查询词典 3-Pentanone

Using butanediol as initiator, boron-trifluoride etherate as catalyst, 3-azidomethyl-3-methyloxetane homopolymer was synthesized by the cationic polymerization of 3-azidomethyl-3-methyloxetane which was carried out in dichlorometane.

以1，4-丁二醇为引发剂，以三氟化硼乙醚络合物为催化剂，以3-叠氮甲基－3-甲基氧丁环为单体，以CH2Cl2为溶剂，按阳离子开环聚合机理，合成了含能粘合剂3-叠氮甲基－3-甲基氧丁环均聚物。

The one is-2-isopropylidene-3-[1-(3,4-dimethoxyphenyl)ethyl-idene] succinic anhydride, the other is-2-isopropylidene-3-[1-(3,4-methylenedioxyphenyl)- ethylidene] succinic anhydride.

合成了三种苯基俘精酸酐，其中具有给电子基的3-(3，4-二甲氧基苯基)亚乙基(2-亚丙基)丁二酸酐与3-(3，4-亚甲二氧基苯基)亚乙基(2-亚丙基)丁二酸酐是新化合物。

Chapter 2 has analysized the conversly synthetic means of solanesol and designed novelly synthetic routes of solanesol and key intermediate Chapter 3 has summarized the preparation of trans-3-methyl-4-hydroxy (bromo-2-butenyl oxy methyl benzene In chapter 4 ,a novel technology of important intermediate(all trans-8-bromo geranyl acetate),which is suitable for industrial procedure , was found .meanwhile,an another new way has been invented ,of which the key intermediate (all trans-8-hydroxy geranyl acetate) has been produced.

第二部分分析了茄尼醇的逆合成方法，设计了一条适合于合成茄尼醇的合成路线及其重要中间体的合成路线。第三部分研究了重要中间体[Trans-3-甲基-4-羟基-2-丁烯基乙酰基(苄基，2，3-二氢吡喃基)醚]的合成新方法，找到了一条适合于工业化生产的制备反式-3-甲基-4-羟基-2-丁烯基苄基醚的新方法。第四部分研究了重要中间体[-3，7-二甲基-8-羟基-2，6-辛二烯-1-醇乙酸酯、-3，7-二甲基-8-溴-2，6-辛二烯-1-醇乙酸酯]的合成新方法，找到了一条适合于工业化生产的制备它们的新方法；同时研究了一条制备-3，7-二甲基-8-羟基-2，6-辛二烯-1-醇乙酸酯的另一新方法。

Female flowers 1-3 at base of inflorescence, sometimes absent; pedicel distinct; sepals [2 or]3, irregularly triangular, fused at base, glandless; petals and disk absent; ovary [2 or]3-locular, smooth, usually glabrous; style present; stigmas [2 or]3, undivided, glandless.

在花序的基部的雌花1-3，有时无；花梗清楚；萼片 [2或者 ]3，不规则三角形，在基部愈合，无腺体；花瓣和花盘无；子房 [2或者 ]3室，平滑，通常无毛；花柱宿存柱头 [2或者 ]3，不裂，。

Tetrachloroterephthalic acid was prepared by chlorinating terephthalic acid, oleumsolvent and iodine catalyst. Tetrachloroterephthalic acid was acylated by sulphurous oxychloride in the presence of DMF to form tetrachloroterephthaloyl chloride. The acyl chloride product was fluorinated by potassium fluoride and esterified by methanol to synthesize dimethyl tetrafluoroterephthalate. The ester was reduced with potassium borohydride and lithium chloride to give tetrafluoroterephthalyl alcohol. The above product was bromated in the hydrobromic acid to obtain 4-bromomethyl-2,3,5,6-tetrafluoro-benzene methanol. 4-Methyl-2,3,5,-6-tetrafluorobenzene ethanol was obtained by reducing the bromide with magnesium. In the exist of DCC and DMAP, tefluthrin was got by the condensation reaction between 4-methyl-2,3,5,6-tetrafluoro-benzene methanol and-(1RS,3RS)- 3-(2- chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropanecar-boxylate acid.

