查询词典 Dinitro

Main production sulfide Green, Chloropicrin, picric acid, dinitro-chlorobenzene, potassium chlorate, high sodium chlorate, ammonium perchlorate, such as more than 30 kinds of products, exports of Asia and Europe more than 30 countries and regions. In 2000 through ISO9002 quality system certification, production scale, cost-effective, enterprise management, technological advancement, product quality, environmental protection are rising, has very broad prospects for development.

主要生产硫化青、氯化苦、苦味酸、二硝基氯化苯、氯酸钾、高氯酸钠、高氯酸铵等30多种产品，出口亚欧30多个国家和地区。2000年通过ISO9002质量体系认证，生产规模、经济效益、企业管理、技术进步、产品质量、环境保护均不断提升，具有十分广阔的发展前景。

P28 紫色 Formation of a peptide bond 肽键形成–4侧链具有的反应–形成二硫键-其它反应 Tyr,His,Arg Review Isoelectric Point Titration滴定 of an amino acid 滴定 Gly幻灯片 18 His Lys Glu Reaction of amino acids Section 4 Protein isolation and purification 蛋白质分离及提纯 Working With Proteins Experimental techniques for protein analysis and characterization Purification steps A cell contains many types of proteins In the lab we want to isolate a single protein for experiments Purification steps We first grow cells or isolate tissues that contain the protein of interest We break open the cells to produce a crude extract Use centrifugation离心 to separate soluble from insoluble material We fractionate 分离 the protein mixture based on properties of such as size, charge affinity or solubility.

丹磺酰氯与氨基酸反应生成荧光性质强和稳定的磺胺衍生物，用于多肽链NH 用于多肽链 3末端氨基酸的标记烃基化反应(1) 2，4-二硝基氟苯2，4-dinitrofluorobenzene，二硝基氟苯(二硝基氟苯 DNFB也叫做试剂。DNFB在弱碱性溶液也叫做Sanger试剂试剂中与氨基酸发生取代反应，生成黄色化合物二硝基二硝基苯基氨基酸(dinitro phenyl amino acid， DNP氨基酸氨基酸)苯基氨基酸氨基酸(2)苯异硫氰酸酯(phenylisothiocyanate， PITC)在弱碱性条件下，与氨基酸反应在弱碱性条件下，生成苯乙内酰硫脲 PTH衍生物，(phenylthiohydantoin， PTH)衍生物，即PTH-氨基酸，此反应又称之Edman反应，该反应是蛋白质或多肽氨基酸序列测定常用的反应。

A quantum chemistry calculation for the crystal structure of 4- benzaldehyde-2,4-dinitro phenyl hydrazone was performed by using Gaussian98 with B3LYP/6-31G basis sets.

利用Gaussian98程序，采用密度泛涵方法(B3LYP/6-31G)对4-苯甲醛缩-2，4-二硝基苯腙化合物的晶体结构进行了量化计算，利用相关参数推测了它的分子特性，结果表明，该化合物的分子结构为一大平面结构，难与金属形成配合物

We focused the study on the synthesis methods of quinoxaline, nitration of its aromatic ring and chlorination of its heterocycle. In this paper, we thought about environmental protection, the cost of material, the feasibility of industrialization, workup easily, and obtained 2,3(1H,4H)-quinoxalinedion, 6-nitro-2,3(1H,4H)-quinoxalinedion, 6,7-dinitro-2,3(1H,4H)–quinoxalinedion, 2,3-dichlo- roquinoxaline, 6–nitro-2,3-dichloroquinoxaline,and 6,7- initro-2,3-dichloro-quinoxaline. A more reasonable, easily, efficient and simple reactive route to synthesize above-mentioned compounds was developed by systematically investigating the yield, the purity and physical character of intermediates.

