查询词典 3-Pentanone

Methyl-2,3,5,6-tetrafluoro-benzene methanol was synthesized by chlorination, acylation, fluorination, esterifica- tion, reduction, bromization, reduction from terephthalic acid. Tefluthrin was obtained from-(1RS,3RS)-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropa-necarboxylate acid by reacting with 4-methyl-2,3,5,6-tetrafluoro-benzene methanol.

以对苯二甲酸为原料，经氯化、酰氯化、氟化、酯化、还原、溴化、还原七步反应合成了4-甲基-2，3，5，6-四氟苄醇，甲基苄醇与-(1RS，3RS)-3-(2-氯-3，3，3-三氟丙-1-丙烯基)-2，2-二甲基环丙甲酸一步酯化合成了七氟菊酯。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先，以巴豆醛与乙硫醇为原料，在三乙胺的催化作用下高收率制得3-乙硫基丁醛；然后从乙酰乙酸甲酯出发，通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮，接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环，再通过皂化和脱羧反应生成中间体5-[2-丙基]-1，3-环己二酮；再与丙酸酐反应丙酰化，最后与0-3-氯-2-丙烯基羟胺肟化，得到目标化合物烯草酮。

Three aspects were included here:The derivatives of dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid were synthesized via three different routes:(1) four new compounds were synthesized via the reaction bet ween dihydrol,2,4,5-tetrazine-3,5-dicarboxylic acid, thionyl chloride and corresponding alcohol ;(2) first ,dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate wer e synthesized, then ,another four new compounds were obtained t hrough the alcoholysis under the catalyst ;(3) three acylamines were got through the ammonolysis betw een dimethyl dihydro-1,2,4,5-tetrazine-3,5-dicarboxylate and amines.

本论文分别通过三条不同的路线合成了1，4-二氢-3，6-二甲酸-s-四嗪的衍生物：(1)通过1，4-二氢-3，6-二甲酸-s-四嗪与氯化亚砜和相应的醇反应，制备了四个新化合物；(2)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪，在催化剂的作用下，与高沸点的醇进行酯交换反应，合成了四个新化合物；(3)合成1，4-二氢-3，6-二甲酸甲酯-s-四嗪后，与胺进行氨解反应，合成三个新的1，4-二氢-3，6-二甲酰胺-s-四嗪化合物。

Formylation and diformylation of dithieno [2,3-b:3',2'-d] thiophene were prepared by two methods. Firstly, aromatic carbanions were prepared by 1 Br/Li exchange of bromo dithieno[2,3-b:3',2'-d]thiophene with n-BuLi in THF at low temperature; 2 deprotonation of dithieno[2,3-b:3',2'-d]thiophene with LDA.

二噻吩并[2，3-b：3'，2'-d]噻吩单醛与双醛的制备首先通过两种方法产生芳基负离子：1溴代并三噻吩在四氢呋喃中与正丁基锂发生的溴锂交换；2用LDA对二噻吩并[2，3-b：3'，2'-d]噻吩去质子化作用。

Forbesii, monoterpenes and sesquiterpenes account for 41.30% and 32.65%, respectively, in which (1R)-α-pinene (3.98%), sabinene (2.51%),(1S)-β-pinene (5.78%), m-cymene (4.05%), limonene (3.55%), 3, 7-dimethyl-1, 3, 7-octatriene (3.98%),γ-terpinene (8.70%), anisole (1.78%) and (1S)-endo-bornyl acetate (2.62%) as the monoterpenes and its derivatives, and-β-elemene (1.17%),α-bulnesene (1.40%),-β-bisabolene (1.21%),-elemol (1.42%), guaiol (1.14%), dehydroxyisocalamendiol (1.13%),-aristolene (1.99%), bulnesol (9.48%),γ-eudesmol (1.77%), guai-1(10)-en-11-ol (1.12%) and α-bisabolol (5.35 %) as the sesquiterpenes and its derivatives are the main components.

