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Double chain naphthyurea/thiourea piperazine derivatives complex with linear dicarboxylate anions with a high stability constant and 1∶1 stoichiometry of the complex-and the complex was formed through six hydrogen bonds.2 Photophysical behaviors and anion binding of three N,N-dimethylaminochalcone derivatives were studied.

二研究了三种N,N-二甲基氨基查耳酮衍生物的光物理行为及与阴离子的结合能力。4'位不同的取代基-氨基和苯脲基对查耳酮的的分子内电荷转移能力有一定的影响,它们减弱了查耳酮衍生物的分子内电荷转移能力,导致发射光谱蓝移。

A kind of intramolecular charge transfer compound——3 methoxy 4' N,N dimethylamino flavone derivateves was used to detect collagen association in aqueous solution.

利用一种分子内电荷转移化合物3-甲氧基-4'N,N-二甲氨基黄酮作为荧光探针,研究了胶原蛋白在水溶液中的聚集状态。

The mobile phase was a mixture of acetonirile-40 mmol·L~(-1) dipotassium hydrogen phosphate solution40∶60,containing 10 mmol·L~(-1 cetrimonium bromide, adjust pH to 7.5 by phosphoric acid and the flow rate was 1.0 mL·min~(-1),with the detection wavelength at 215 nm.

结果马来酸、叶酸和依那普利之间能够达到很好分离;马来酸依那普利的线性范围为202.5~810.0 mg.L-1,r=0.999 8(n=6),平均回收率为99.91%,RSD=1.15%(n=9);叶酸的线性范围为16.28~65.12 mg.L-1,r=0.999 8(n=6),平均回收率为100.11%,RSD=1.20%(n=9)。

Subcordiformis in Huanghai Sea near Dalian, it can be able to evolve H〓 photosynthetically. Comparing with Chlamydomonas reinhardtii in our lab, the H〓 productivity is same. By the elementary macro regulation of H〓 production with 2, 5-dibromo-3-methyl-6-isopropyl-p-benzoquinone , N, N'-dicyclohexylcarbodiimide , 3-(3, 4-dichlorophenyl)-1, 1-dimethylurea , sodium dithionate, sulfur-deprivation and cell immobilization, the results show that DCCD, immobilization and sulfur-deprivation has a positive effects on the H〓 production.

利用DCCD(质子泵抑制剂N,N'-dicyclohexylcarbodiimide)、DBMIB(光合电子传递抑制剂2,5-dibromo-3-methyl-6-isopropyl-p-benzoquinone)、DCMU[PSⅡ光合放氧抑制剂3-(3,4-dichlorophenyl)-1,1-dimethylurea]、连二亚硫酸钠、无硫调控及固定化扁藻等手段,对该扁藻产氢进行初步的宏观调控,发现DCCD的加入、扁藻的固定化和无硫调控对产氢均有正效应,其中无硫调控使扁藻产氢时间延长,总产氢量提高了近10倍。

For the reaction between divinyl sulfone and N-ethylethylene-diamine or N-methylpropane-1, 3-diamine , no cross-linking occurred when the feed ratio of A〓 to BB'〓 was 1/1. When the feed ratio of DV to NDA or NPA is 3/2, no cross-linking occurred too in organic solvents such as DMSO, DMF and NMP, while cross-linking does occur in water.

对于二乙烯基砜与N-乙基乙二胺或N-甲基-1,3-丙二胺的反应,当加料配比为1/1时,反应在水和有机溶剂中不会凝胶;当配比为3/2时,反应在有机溶剂中亦不凝胶,而在水中反应时,会经过一种&假凝胶&过程,并最终发生凝胶。

The main contributions are as follows:(1) The decoherence suppression of N level Markovian systems is investigatedby the optimal control in the coherence vector representation. The N level Markoviansystem can be described by the master equation, and possesses a standard bilinear formin the coherence vector representation.

本论文利用密度矩阵相干向量表示研究了退相干效应的抑制和相应的纠缠控制问题,论文主要工作包括:(1)在密度矩阵相干向量表示下,利用最优控制研究N能级Markov系统的退相干抑制问题。N能级Markov系统可以用主方程模型描述,在相干向量表示下具有标准的双线性形式。

The cannas natural antistaling agent is separated by column separation methods and recrystallization. Fraction Ⅱ-2 is analyzed by GC-MS. Three compounds which are n-Octadecane, n- Heptacosane and Decanoic acid heptyl ester were identified.A new way of litchi preservation is provided in this paper.

本论文还对此美人蕉天然保鲜剂进行了分离研究,先对其乙醇提取物进行柱层析粗分,然后对组分Ⅱ进一步细分,对其中的组分Ⅱ-2进行了GC-MS分析,鉴定出3个物质,它们分别是正十八烷(n-Octadecane)、正二十七烷(n-Heptacosane)和癸酸庚酯。

The invention relates to a synthesis method of N-acetylaminoglucose, which comprises dissolving D-glucosamine hydrochlorate and alcohol at the mass ratio of 2-2.5:100, adjusting the pH value of the solution to 9-10, filtering, taking the filter liquor, mixing and adding acetic anhydride at the 50-60wt% amount of D-glucosamine hydrochlorate, mixing and reacting for 2h, using absolute ethyl alcohol to recrystallizing, filtering and recrystallizing via water, to obtain rod-shape food grade N-acetylaminoglucose.

本发明涉及一种N-乙酰氨基葡萄糖的合成方法。该方法的具体步骤为:将D-葡萄糖胺盐酸盐和乙醇按2~2.5∶100的质量比溶于水中,调节该溶液的pH值为9~10;过滤,取滤液,搅拌下加入乙酸酐,其加入量为原料D-葡萄糖胺盐酸盐量的50~60wt%;搅拌反应2小时后,用无水乙醇进行重结晶;过滤,晶体再用水重结晶,得棒状食品级N-乙酰氨基葡萄糖。

A type of novel dis-substituted α-arylglycine derivatives was synthesized in high yields and high regioselectivity via the stepwise Friedel-Crafts reaction of phenols with N-tosyl imino ester promoted by TiCl〓.

发现在Mg/MeOH/超声波条件下,能高产率的得到N-Tos裂解后N-Boc保护的α-芳香甘氨酸衍生物,实现了一条简单、实用的合成N-Boc保护的α-芳香甘氨酸衍生物的方法。

After model reproducing, the rabbits were randomized to receive a directly intramyocardial injection of either pcDNA3-bFGF 100μg (n=19) or pcDNA3 100μg (n=18). Animals were sacrificed 2, 6 or 12 weeks later, immunohistochemistry analysis was performed to study expression of bFGF gene at protein level, histologic analysis was performed to evaluate the effect of angiogenesis induced by gene therapy.

模型制备成功后将动物分为治疗组(n=19)和对照组(n=18),并于心肌内分别注射pcDNA3-bFGF100μg或pcDNA3 100μg,饲养至2、6、12周处死;免疫组化观察蛋白表达;行病理切片观察缺血坏死心肌面积的变化和缺血心肌内血管新生的情况。

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A.N.T.S.
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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。