Power windows with one-touch down, lock-out for rear windows, pinch protection and one-touch up for front windows · Retained accessory power for windows and sunroof · Tinted glass, banded windshield · Power rack and pinion steering · Convenience close feature for windows and optional sunroof · Electronic cruise control with resume and speed up features · Dual power mirrors with defog feature · Electric rear window defogger · Power central locking system including trunk and fuel door; selective unlocking · Heat ducts to rear seat area · Illuminated glove box, trunk, lighter/ashtrays, engine compartment · Ignition key with integral light · Dual illuminated vanity mirrors · 4-passenger assist handles · Time delay interior light · Anti-theft vehicle alarm system · Cupholders · Fuel cap hanger feature Interior/Seating and trim:· 8-way power front seats with manual lumbar adjustment · Front seat map pockets · Facette weave cloth · Leather-wrapped steering wheel · Fold down rear-center armrest with storage container · Rear center armrest · Full length center console with forward storage bin, including cupholders · 60/40 split/fold rear seat with locking seat back · Genuine burled walnut wood trim for dash, door panels and console · Front and rear carpet floor mats Instrumentation:· Backlit instrument cluster, red illumination · Tachometer and electric speedometer · Analog clock · Outside temperature gauge · Trip odometer · Coolant temperature gauge · Oil temperature gauge · Voltmeter · Intermittent wiper mode Audio Systems:· AM/FM stereo cassette radio with anti-theft · 6-speaker sound package · Rear window antenna · Preparation wiring for CD changer · Preparation for cellular phone Exterior:· Aerodynamic 3-way halogen headlights · 5 mph bumpers, painted in body color · Body color, protective side moldings · Retractable headlight washer system · Body color, flush door handles · Body color, outside mirror: right convex, left side flat · Front fog lights · Rear fog light (integrated with left light cluster) Safety:· Anti-lock brake system · Driver and front passenger air bag supplemental restraints · Automatic self-tensioning front seat belt system · Rear outboard 3-point seat belts with comfort adjustment · Rear center lap safety belt with retractor · Child-safety rear door locks

1 / 4 mile ：无/ 1 顶端估计速度：一百三十零英里每小时-电子有限公司，为北美洲燃油经济性市： 19 / 18哩（ 19 / 18哩quattro的）公路： 27 / 28哩（ 26 / 27哩quattro的）结合： 23 / 23哩（ 22 / 21哩quattro的）标准功能舒适/方便：·电子自动气候控制系统，包括空调·电源钢天窗·电源的Windows与一触式下降，锁定为后方的Windows ，夹保护和一触式，为前线的Windows ·保留配件权力for Windows和天窗·有色玻璃，带状挡风玻璃·电源机架和齿轮督导·方便接近的特点，用于Windows和可选的天窗·电子巡航控制与恢复，并加快特色·双电源镜与defog功能·电动后窗defogger ·电源中央门锁系统，包括主干和燃料的大门；选择性解锁·热导管后座区·照明手套箱，躯干，打火机/烟灰缸，引擎·点火的关键与积分光·双发亮的虚荣心镜· 4名乘客协助处理·时间延迟内部轻·反盗窃车辆报警系统· cupholders ·燃油上限吊架功能内部/座位和修剪：· 8路的权力前排座椅手动腰调整·前座地图的口袋· facette编织布·皮革包裹方向盘·折叠后方中心扶手与储藏容器·后方中心扶手·充分的长度中心控制台与储存着斌，包括cupholders · 60/40分裂/倍后座锁定椅背·真正的burled核桃木材装饰为短跑，车门面板和控制台·前方和后方，地毯，地板垫仪器仪表：·背光文书集群，红色照明·转速表和电动里程表·模拟时钟·室外温度衡量·行程里程表·冷却液温度衡量·油温计·伏特·间歇雨刮模式音频系统：·调幅/调频立体声收音机，镭射与反盗窃· 6喇叭声包·后窗天线·准备布线的CD换·准备蜂窝电话外墙：·气动3路卤素头灯·五英里每小时保险杠，描绘了在体色·车身颜色，保护方成型·可伸缩的头灯清洗系统·车身颜色，冲水门把手·车身颜色，外镜：右凸，左侧单位·前雾灯·后方雾轻安全：·汽车防抱死制动系统·司机及前座乘客安全气囊的补充约束·自动自我拉紧前座安全带系统·后方的舷外3点安全带与舒适性调整·后方中心濸安全带与retractor ·儿童安全后门的锁

Major content of this work includes five aspects as follows:(1). Oxygen sensitive materials had been prepared by carrier covalence method, and the preparation mechanism of the materials had been investigated by FI-IR, SEM, and the detection experiment of oxygen. Then through the detection of oxygen, the sensitivity and stability had been estimated, and it was studied that the properties of materials would be affected by the various factors.(2). Oxygen sensitive materials had been prepared by carrier covalence-cross linking method, and the preparation mechanism of the materials had been investigated by FI-IR, SEM, and the detection experiment of oxygen. Then through the detection of oxygen and spectrophotometer, the sensitivity and stability had been estimated, and it was studied that the properties of materials would be affected by the various factors.(3). For the detection of gaseous oxygen, the fiber optical sensor on basis of oxygen sensitive materials had a respond time of 10s, detection limit of 5ppmand detection precision of 0.5%. The sensor had good repeatability and stability, a less delay and at least 1 year life-span.