1R-α-蒎烯(3·98 %)、桧烯(2·51 %)、(1S)-β-蒎烯(5·78 %)、m-月桂烯(4·05 %)、柠檬烯(3·55 %)、3，7-二甲基-1，3，7-庚三烯(3·98 %)、γ-萜品烯(8·70 %)、茴香醚(1·78 %)和(1S)-桥环醋酸冰片酯(2·62 %)为单萜类化合物及其衍生物中的主要成分；-β-榄香烯(1·17 %)、异愈创木烯(1·40 %)、-β-没药烯(1·21 %)、-榄香醇(1·42 %)、愈创木醇(1·14 %)、去羟基异菖蒲二醇(1·13 %)、-土青木香烯(1·99 %)、异愈创木醇(9·48 %)、γ-桉醇(1·77 %)、愈创木-1(10)-烯-11-醇(1·12 %)和α-没药醇(5·35 %)为倍半萜类化合物及其衍生物中的主要成分。

We reconstructed the 3-D and virtual endoscopy image about nasal septum, frontal area of the apertura of sphenoidal sinus, sphenopalatine foramen, sphenopalatine artery and sphenoidal sinus use Volume Rendering, Multiplanar Reformation, Virtual Endoscopy and Curved Planar Reformat, and measured and ,about undertaked The nose, nasal septum, sphenopalatine artery, anterior region of the aperture of sphenoidal sinus, sphenopalatine artery and adjacent structures of hypophysial fossa were dissected, observed, measured and analysised the dependency anatomic structure at the same time.

结果： 一、标本解剖 1、鼻孔长径11.32±0.82(10.2~13.2)mm，鼻孔短径7.85±1.21(5.2~9.8)mm。鼻中隔厚度在前、中、后部分别为5.02±0.42(3.8~5.4)mm、5.57±0.47(4.5~6.4)mm、5.55±0.55(4.8~6.4) mm。 2、鼻中隔骨与软骨交界处距前鼻棘21.26±2.47(18.1~27.6)mm，距鼻孔内侧缘中点33.72±3.52(27.1~40.6)mm，距鼻小柱30.12±2.84(26.9~36.8)mm，距蝶窦口下缘38.04±3.49(32.4~45.1)mm，距后鼻孔41.82±3.96(36.9~50.1)mm。四方软骨中部厚度、边缘厚度、前后径、上下径分别为：1.12±0.13(0.92~1.42)mm、1.28±0.24 (0.83~1.67)mm、30.93±4.52(24.9~40.6)mm、29.94±2.14(24.8~34.3)mm。 3、蝶窦口长5.64±0.39(4.92~5.94)mm，宽3.58±0.22(3.10~3.96)mm，距上鼻甲尾部9.5±0.9(8.5~12.1)mm，距上鼻道未端14.5±1.1(12.5~16.4)mm，距中鼻甲尾

The invention adopts the technical proposal that the nucleation and process of growth of the molecular sieve are controlled properly in the synthetic process of the ZSM-5 molecular sieve material for producing the Magadiite/ZSM-5 intergrowth material, wherein the proportion of intergrown phases is adjustable, and the synthesized Magadiite/ZSM-5 intergrowth material adopts the compositions including the following mole relation: nSiO2:Al2O3, where n is between 50 and 1000 in the formula, and the method is characterized in that the Magadiite/ZSM-5 intergrowth material has two intergrown phases and an XRD diffraction pattern thereof has the d-space maximum value at the lengths of 15.73+-0.1, 11.14+-0.1, 9.97+-0.1, 7.74+-0.1, 5.14+-0.1, 3.86+-0.05, 3.66+-0.05, 3.45+-0.05, 3.30+-0.05 and 3.14+-0.1 angstroms, thereby solving the problems properly.

本发明通过采用在ZSM-5分子筛材料合成过程中，控制好分子筛的成核和生长过程，制备出了一种Magadiite/ZSM-5共生材料，其中共生物相比例可调，合成的Magadiite/ZSM-5共生材料采用包括以下摩尔关系的组成：nSiO2∶Al2O3，式中n＝50～1000，其特征在于所述Magadiite/ZSM-5共生材料具有两种共生物相，其XRD衍射图谱在15.73±0.1，11.14±0.1，9.97±0.1，7.74±0.1，5.14±0.1，3.86±0.05，3.66±0.05，3.45±0.05，3.30±0.05，3.14±0.1埃处有d-间距最大值的技术方案，较好地解决了上述问题。

Percentage of dressing, eviscerated carcass decreased significantly as dietaryω6/ω3 was reduced; percentage of abdominal fat, subcutaneous fat and intermuscular fat were higher in birds fed lower ratio diets. Drip loss in both breast and thigh muscle increased significantly in birds fedω6/ω3 ratio from 18 to 2.6. Except b* value in breast muscle decreased as birds fed dietary ratio from 5 to 2.6, the tendency for breast and thigh muscle were almost similar; a* values progressively increased as the diets contained increasingω3 content, changes in b* were also significant but the pattern was almost the reverse for changes in a*. Decreasing the dietaryω6/ω3 clearly increased the contents of ALA, EPA and DPA, but not for DHA.

