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1 Heptane, it was revealed that the Cr〓/ Catsan and ZnCl〓 could catalyze the Michael addition of pyrrole with conjugate olefine at α-position of pyrrole to get mono- or bi-Michael addition product selectively under mild condition in good yield. Totally, forty-six new compounds, including thirty target compounds, were prepared.

在探索7-氮杂桥环母体的构建方法过程中，发现了Cr〓／Clay和ZnCl〓可有效地催化吡咯的α-位与多种共轭烯烃发生Michael加成反应，可在温和的条件下，以良好的收率选择性地得到单或双Michael加成产物。

As to Gd/Cr system,alower deposition rate of the Gd overlayer〓favors the smooth growth of Gd/Crinterface.

结果表明，低的Gd沉积速率(1.0〓/min)有利于Gd/Cr界面的平滑、均一的生长。

Based on the failure analysis of hot roll, this paper optimizedly adjusts alloy system and summarizes the experience of rolling wiresand improves ail processing properties. Then, it analyses the effects on some natural parameters such as alloy transfer coefficient, surfacing layers, welding current and arc voltage etc.. It confirms the fitting ageing technique. Also, it discusses the microscopic structural transformation back and forth ageing and the effects on hardness change of overlaying metal by some alloying elements including C, Cr, V, W, Mo, Ni, Mn, B, Re through OM, SEM and X-ray diffraction analyses. Finally the abrasive resistance, red hardness, thermal fatigue property and anti-high temperature oxidability are investigated in experimentation.

全文在热轧辊失效分析的基础上优化调整合金体系，总结了焊丝轧制的经验，改善各种工艺性能，分析了几个特性参数的影响，确定了适宜的时效工艺，并通过光学显微镜、扫描电镜和X-射线衍射对时效前后的显微组织转变以及部分合金元素如C、Cr、V、W、Mo、Ni、Mn、B、Re对堆焊层硬度变化的影响进行分析，最后通过试验考察了堆焊层金属的耐磨粒磨损性能、红硬性、耐热疲劳性和抗高温氧化性。

From the results,it was shown that there existed Cr,O and Sn in the passivation film.

结果表明，钝化膜中主要含有Cr，O，Sn元素。

Dissimilar metal welds between the austenitic stainless steel and Cr-Mo pearlitic heat-resistant steels are widely used in ...

国内外石油化工装置和电站的高温压力容器管线及锅炉蒸汽管道等大量使用Cr-Mo类珠光体热强钢。

The same procedure was carried out 14 days later. Results The temperature of inferior segment of esophagus was significantly increased at 60min. The temperature of physic liquor was significant higher than that of perfusion. The temperature of perfusion was becoming significantly increased at 5min (P.05). The WBC, PLT, ALT, AST, Cr and CO2CP of preoperative and postoperative had no significant changes. Only lightly peritoneum dropsy and infiltrate slight phlegmasia were observed postoperatively and 14 days later. There were no significant differences among groups.

结果 在60min时食道下段温度显著升高，灌注温度明显高于抽取温度，抽取温度5min时开始升高(P.05)；各组术前和术后WBC、PLT、ALT、AST、Cr和CO2CP无明显变化，组间比较也无明显差异；术后和术后2wk腹膜均见轻度水肿、少量的炎细胞浸润；吻合口见黏膜层有小溃疡形成，表面有渗出，组间无明显差异。

Based on the above experiments, the author studied the mixed metallic pillared and modified montmorillonites. The experimental result indicated that the microporous structure of Fe-Al-PLMs was affected by the changing of interlayer Fe-Al polymer with different Fe/Al ratio. But the presence of Al iron was helpful to incorporate Fe iron into interlayer of montmorillonites.. Introducing Zr helped Al-PLMs getting better larger spacing, thermal stability, surface area and pore volumes. Its successful to apply Zr-Al-PLMs to treat wastewater containing Cr iron. The experiment of modifying Al-PLMs by PVA showed that the order of adding starting materials (Al-pillaring solution, PVA, montmorillonite solution) was related to the property of Al-PLMs. The PVA as precursor was beneficial for Al to go into interlayer of the clay and to form larger basal spacing porous clay. The surface area and pore volumes of Al-PLMs increased mainly because of increasing the external surface area and mesoporous volumes after acid-activating. This conclusion confirmed that the microporous structure of pillaring clay depends upon the interlayer pillar.