本文针对喹喔啉及其芳环硝化、杂环氯代的合成进行研究，主要考虑了环保性、原料成本、产业化的可行性、反应操作的简便性等问题，获得了2，3(1H，4H)-喹喔啉二酮、6-硝基-2，3(1H，4H)-喹喔啉二酮、6，7-二硝基-2，3(1H，4H)-喹喔啉二酮、2，3-二氯喹喔啉、6-硝基-2，3-二氯喹喔啉和6，7-二硝基-2，3-二氯喹喔啉等六个中间体，考察了反应产物的产率、纯度和性状等因素，得到了更为合理、方便、实用、简洁的可供产业化的合成路线。

In this research, the activities of CWDE were measured by saccharifying according to the theory that red-brown amino compounds were produced when 3, 5-dinitro salicylic acid and aldehyde were heated together. And the testing conditions were made clear. The activity of Cx should be tested with optimal temperature of 50℃, optimal pH of 4.8, incubation time of 30 min, and optimal substrate of 0.6% CMC-Na. Due to the heat-libality, Cx should be sterilized more than 10 min. The testing conditions of the activity ofβ-G were almost the same with Cx except the substrate of 0.5% salicin and the sterilization time of more than 15 min.

主要取得了一下成果：(1)明确了条锈菌细胞壁降解酶活性测定的条件：羧甲基纤维素酶活性的测定条件为50℃，pH4.8，反应时间30min，底物浓度为0.6%羧甲基纤维素钠，以DNS法测定，且失活酶液的灭活时间应大于10min；β-葡萄糖苷酶活性的测定条件为：50℃，pH4.8，反应时间30min，底物浓度为0.5%水杨苷，以DNS法测定，且失活酶液的灭活时间应大于15min；果胶酶活性的测定条件为：50℃，pH4.8，反应时间1h，底物浓度为0.25%果胶，以DNS法测定，且失活酶液的灭活时间应大于10min。

According to the structure and synthesis character of the geminal dinitro energetic plasticizers,the current situation about the synthesis,the property and application of geminal dinitro aldehyde acetals,esters and ether energetic plasticizers is summarized with 21 references.

从偕二硝基含能增塑剂的结构和合成特点出发，综述了偕二硝基缩醛类、酯类及醚类等含能增塑剂的合成、性能及应用研究现状。

Aromatic dinitro compounds were reduced irrespective of the presence or absence of β-CD in sodium hydroxide solution, which revealed particularity of aromatic dinitro compounds.These reactions have advantages below over past research results of aromatic nitro compounds:(1) The synthetic method using water as the reaction medium may

这些反应与过去人们对硝基化合物反应的研究结果相比，具有以下优点：(1)反应在水介质中进行，避免使用辅助有机溶剂和金属催化剂，是环境友好的清洁反应，比较符合绿色化学的发展要求；(2)反应中所用的β-环糊精无毒，价廉，易得

Hydroxy-5, 10-dihydrophenophosphazine 10-oxide (1) reacted with SOCl2, and then with MeONa in MeOH to give a methyl phosphinate (2) which can be converted to a dinitro compound 3 (62%) by nitration and the resulting dinitro compound 3 can further be converted to 2, 8-diamino-10-methoxy-5, 10-dihydrophenophosphazine 10-oxide (4, 71%) by hydrogenation over Pd/C (w = 0.05). And the effect of amount of Pd/C (w = 0.05) on the reduction was also studied.

10－羟基－5，10－二氢磷杂吖嗪－10－氧化物（1）经醯氯化、甲基化得到10－甲氧基－5， 10－二氢磷杂吖嗪－10－氧化物（2），2经硝化得到10－甲氧基－2，8－二硝基－5，10－二氢磷杂吖嗪－10－氧化物（3，62%）。3在Pd／C（w = 0.05）存在下，用氢气还原为2，8二氨基－10－甲氧基－5，10－二氢磷杂吖嗪－10－氧化物（4，71%），考察了Pd／C（w = 0.05）用量对氢化还原反应的影响。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料，先将二酚与碳酸钾成盐，甲苯带水回流反应，然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体；再以二硝基单体，铁粉，HCl为原料，乙醇和水做溶剂，回流反应、乙醇重结晶，得到含氟芳香二胺基单体。

The cesium fluoride-mediated N,N-diarylation of 4-(biphenyl-4-oxy)aniline with 4-fluoronitrobenzene and subsequent reduction of the dinitro intermediate led to a new triphenylamine-based diamine monomer, 4,4'-diamino-4-(biphenylyl-4-oxy)triphenylamine.

以氟化铯为媒介将此苯胺与 4-fluoronitrobenzene 进行芳香族亲核取代反应，随后再进行dinitro中间体的还原反应，制得ㄧ种新型具有三苯胺结构的芳香族二胺单体4，4'-diamino-4-(biphenylyl-4-oxy)triphenylamine。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失