结果表明：①饲喂10：1的日粮显著增加6周龄AA鸡的体重和日采食量；②随着日粮ω6/ω3比值的降低，屠宰率和净膛率显著下降；低ω6/ω3比值的日粮增加腹脂率、皮下脂肪和肌间脂肪；③日粮ω6/ω3比值从18下降到2.6时，胸、腿肌滴水损失显著下降；除日粮比值从5降到2.6时胸肌b*值下降外，胸、腿肌变化规律相似，a*值和b*值变化趋势相反：a*值下降，b*值上升；④日粮ω6/ω3的降低，ω3 PUFA中ALA、EPA和DPA显著增加；⑤肝脏中ALA含量低于胸肌，而其长链衍生物C20：3、EPA和DHA的含量则是肝脏中含量较高。

CT images of the 6 UAs showed homogenous and low density in comparison with muscles. Of the 6 UAs, 2 (33%) were lobulate, 4 (67%) were regularly round or oval; 1 (17%) had bone septa, 2 (33%) had root resorption of the neighboring teeth, 3 (50%) had cortical perforation. All UAs showed well-circumscribed margins without soft tissue masses. Three UAs were examined by enhanced studies and showed mild to moderate enhancement of the wall. Of the 5 MAs, 3 (60%) showed low to intermediate density as compared with muscles, 2 (40%) showed homogenous and intermediate density; 3 (60%) had bone septa; 3 (60%) showed root resorption or destruction of the neighboring teeth. All 5 MAs were lobulate with cortical perforation, soft tissue masses, and ill-defined margins. All 3 MA5 examined by enhanced studies showed strong enhancement. CONCLUSIONS: SMAs are usually seen in middle-aged patients.

UA病变平扫时与肌肉相比内部都呈均匀低密度，其中4例(67%)呈较规整的圆形或椭圆形，2例(33%)呈分叶状，3例(50%)局部骨皮质有缺损，但未见软组织肿块形成，l例(17%)见不全骨性分隔，2例(33%)邻近牙根有吸收，行增强扫描的3例囊壁均呈轻中度的强化。5例MA的病灶都呈分叶状，且骨皮质均被穿破并有软组织肿块形成，边界不清，其中3例(60%)平扫时与肌肉相比呈等低混杂密度，2例(40%)呈较均匀等密度，3例(60%)可见不全的骨性分隔，3例(60%)见牙根的吸收或破坏，行增强扫描的3例都呈明显强化。

The side effects in two groups were observed.Results 3~7 days after the end of treatment,the cure rate and efficacy rate were 64.3%and 82.5%in control group and 76.2%and 91.5%in trial group,respectively.3~7 days after menorrhea,the cure rate andefficacy rate were 65.9%and 83.3%in control group and 78.5%and 92.3%in trial group,respectively.There was a significant difference between two groups.

结果 停药后3~5 d，对照组的治愈率和有效率分别为64.3%和82.5%，试验组的治愈率和有效率分别为76.2%和91.5%；停药后下次月经来潮干净后3~7 d对照组的治愈率和有效率分别为65.9%和83.3%，试验组的治愈率和有效率分别为78.5%和92.3%；两组比较有显著性差异(P.05)。

The reasons of iron ions content overproof in grade Ⅱ desalting water system,such as variation water quality,contamination of regenerant , operation adjustment of pretreatment system and switching operation of bed were discussed.

对二级脱盐水系统中铁离子含量超标的原因，如来水水质发生波动、再生剂受到污染、预处理系统操作调整、床体运行切换等进行了论述。

You were hired to drum up new business, so go and do it.

公司雇你招徕新业务，你就做你的事好了。