本论文主要包括以下五个方面的内容：(1)载体共价法制备氧敏感材料：通过红外光谱、扫描电镜图谱和氧测试实验探讨该氧敏感材料的制备机理，通过氧测试实验评价该氧敏感材料的氧敏感性和稳定性，同时研究了各种因素对该氧敏感材料性能的影响(2)载体共价—交联法制备氧敏感材料：通过红外光谱、扫描电镜图谱和氧测试实验探讨该氧敏感材料的制备机理，通过氧测试实验和分光光度计评价该氧敏感材料的氧敏感性和稳定性，同时研究了各种因素对该氧敏感材料性能的影响(3)氧敏感材料在光纤气态氧传感器中的应用：该传感器的响应时间为10s，检测下限为5ppm，检测精度为0.5％，具有较好的重复性和稳定性，迟滞较小，使用寿命至少为1年，适合各种环境下气态氧浓度的检测。

A preparation method of monodisperse high crystallinity copper powder is provided, which relates to a method for preparing copper powder used in conductive paste by using cupreous compound, in particular to a preparation method of the copper powder used in the conductive paste that is applicable to ceramic electronic components with a plurality of layers.

一种单分散高结晶度铜粉的制备方法，涉及用铜的化合物制备导电浆料用铜粉的方法，特别是涉及适用于多层陶瓷电子元件的导电浆料用铜粉的制备方法。

The research and development of CWM preparation with flotation tailings and combustion in FBC boiler for power generation in Pangzhuang Preparation Plant are in- troduced in this paper.

介绍了庞庄煤矿利用浮选尾煤制水煤浆沸腾炉燃发电的研究开发过程，找出了一条解决煤泥综合利用的新途径，并具有良好的推广应用价值。

The paper mainly studies the new preparation technologies of cyanamide. The paper reviews the preparation technologies of cyanamide in domestic and overseas. We analyze the advantage and disadvantage of all the technologies, and we design two new technologies: urea- cyanamide method and ammonia, carbon dioxide- cyanamide method.

本文主要研究了制备氰胺的新工艺，综述了国内外氰胺工业生产的几种主要工艺，分析了各工艺的利弊，设计了两条新的工艺路线，即尿素-氰胺法和氨气、二氧化碳-氰胺法。

The preparation of polymer is required for high purity of glycolic acid, if not, low-weight polymer is obtained, therefore, high purity glycolic acid is scarce in the market. So, the research for the synthesis of glycolic acid is essential. In domestic and overseas, there are many methods for preparation of glycolic acid, including glycin oxidation, cyanogenesis, aldehyde oxidation, coupling of maldehyde and methyl formate, oxalic acid electrolysis, chloroactic acid hydrolysis and so on.

制备羟基乙酸的聚合物时，对羟基乙酸单体的纯度要求较高，否则得到的聚合物分子量较低，导致高纯度羟基乙酸的需求量逐年增长，目前在国内，高纯度的羟基乙酸还没有形成工业化规模生产，对羟基乙酸的合成进行研究是非常有意义的。

Component: Pure water, Cymene, Active Surface Chemical Preparation, Anlistatig Chemical preparation etc

成份：纯净水，异丙醇，进口表面活性剂，抗静电剂等。

This specific preparation methods including: parathion of the initial reaction in acid and zinc metal in the common under redox reaction, a product of the reduction of parathion - parathion, with the sodium nitrite in the cold under diazotization reaction, and bovine serum protein tyrosine on the o-hydroxy combination of the adult immune original and immune rabbit polyclonal antibody preparation.

本发明制备方法具体包括：以对硫磷为反应初始物，在酸和金属锌的共同参与下进行氧化还原反应，得对硫磷还原产物对氨基对硫磷，再与亚硝酸钠在低温下进行重氮化反应后，与牛血清蛋白酪氨酸上羟基的邻位结合，制备成人工免疫原，并免疫新西兰大白兔制备多克隆抗体。

The work of this paper is as follows: 1. Looking back the progressing history of the linear motor, introducing the features of the elevator driven by linear induction motor, radicating the topic of this paper "the digital frequency variable control of the elevator bi-side direct driven by linear induction motor". The research of this paper covers the conventional VVVF control, space vector based VVVF control, vector control and DTC.

本文主要开展了以下几个方面的工作： 1 回顾了直线电机发展历史，电机的驱动技术演变，特别是针对直线电机的驱动，简要介绍了直线感应电机驱动电梯的优点和不同结构类型，对传统的v／f控制，基于空间矢量法的v／f控制，矢量控制，和基于电压空间矢量的直接转矩控制进行了比较，确立了本课题的研究主题：直线感应电机双边直推式驱动电梯的全数字变频控制。

The article combines with the treatment of a superficial civil air defense work to introduce how the grouting method to improve the performance of the backfill soil.

文章从治理漂浮人防工事的角度提出了注浆技术在改善回填土性质方面的应用，并详细阐述了注浆技术的施工流程。