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Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用&一勺烩&方法，以4-羟基苯甲腈为起始原料，首先与硫氢化钠和无水氯化镁在N，N-二甲基甲酰胺中反应，所得中间体不经分离，直接加入2-氯乙酰乙酸乙酯进行环合反应，得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（2）；然后通过六亚甲基四胺/三氟乙酸进行Duff反应，得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（3）；再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

Diamines are performed. An new and effective atom economy, domino reaction is developed, and 5, 6dihydro-4H-thieno [2, 3-b] thiopyran are synthesized by 4-(4-methyl-1, 3-dithiol-2-ylidene)-1, 7-diaryl-1, 6-diene-3, 5-dione

然后以4-[（4-甲基-1，3-二噻烷-2-亚甲基）-1，7-二芳基]-1，6-二烯-3，5-二酮类化合物为合成子探索稠杂环合成方法，并发现一个高效的，具有原子经济性的多米诺效应合成方法，并成功的利用其合成了一系列噻喃并噻吩衍生物。

Using the optimized MDCTA techniques, we prospectively scanned 23 consecutive patients with thoracoabdominal aortic aneurysms (aneurysmal dilatation of thoracic aorta in 7 and abdominal aorta in 10, 3 thoracoabdominal aortic dissecting aneurysms, and 3 aortic dissection) in same period of time.

采用上述MDCTA技术，纳入同期连续性的胸腹主动脉瘤病人作为病例组研究对象进行CT增强扫描，共计23例（胸主动脉瘤7例，腹主动脉瘤10例，胸腹主动脉夹层动脉瘤3例，胸腹主动脉夹层分离3例）。3。

An expansion monomer 3, 9-dihydroxymethyl-di (6-methyl-5 -hydroxyl)-2- heptanone-1, 5, 7, 11tetraoxaspiro [5, 5] undecane was synthesized and its volume change during polymerization is about +3.04%. Its prepolymer was also synthesized by toluene 2, 4-diisocyanide with it.

由三经甲基丙烷合成了螺环原碳酸酯单体3'、9'－二羟甲基－3'，9'-二乙基－1，5，7，11－-四氧杂螺环[5、5]十一烷单体（体积膨胀率＋3.04%）以及它的预聚物，并用其来改性环氧树脂B-63。

ResultsThere was no expression of Caspase-3 in group A. The expression of Caspase-3 in group C was decreased compared with that in group B（P＜0.01. In groups B and C, expansion and vacuolization of mitochondria, swollen neurons and apoptotic bodies appeared, which suggested that WBH could induce neuron injury, and the neuron injury in group C was more severe than that in group B.

结果A组大鼠海马区神经元无Caspase-3表达，B、C两组大鼠海马区神经元有Caspase-3表达，B组较C组Caspase-3表达平均灰度值减小。B、C两组大鼠海马神经元超微结构发生改变、细胞器水肿，部分线粒体空化，内质网稀疏，突触前膜、后膜结构不完整，可见自噬体结构；B组大鼠的神经元超微结构损害较C组轻。

In this research, the complete ipt gene was cloned from Agrobacterium pTiAch 58 Hind Ⅲ fragment and its promoter was re-constructed so that following three chimaeric genes were created:(1) ipt promoter plus ipt coding region and terminator ,(2) RuBP SSU 301 promoter from petunia plus ipt coding region and terminator ,(3) pea seed-specific vicilin promoter plus ipt coding region and terminator .

将ipt基因克隆后对其启动子进行了改造，分别构建了如下三种基因：（1）ipt启动子+ipt编码区和3′区，（2）磷酸核酮糖羧化酶小亚基启动子SSU 301+ipt编码区和3′区，（3）豌豆种子特异性启动子vicilin+ipt编码区和3′区。

Gas chromatography and mass spectrometry technique were employed to analyze the ginger oleoresin. This analysis resulted in the detection of 3 hitherto unknown natural compounds, 24 compounds previously reported as pungent compounds and 50 volatile compounds from ginger. The volatile compounds were mainly α-zingiberene (22.29%),β-sesquiphellandrene (8.58%),α-farnesene (3.93%),β-bisabolene (3.87%),α-curcumene (2.63%), which were mostly consisted of sesquiterpene hydrocarbons.

从姜油树脂中分析出77种化合物，其中挥发油成分50种，主要是α-姜烯(22.29%)、β-倍半水芹烯(8.58%)、α-法尼烯(3.93%)、β-没药烯(3.87%)和α-姜黄烯(2.63%)等倍半萜类化合物；姜辣素成分27种，主要成分为6-姜酚(9.38%)、6-姜烯酚(7.59%)和分析过程中由姜酚类或姜烯酚类化合物受热分解而形成的姜油酮(9.24%)。

As CAAX-mimetics, 1, 3-dihydro-5-phenyl-2-H-1, 4-benzodiazepin-2-one was modified by linking carboxyl groups with various carbon through N-1 and C-3, 3-(imidazol-4-yl) propion amido group with different substituents was connected at C-7; In the synthesis of bisubstrate analogues, thiocarbamido compounds was alkylated by alkyl iodide and then hydrolyzed to give alkylthiol benzoate compounds.

1，4-苯并二氮杂草-2-酮类化合物的合成过程中分别对其1、3、4和7位进行了基团变化，在1和3位连接不同长度含羧基或酯基的侧链，在7位连接不同取代的咪唑丙酰氨基。在苯甲酸硫醇酯化合物合成过程中，建立了一种硫原子连有不同长度碳链的苯甲酸硫醇酯的合成方法。

Conc1usion: CD4(superscript +)T cells subset may bear a part in protection induced in mice by mixed recombinant BCG-Em Ⅱ/3 and BCG-Em14-3-3 vaccine against challenge with Em protoscoleces.

CD4T细胞亚群在多房棘球绦虫重组BCG-Eml4-3-3疫苗诱导的小鼠抗Em原头节攻击感染的保护性免疫机制中起一定作用。

Product features include : 316 import hairpin will not break off if circumvolving by 180 degrees, repeating for three times remain 3-8KG pounds and 3/4 hardness. The 316L material machine's teeth are clear and teeth diameter discrepancy is +0.02mm etc.

产品的特色有：316进口发夹可连续三次180度不折断，反复折3次仍保持3-8KG磅力，3/4硬度316L料花枝牙缝清晰、牙直径差±0.02mm等等。

The reasons of iron ions content overproof in grade Ⅱ desalting water system,such as variation water quality,contamination of regenerant , operation adjustment of pretreatment system and switching operation of bed were discussed.

对二级脱盐水系统中铁离子含量超标的原因，如来水水质发生波动、再生剂受到污染、预处理系统操作调整、床体运行切换等进行了论述。

You were hired to drum up new business, so go and do it.

公司雇你招徕新业务，你就做你的事好了。