对苯二甲酸与氯气在碘存在下以发烟硫酸为溶剂进行氯化制备四氯对苯二甲酸；再以DMF为催化剂与二氯亚砜反应生成四氯对苯二甲酰氯；以氟化钾为氟化剂，环丁砜为溶剂置换氟化，再与甲醇酯化得到四氟对苯二甲酸甲酯；以KBH4-LiCl为还原剂二甲醚为溶剂反应制得四氟对苯二甲基苄醇；以氯苯为溶剂在溴化氢溶液中溴化得到溴化产物；在乙醇溶液中经镁粉还原得到4-甲基-2，3，5，6-四氟苄醇；甲基苄醇与功夫酸在催化剂二环己基碳二亚胺和4-二甲氨基吡啶作用下缩合得到七氟菊酯，总收率达43.6%。

A mild and convenient method for the synthesis of 4(3)-substituted 3(4)-nitro-1H-pyrroles and 3-substituted 4-methyl-2-tosyl-1H-pyrroles from nitroolefins and tosylmethyl isocyanide in ionic liquid 1-butyl-3- methylimidazolium bromide was developed.

本文以离子液体－溴化1-丁基-3-甲基咪唑为溶剂，采用对甲苯磺酰基甲基异腈与硝基烯反应生成4(3)-取代-3(4)-硝基-1-氢吡咯或3-取代-4-甲基-2-对甲苯磺酰基-1-氢吡咯。

Methods :25 cases of traumatic hydrocephalus were analysed retrospectively.Among them,3 cases showed brain contusion,4 with subrarchnoid hemorrhage,5 with subdural effusion,2 with epidural hematoma,1 with subdural hematoma,1 with fracture of skull,3 with malacia lesions,3 with cerebral infarction,and 2 with cerebral hernia.The other 3 cases were not associated,with intracranial traumatic anomaly.

回顾分析25例外伤性脑积水，其中分别伴颅脑损伤有3例脑挫伤、4例蛛网膜下腔出血、5例硬膜下积液、1例颅骨骨折、3例脑内软化灶、3例脑梗塞、2例硬膜外血肿、1例硬膜下血肿、2例脑疝(大脑镰下疝及钩回疝各1例)，另3例颅内未见外伤性异常改变与其并存。

Results: Cerebral low density lesion was absorbed in 3 months;HIE might cause ext ernal hydrocephalus at 3rd-6th month,and EH disappeared one year later;HIE might cause periventricular leukomalacia after the 3rd month.The incidenc e of PVL was 11.6%,64.3%and 80%,respectively with mild,moderate and severe degree HIE,and that of severe degree PVL was 20%,33.3%and 75%. Severe degree HI E might cause cerebral malacia and atrophy (80%) in 2 months.

结果：HIE所致脑低密度灶在生后3个月内吸收消失；3～6个月时可引起外部性脑积水，1岁以后，EH的表现消失；3个月及以后可引起脑室周围白质软化症，其中轻、中、重度HIE的PVL发生率为11.6 ％、64.3％和80％；重度PVL的发生率为20％、33.3 ％和75％；重度HIE在2个月内可引起脑软化和脑萎缩(80％)。

The invention comprises that:(1) an injectant containing air is formed and the injectant is injected into a manto (3) through an injection well (2) or a recovery well (1);(2) the pressure of the injection well (2) and the recovery well is kept (1) for a period of time so that the oil and the injectant are mixed into more uniform fluid;(3) the pressure of the injection well (2) and the recovery well (1) is decreased, the pressure of the manto(3) is decreased and the oil-containing mixed fluid is obtained from the recovery well (1) or the injection well (2);(4) the procedure of (1),(2) and (3) is repeated, the pressure fluctuation of the fluid in the manto (3) is realized until the oil recovery rate is less than the economic recovery rate.

本发明包括：①形成包含气体的注入剂，将注入剂通过注入井(2)或采收井(1)注入矿层(3)；②保持注入井(2)和采收井(1)的压力一段时间，使油分和注入剂混合形成比较均匀的流体；③然后降低注入井(2)和采收井(1)的压力，降低矿层(3)压力，并在采收井(1)或者注入井(2)获取含油混合流体；④不断重复步骤①②③，实现矿层(3)中流体的压力波动，直到石油的采收率低于经济开采率为止。

The average weight of the tumors in control group, metronomic group and MTD group were (3.72±0.60)g,(1.85±0.38)g and (1.93±0.41)g, the average microvessel count were 26.38±2.56, 15.09±3.03 and 23.51±2.78, PCNA index were 83.88±3.72, 81.60±4.21 and 71.80±3.86, respectively.

对照组、节律组和MTD组皮下瘤重分别为(3.72±0.60)g、(1.85±0.38)g和(1.93±0.41)g，微血管计数分别为(26.35±2.56)个、(15.09±3.03)个和(23.51±2.78)个，PCNA指数分别为83.88±3.72、81.60±4.21和71.80±3.86。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。