实验结果表明：在Al-PLMs中引入Fe离子，不同Fe／Al比制得的Fe-Al-PLMs因层间的Fe-Al聚合离子结构不同而影响其微孔结构，但羟基Al离子的存在有利于Fe离子进入蒙脱石层间；在Al-PLMs中引入Zr离子，有助于其层间距、比表面积、孔体积增大，所得Zr-Al-PLMs应用于含Cr废水处理效果显著；PVA改性后的Al-PLMs其物化性质变化与铝柱化剂、PVA溶液、蒙脱石溶液三者不同添加顺序有关，说明PVA的前撑有利于Al进入蒙脱石层间得到较大层间距的Al-PLMs；经酸化处理得Al-acid-PLMs，其比表面积增大以外表面积为主，孔体积增大以中孔为主，这也证实了柱撑蒙脱石的微孔结构取决于其层间的柱化物。

Extensive soil sampling of the crop-reclaimed Mn mine wastelands was conducted in the six typical manganese minelands (Bayi, Lipu, Pingle, Quanzhou, Bansu and Xialei) in Guangxi, China. In the six reclaimed minesoils, the heavy metal concentrations were Pb 41.63~348.31 mgkg^(-1), Cr 48.12~287.29 mgkg^(-1), Zn 47.38~269.92 mgkg^(-1), Cu 12.71~138.03 mgkg^(-1), Cd 0.73~46.50 mgkg^(-1), and Mn 676.7~41996.4 mgkg^(-1) respectively.

对广西八一、荔浦、平乐、全州、板苏和下雷6个锰矿食用农作物恢复区土壤重金属进行含量测定，结果表明，土壤各元素含量为：Pb 41.63~348.31 mgkg^(-1)、Cr 48.12~287.29 mgkg^(-1)、Zn 47.38~269.92 mgkg^(-1)、Cu 12.71~138.03 mgkg^(-1)、Cd 0.73~46.50 mgkg^(-1)、Mn 676.7~41996.4 mgkg^(-1)。

The floatation rate of Pd (superscript 2+) reaches 100% when the concentrations of NaNO3, KBr and cetyl pyridinium bromide in solution are 0.05 g/mL, 3.0×10^(-2) mol/L, 5.0×10^(-4) mol/L(pH 4.0), respectively. Pd (superscript 2+) could be separated from Ru (superscript 3+), Al (superscript 3+), Cr (superscript 3+), Ni (superscript 2+), Ga (superscript 3+), Fe (superscript 3+) and Zn (superscript 2+) by floatation quantiatively. A method of flotation separation and enrichment of Pd (superscript 2+) was established.

当溶液中硝酸钠、溴化钾、溴化十六烷基吡啶的浓度分别为0.05 g/mL，3.0×10^(-2)mol/L，5.0×10^(-4)mol/L，在pH 4.0时，Pd(上标 2+)的浮选率达到100%，Pd(上标 2+)可与Ru(上标 3+)，Al(上标 3+)，Cr(上标 3+)，Ni(上标 2+)，Ga(上标 3+)，Fe(上标 3+)，Zn(上标 2+)定量分离，据此建立了浮选分离和富集Pd(上标 2+)的新方法。

All companies in Thailand in early 2002 that a 'high-tech world, as China's first China Aerospace Group / Houston hospital / yellow rope lead the entire group radiation center Thai Plant, in full production, pyrocondensation Casing has approved UL / cUL International Security Certification, the industry took the lead at home and abroad by SGS comprehensive test: lead Pb, Cd Cd, mercury Hg, hexavalent chromium Cr, PBB PBBS, PBBs ether PBDES.

全泰公司于2002年初在著称'世界高科技、中国第一照的中国航天集团/中国火箭院/中国黄缆集团辐照中心筹建全泰二厂，已全面投产，热缩套管已通过UL/cUL国际安规认证，国内外同行业率先全面通过SGS测试：铅Pb、镉Cd、汞Hg、六价铬Cr、多溴联苯PBBS、多溴联苯醚PBDES。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。